Structure of the oligosaccharides isolated from Prosopis juliflora (Sw.) DC. seed polysaccharide
•Partial hydrolysis of polysaccharide furnished three oligosaccharides.•Hydrolysis followed by GLC analysis furnished d-galactose and d-mannose.•Further studies indicated (1→4) mannose units linked to (1→6) galactose units. A water soluble polysaccharide isolated from Prosopis juliflora seed was pur...
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| Veröffentlicht in: | Carbohydrate polymers 2014-01, Vol.101, p.438-443 |
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| creator | Bhatia, Himani Gupta, P.K. Soni, P.L. |
| description | •Partial hydrolysis of polysaccharide furnished three oligosaccharides.•Hydrolysis followed by GLC analysis furnished d-galactose and d-mannose.•Further studies indicated (1→4) mannose units linked to (1→6) galactose units.
A water soluble polysaccharide isolated from Prosopis juliflora seed was purified and major homogenous fraction obtained by GPC. Complete hydrolysis of the polysaccharide followed by paper chromatography and GLC analysis indicated the presence of d-galactose and d-mannose in the ratio 1:1.10, respectively. Partial hydrolysis of the polysaccharide furnished one hepta-(I), one octa-(II) and nona-(III) saccharides. Hydrolysis of oligosaccharide I, II and III followed by GLC analysis furnished d-galactose and d-mannose in the ratio 3:4, 3:5 and 5:4, respectively. Methylation analysis, periodate oxidation and 1H NMR spectral studies of oligosaccharides indicated the presence of (1→4) mannose units linked to (1→6) galactose units. |
| doi_str_mv | 10.1016/j.carbpol.2013.09.039 |
| format | Article |
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A water soluble polysaccharide isolated from Prosopis juliflora seed was purified and major homogenous fraction obtained by GPC. Complete hydrolysis of the polysaccharide followed by paper chromatography and GLC analysis indicated the presence of d-galactose and d-mannose in the ratio 1:1.10, respectively. Partial hydrolysis of the polysaccharide furnished one hepta-(I), one octa-(II) and nona-(III) saccharides. Hydrolysis of oligosaccharide I, II and III followed by GLC analysis furnished d-galactose and d-mannose in the ratio 3:4, 3:5 and 5:4, respectively. Methylation analysis, periodate oxidation and 1H NMR spectral studies of oligosaccharides indicated the presence of (1→4) mannose units linked to (1→6) galactose units.</description><identifier>ISSN: 0144-8617</identifier><identifier>EISSN: 1879-1344</identifier><identifier>DOI: 10.1016/j.carbpol.2013.09.039</identifier><identifier>PMID: 24299795</identifier><identifier>CODEN: CAPOD8</identifier><language>eng</language><publisher>Kidlington: Elsevier Ltd</publisher><subject>Applied sciences ; Biological and medical sciences ; Carbohydrate Sequence ; Chemical constitution ; Exact sciences and technology ; Fundamental and applied biological sciences. Psychology ; Galactomannan ; Hydrolysis ; Molecular Sequence Data ; Natural polymers ; Oligosaccharide ; Oligosaccharides - chemistry ; Physicochemistry of polymers ; Plant physiology and development ; Polysaccharide ; Prosopis - chemistry ; Prosopis juliflora (Sw.) DC ; Seeds - chemistry ; Solubility ; Starch and polysaccharides ; Structure ; Water - chemistry</subject><ispartof>Carbohydrate polymers, 2014-01, Vol.101, p.438-443</ispartof><rights>2013 Elsevier Ltd</rights><rights>2015 INIST-CNRS</rights><rights>Copyright © 2013 Elsevier Ltd. All rights reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c395t-7374e2788774f12c7b2bf9fc49353c4b5d85161f40ad4b0ad5b6d652aa7ceaa03</citedby><cites>FETCH-LOGICAL-c395t-7374e2788774f12c7b2bf9fc49353c4b5d85161f40ad4b0ad5b6d652aa7ceaa03</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0144861713009314$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3536,27903,27904,65309</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=28344828$$DView record in Pascal Francis$$Hfree_for_read</backlink><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/24299795$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Bhatia, Himani</creatorcontrib><creatorcontrib>Gupta, P.K.</creatorcontrib><creatorcontrib>Soni, P.L.</creatorcontrib><title>Structure of the oligosaccharides isolated from Prosopis juliflora (Sw.) DC. seed polysaccharide</title><title>Carbohydrate polymers</title><addtitle>Carbohydr Polym</addtitle><description>•Partial hydrolysis of polysaccharide furnished three oligosaccharides.•Hydrolysis followed by GLC analysis furnished d-galactose and d-mannose.•Further studies indicated (1→4) mannose units linked to (1→6) galactose units.
