High-performance liquid chromatographic enantioseparation of isoxazoline-fused 2-aminocyclopentanecarboxylic acids on a chiral ligand-exchange stationary phase

The application of a chiral ligand‐exchange column for the direct high‐performance liquid chromatographic enantioseparation of unusual β‐amino acids with a sodium N‐((R)‐2‐hydroxy‐1‐phenylethyl)‐N‐undecylaminoacetate‐Cu(II) complex as chiral selector is reported. The investigated amino acids were is...

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Veröffentlicht in:	Journal of separation science 2013-04, Vol.36 (8), p.1335-1342
Hauptverfasser:	Gecse, Zsanett, Ilisz, István, Nonn, Melinda, Grecsó, Nóra, Fülöp, Ferenc, Agneeswari, Rajalingam, Hyun, Myung Ho, Péter, Antal
Format:	Artikel
Sprache:	eng
Schlagworte:	Amino acids Analytical chemistry Chemistry Chiral ligand-exchange chromatography Chromatographic methods and physical methods associated with chromatography Chromatography Chromatography, High Pressure Liquid - methods Cycloleucine - analogs & derivatives Cycloleucine - chemistry Exact sciences and technology Isoxazoles - chemistry Isoxazoline-fused 2-aminocyclopentanecarboxylic acids Ligands Liquids Mathematical analysis Optimization Other chromatographic methods Selectors Separation Sodium Sodium N-((R)-2-hydroxy-1-phenylethyl)-N-undecylaminoacetate-based column Stereoisomerism Thermodynamics
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