Shape-controlled synthesis of silver nanocrystals via γ-irradiation in the presence of poly(vinyl pyrrolidone)
Silver nanocrystals with controlled morphologies were facilely synthesized via γ-irradiation on aqueous solutions containing AgNO3 and poly(vinyl pyrrolidone)(PVP) by adjusting the adsorption dose. UV–vis spectroscopy, TEM, XRD and X-ray photoelectron spectroscopy were used to characterize these sil...
Gespeichert in:
| Veröffentlicht in: | Journal of crystal growth 2013-06, Vol.372, p.116-120 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 120 |
|---|---|
| container_issue | |
| container_start_page | 116 |
| container_title | Journal of crystal growth |
| container_volume | 372 |
| creator | Zhao, Yongbin Chen, Aihua Liang, Shu |
| description | Silver nanocrystals with controlled morphologies were facilely synthesized via γ-irradiation on aqueous solutions containing AgNO3 and poly(vinyl pyrrolidone)(PVP) by adjusting the adsorption dose. UV–vis spectroscopy, TEM, XRD and X-ray photoelectron spectroscopy were used to characterize these silver nanocrystals. Spherical silver nanoparticles with diameter of ∼20nm were formed irradiated by γ-ray with dose of 12kGy, and one-dimensional silver nanowires with average diameter of 30nm and length up to 20–30μm were obtained with dose increased to 36kGy. In this process, γ-ray and PVP have synergistic effects on the formation of silver nanocrystals, leading to the formation of highly pure phase, as well as a uniform size of each structure.
•Silver nanocrystals with controlled morphologies were synthesized.•The irradiated aqueous solution contains AgNO3 and PVP.•The morphology was controlled by adjusting the adsorption dose.•PVP and γ-irradiation have synergistic effects on the morphologies.•The pure morphology was also proved by UV–vis spectra. |
| doi_str_mv | 10.1016/j.jcrysgro.2013.03.017 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1464548019</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><els_id>S0022024813002042</els_id><sourcerecordid>1464548019</sourcerecordid><originalsourceid>FETCH-LOGICAL-c375t-5f326b77af3987b369688dfcf723b8f8552f93d15ad81f4e41bbd39658c84d533</originalsourceid><addsrcrecordid>eNqFkMtqHDEQRUVIIBMnvxC0CTiLHuvRaql3CSYvMHhhey3UesQaZKmjag_0d-U_8k1RM062hqJqc8-91EXoPSV7SuhwcdgfbF3hZy17RijfkzZUvkA7qiTvBCHsJdq1zTrCevUavQE4ENJISnao3Nyb2Xe25KWWlLzDsObl3kMEXAKGmI6-4mxy2TIWkwAfo8F_fnexVuOiWWLJOGbcGDxXDz5bv5FzSev5MeY14XmtzTu6kv3Ht-hVaCb-3dM9Q3dfv9xefu-urr_9uPx81VkuxdKJwNkwSWkCH5Wc-DAOSrlgg2R8UkEJwcLIHRXGKRp639NpcnwchLKqd4LzM3R-8p1r-fXoYdEPEaxPyWRfHkHTfuhFrwgdm3Q4SW0tANUHPdf4YOqqKdFbw_qg_zWst4Y1aUNlAz88ZRiwJoVqso3wn2aSK9aLTffppPPt4WP0VYONW08uVm8X7Up8LuovPraYKw</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1464548019</pqid></control><display><type>article</type><title>Shape-controlled synthesis of silver nanocrystals via γ-irradiation in the presence of poly(vinyl pyrrolidone)</title><source>Elsevier ScienceDirect Journals</source><creator>Zhao, Yongbin ; Chen, Aihua ; Liang, Shu</creator><creatorcontrib>Zhao, Yongbin ; Chen, Aihua ; Liang, Shu</creatorcontrib><description>Silver nanocrystals with controlled morphologies were facilely synthesized via γ-irradiation on aqueous solutions containing AgNO3 and poly(vinyl pyrrolidone)(PVP) by adjusting the adsorption dose. UV–vis spectroscopy, TEM, XRD and X-ray photoelectron spectroscopy were used to characterize these silver nanocrystals. Spherical silver nanoparticles with diameter of ∼20nm were formed irradiated by γ-ray with dose of 12kGy, and one-dimensional silver nanowires with average diameter of 30nm and length up to 20–30μm were obtained with dose increased to 36kGy. In this process, γ-ray and PVP have synergistic effects on the formation of silver nanocrystals, leading to the formation of highly pure phase, as well as a uniform size of each structure.
