Identification of radiation‐induced radical structure in azocalix[4]arene: an EPR study

A macrocyclic azocalix[4]arene (1) based ester derivative was synthesized. The single crystals of azocalix[4]arene were produced by slow evaporation of concentrated ethyl acetate solutions. These single crystals were exposed to 60Co gamma rays with a dose rate of 0.980 kGy h‐1 for 48 and 72 h to pro...

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Veröffentlicht in:	Magnetic resonance in chemistry 2013-10, Vol.51 (10), p.671-675
Hauptverfasser:	Usta, Keziban, Ozen Karakus, Ozlem, Usta, Ayhan, Deligoz, Hasalettin
Format:	Artikel
Sprache:	eng
Schlagworte:	azocalixarene Bonding Carbon chemical synthesis electron paramagnetic resonance (EPR) Esters Free radicals irradiation effects Radicals Scission Single crystals Spectra
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