A water soluble polysaccharide isolated from Prosopis juliflora seed was purified and major homogenous fraction obtained by GPC. Complete hydrolysis of the polysaccharide followed by paper chromatography and GLC analysis indicated the presence of d-galactose and d-mannose in the ratio 1:1.10, respectively. Partial hydrolysis of the polysaccharide furnished one hepta-(I), one octa-(II) and nona-(III) saccharides. Hydrolysis of oligosaccharide I, II and III followed by GLC analysis furnished d-galactose and d-mannose in the ratio 3:4, 3:5 and 5:4, respectively. Methylation analysis, periodate oxidation and 1H NMR spectral studies of oligosaccharides indicated the presence of (1→4) mannose units linked to (1→6) galactose units.</description><subject>Applied sciences</subject><subject>Biological and medical sciences</subject><subject>Carbohydrate Sequence</subject><subject>Chemical constitution</subject><subject>Exact sciences and technology</subject><subject>Fundamental and applied biological sciences. Psychology</subject><subject>Galactomannan</subject><subject>Hydrolysis</subject><subject>Molecular Sequence Data</subject><subject>Natural polymers</subject><subject>Oligosaccharide</subject><subject>Oligosaccharides - chemistry</subject><subject>Physicochemistry of polymers</subject><subject>Plant physiology and development</subject><subject>Polysaccharide</subject><subject>Prosopis - chemistry</subject><subject>Prosopis juliflora (Sw.) DC</subject><subject>Seeds - chemistry</subject><subject>Solubility</subject><subject>Starch and polysaccharides</subject><subject>Structure</subject><subject>Water - chemistry</subject><issn>0144-8617</issn><issn>1879-1344</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2014</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNqFkU1v3CAQhlGUKtls8xMScYm0OdgFG4w5RdH2U4rUSGnPFOMhYcUuG7Bb7b8P0TrZYznMXJ4XZh4QuqCkpIQ2n1al0bHbBl9WhNYlkSWp5RGa0VbIgtaMHaMZoYwVbUPFKTpLaUXyaSg5QacVq6QUks_Qn4chjmYYI-Bg8fCUm3ePIWljnnR0PSTsUvB6gB7bGNb4PoYUti7h1eid9SFqvHj4V17jz8sSJ8hYnml3yH9EH6z2Cc6nPke_v375tfxe3P389mN5e1eYWvKhELVgUIm2FYJZWhnRVZ2V1jBZ89qwjvctpw21jOiedbnwrukbXmktDGhN6jla7O_dxvA8QhrU2iUD3usNhDEpyhpOBeOCZpTvUZN3SRGs2ka31nGnKFGvctVKTXLVq1xFpMpyc-5yemLs1tC_p95sZuBqAnQy2tuoN8alA9fmb2lznaObPQdZyF8HUSXjYGOgdxHMoPrg_jPKCwnBmwI</recordid><startdate>20140130</startdate><enddate>20140130</enddate><creator>Bhatia, Himani</creator><creator>Gupta, P.K.</creator><creator>Soni, P.L.</creator><general>Elsevier Ltd</general><general>Elsevier</general><scope>IQODW</scope><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>20140130</creationdate><title>Structure of the oligosaccharides isolated from Prosopis juliflora (Sw.) DC. seed polysaccharide</title><author>Bhatia, Himani ; Gupta, P.K. ; Soni, P.L.