•Silver nanocrystals with controlled morphologies were synthesized.•The irradiated aqueous solution contains AgNO3 and PVP.•The morphology was controlled by adjusting the adsorption dose.•PVP and γ-irradiation have synergistic effects on the morphologies.•The pure morphology was also proved by UV–vis spectra.</description><identifier>ISSN: 0022-0248</identifier><identifier>EISSN: 1873-5002</identifier><identifier>DOI: 10.1016/j.jcrysgro.2013.03.017</identifier><identifier>CODEN: JCRGAE</identifier><language>eng</language><publisher>Amsterdam: Elsevier B.V</publisher><subject>A1. Crystal morphology ; A1. Nanostructure ; A2. Growth from solutions ; B1. Nanomaterials ; Condensed matter: structure, mechanical and thermal properties ; Cross-disciplinary physics: materials science; rheology ; Exact sciences and technology ; Materials science ; Methods of nanofabrication ; Nanocrystals ; Nanoparticles ; Nanoscale materials and structures: fabrication and characterization ; Nanowires ; Other topics in nanoscale materials and structures ; Physics ; Quantum wires ; Silver ; Solid surfaces and solid-solid interfaces ; Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties) ; Synthesis ; Transmission electron microscopy ; X-rays</subject><ispartof>Journal of crystal growth, 2013-06, Vol.372, p.116-120</ispartof><rights>2013 Elsevier B.V.</rights><rights>2014 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c375t-5f326b77af3987b369688dfcf723b8f8552f93d15ad81f4e41bbd39658c84d533</citedby><cites>FETCH-LOGICAL-c375t-5f326b77af3987b369688dfcf723b8f8552f93d15ad81f4e41bbd39658c84d533</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://dx.doi.org/10.1016/j.jcrysgro.2013.03.017$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,777,781,3537,27905,27906,45976</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=27382457$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Zhao, Yongbin</creatorcontrib><creatorcontrib>Chen, Aihua</creatorcontrib><creatorcontrib>Liang, Shu</creatorcontrib><title>Shape-controlled synthesis of silver nanocrystals via γ-irradiation in the presence of poly(vinyl pyrrolidone)</title><title>Journal of crystal growth</title><description>Silver nanocrystals with controlled morphologies were facilely synthesized via γ-irradiation on aqueous solutions containing AgNO3 and poly(vinyl pyrrolidone)(PVP) by adjusting the adsorption dose. UV–vis spectroscopy, TEM, XRD and X-ray photoelectron spectroscopy were used to characterize these silver nanocrystals. Spherical silver nanoparticles with diameter of ∼20nm were formed irradiated by γ-ray with dose of 12kGy, and one-dimensional silver nanowires with average diameter of 30nm and length up to 20–30μm were obtained with dose increased to 36kGy. In this process, γ-ray and PVP have synergistic effects on the formation of silver nanocrystals, leading to the formation of highly pure phase, as well as a uniform size of each structure.
•Silver nanocrystals with controlled morphologies were synthesized.•The irradiated aqueous solution contains AgNO3 and PVP.•The morphology was controlled by adjusting the adsorption dose.•PVP and γ-irradiation have synergistic effects on the morphologies.•The pure morphology was also proved by UV–vis spectra.</description><subject>A1. Crystal morphology</subject><subject>A1. Nanostructure</subject><subject>A2. Growth from solutions</subject><subject>B1. Nanomaterials</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Exact sciences and technology</subject><subject>Materials science</subject><subject>Methods of nanofabrication</subject><subject>Nanocrystals</subject><subject>Nanoparticles</subject><subject>Nanoscale materials and structures: fabrication and characterization</subject><subject>Nanowires</subject><subject>Other topics in nanoscale materials and structures</subject><subject>Physics</subject><subject>Quantum wires</subject><subject>Silver</subject><subject>Solid surfaces and solid-solid interfaces</subject><subject>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</subject><subject>Synthesis</subject><subject>Transmission electron microscopy</subject><subject>X-rays</subject><issn>0022-0248</issn><issn>1873-5002</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNqFkMtqHDEQRUVIIBMnvxC0CTiLHuvRaql3CSYvMHhhey3UesQaZKmjag_0d-U_8k1RM062hqJqc8-91EXoPSV7SuhwcdgfbF3hZy17RijfkzZUvkA7qiTvBCHsJdq1zTrCevUavQE4ENJISnao3Nyb2Xe25KWWlLzDsObl3kMEXAKGmI6-4mxy2TIWkwAfo8F_fnexVuOiWWLJOGbcGDxXDz5bv5FzSev5MeY14XmtzTu6kv3Ht-hVaCb-3dM9Q3dfv9xefu-urr_9uPx81VkuxdKJwNkwSWkCH5Wc-DAOSrlgg2R8UkEJwcLIHRXGKRp639NpcnwchLKqd4LzM3R-8p1r-fXoYdEPEaxPyWRfHkHTfuhFrwgdm3Q4SW0tANUHPdf4YOqqKdFbw_qg_zWst4Y1aUNlAz88ZRiwJoVqso3wn2aSK9aLTffppPPt4WP0VYONW08uVm8X7Up8LuovPraYKw</recordid><startdate>20130601</startdate><enddate>20130601</enddate><creator>Zhao, Yongbin</creator><creator>Chen, Aihua</creator><creator>Liang, Shu</creator><general>Elsevier B.V</general><general>Elsevier</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20130601</creationdate><title>Shape-controlled synthesis of silver nanocrystals via γ-irradiation in the presence of poly(vinyl pyrrolidone)</title><author>Zhao, Yongbin ; Chen, Aihua ; Liang, Shu</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c375t-5f326b77af3987b369688dfcf723b8f8552f93d15ad81f4e41bbd39658c84d533</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>A1. Crystal morphology</topic><topic>A1. Nanostructure</topic><topic>A2. Growth from solutions</topic><topic>B1. Nanomaterials</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Exact sciences and technology</topic><topic>Materials science</topic><topic>Methods of nanofabrication</topic><topic>Nanocrystals</topic><topic>Nanoparticles</topic><topic>Nanoscale materials and structures: fabrication and characterization</topic><topic>Nanowires</topic><topic>Other topics in nanoscale materials and structures</topic><topic>Physics</topic><topic>Quantum wires</topic><topic>Silver</topic><topic>Solid surfaces and solid-solid interfaces</topic><topic>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</topic><topic>Synthesis</topic><topic>Transmission electron microscopy</topic><topic>X-rays</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zhao, Yongbin</creatorcontrib><creatorcontrib>Chen, Aihua</creatorcontrib><creatorcontrib>Liang, Shu</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of crystal growth</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zhao, Yongbin</au><au>Chen, Aihua</au><au>Liang, Shu</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Shape-controlled synthesis of silver nanocrystals via γ-irradiation in the presence of poly(vinyl pyrrolidone)</atitle><jtitle>Journal of crystal growth</jtitle><date>2013-06-01</date><risdate>2013</risdate><volume>372</volume><spage>116</spage><epage>120</epage><pages>116-120</pages><issn>0022-0248</issn><eissn>1873-5002</eissn><coden>JCRGAE</coden><abstract>Silver nanocrystals with controlled morphologies were facilely synthesized via γ-irradiation on aqueous solutions containing AgNO3 and poly(vinyl pyrrolidone)(PVP) by adjusting the adsorption dose. UV–vis spectroscopy, TEM, XRD and X-ray photoelectron spectroscopy were used to characterize these silver nanocrystals. Spherical silver nanoparticles with diameter of ∼20nm were formed irradiated by γ-ray with dose of 12kGy, and one-dimensional silver nanowires with average diameter of 30nm and length up to 20–30μm were obtained with dose increased to 36kGy. In this process, γ-ray and PVP have synergistic effects on the formation of silver nanocrystals, leading to the formation of highly pure phase, as well as a uniform size of each structure.
•Silver nanocrystals with controlled morphologies were synthesized.•The irradiated aqueous solution contains AgNO3 and PVP.•The morphology was controlled by adjusting the adsorption dose.•PVP and γ-irradiation have synergistic effects on the morphologies.•The pure morphology was also proved by UV–vis spectra.</abstract><cop>Amsterdam</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jcrysgro.2013.03.017</doi><tpages>5</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0022-0248 |
| ispartof | Journal of crystal growth, 2013-06, Vol.372, p.116-120 |
| issn | 0022-0248 1873-5002 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1464548019 |
| source | Elsevier ScienceDirect Journals |
| subjects | A1. Crystal morphology A1. Nanostructure A2. Growth from solutions B1. Nanomaterials Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology Exact sciences and technology Materials science Methods of nanofabrication Nanocrystals Nanoparticles Nanoscale materials and structures: fabrication and characterization Nanowires Other topics in nanoscale materials and structures Physics Quantum wires Silver Solid surfaces and solid-solid interfaces Surfaces and interfaces thin films and whiskers (structure and nonelectronic properties) Synthesis Transmission electron microscopy X-rays |
| title | Shape-controlled synthesis of silver nanocrystals via γ-irradiation in the presence of poly(vinyl pyrrolidone) |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-19T13%3A22%3A36IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Shape-controlled%20synthesis%20of%20silver%20nanocrystals%20via%20%CE%B3-irradiation%20in%20the%20presence%20of%20poly(vinyl%20pyrrolidone)&rft.jtitle=Journal%20of%20crystal%20growth&rft.au=Zhao,%20Yongbin&rft.date=2013-06-01&rft.volume=372&rft.spage=116&rft.epage=120&rft.pages=116-120&rft.issn=0022-0248&rft.eissn=1873-5002&rft.coden=JCRGAE&rft_id=info:doi/10.1016/j.jcrysgro.2013.03.017&rft_dat=%3Cproquest_cross%3E1464548019%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1464548019&rft_id=info:pmid/&rft_els_id=S0022024813002042&rfr_iscdi=true |