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c395t-7374e2788774f12c7b2bf9fc49353c4b5d85161f40ad4b0ad5b6d652aa7ceaa03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2014</creationdate><topic>Applied sciences</topic><topic>Biological and medical sciences</topic><topic>Carbohydrate Sequence</topic><topic>Chemical constitution</topic><topic>Exact sciences and technology</topic><topic>Fundamental and applied biological sciences. Psychology</topic><topic>Galactomannan</topic><topic>Hydrolysis</topic><topic>Molecular Sequence Data</topic><topic>Natural polymers</topic><topic>Oligosaccharide</topic><topic>Oligosaccharides - chemistry</topic><topic>Physicochemistry of polymers</topic><topic>Plant physiology and development</topic><topic>Polysaccharide</topic><topic>Prosopis - chemistry</topic><topic>Prosopis juliflora (Sw.) DC</topic><topic>Seeds - chemistry</topic><topic>Solubility</topic><topic>Starch and polysaccharides</topic><topic>Structure</topic><topic>Water - chemistry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bhatia, Himani</creatorcontrib><creatorcontrib>Gupta, P.K.</creatorcontrib><creatorcontrib>Soni, P.L.</creatorcontrib><collection>Pascal-Francis</collection><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Carbohydrate polymers</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bhatia, Himani</au><au>Gupta, P.K.</au><au>Soni, P.L.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Structure of the oligosaccharides isolated from Prosopis juliflora (Sw.) DC. seed polysaccharide</atitle><jtitle>Carbohydrate polymers</jtitle><addtitle>Carbohydr Polym</addtitle><date>2014-01-30</date><risdate>2014</risdate><volume>101</volume><spage>438</spage><epage>443</epage><pages>438-443</pages><issn>0144-8617</issn><eissn>1879-1344</eissn><coden>CAPOD8</coden><abstract>•Partial hydrolysis of polysaccharide furnished three oligosaccharides.•Hydrolysis followed by GLC analysis furnished d-galactose and d-mannose.•Further studies indicated (1→4) mannose units linked to (1→6) galactose units.
A water soluble polysaccharide isolated from Prosopis juliflora seed was purified and major homogenous fraction obtained by GPC. Complete hydrolysis of the polysaccharide followed by paper chromatography and GLC analysis indicated the presence of d-galactose and d-mannose in the ratio 1:1.10, respectively. Partial hydrolysis of the polysaccharide furnished one hepta-(I), one octa-(II) and nona-(III) saccharides. Hydrolysis of oligosaccharide I, II and III followed by GLC analysis furnished d-galactose and d-mannose in the ratio 3:4, 3:5 and 5:4, respectively. Methylation analysis, periodate oxidation and 1H NMR spectral studies of oligosaccharides indicated the presence of (1→4) mannose units linked to (1→6) galactose units.</abstract><cop>Kidlington</cop><pub>Elsevier Ltd</pub><pmid>24299795</pmid><doi>10.1016/j.carbpol.2013.09.039</doi><tpages>6</tpages></addata></record> |
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| subjects | Applied sciences Biological and medical sciences Carbohydrate Sequence Chemical constitution Exact sciences and technology Fundamental and applied biological sciences. Psychology Galactomannan Hydrolysis Molecular Sequence Data Natural polymers Oligosaccharide Oligosaccharides - chemistry Physicochemistry of polymers Plant physiology and development Polysaccharide Prosopis - chemistry Prosopis juliflora (Sw.) DC Seeds - chemistry Solubility Starch and polysaccharides Structure Water - chemistry |
| title | Structure of the oligosaccharides isolated from Prosopis juliflora (Sw.) DC. seed polysaccharide |
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