Effect of processing techniques on the performance of Epoxy/MWCNT nanocomposites
The aim of this study is to investigate the optimum technique to disperse Multi‐Walled Carbon Nanotubes (MWCNTs) in SC‐1 epoxy uniformly and to evaluate the effect of processing technique on the performance of SC‐1 epoxy. To achieve better dispersion, MWCNT was mixed with SC‐1 resin directly or prem...
Gespeichert in:
| Veröffentlicht in: | Journal of applied polymer science 2013-03, Vol.127 (6), p.4211-4224 |
|---|---|
| Hauptverfasser: | , , , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 4224 |
|---|---|
| container_issue | 6 |
| container_start_page | 4211 |
| container_title | Journal of applied polymer science |
| container_volume | 127 |
| creator | Hosur, Mahesh Barua, Rajib Zainuddin, Shaik Kumar, Ashok Trovillion, Jonathan Jeelani, Shaik |
| description | The aim of this study is to investigate the optimum technique to disperse Multi‐Walled Carbon Nanotubes (MWCNTs) in SC‐1 epoxy uniformly and to evaluate the effect of processing technique on the performance of SC‐1 epoxy. To achieve better dispersion, MWCNT was mixed with SC‐1 resin directly or premixed with a solvent and then mixed with SC‐1 resin after evaporating the solvent using sonication, thinky mixing and three‐roll mill methods either in isolation or combination. Flexural tests were performed to evaluate mechanical performances and results exhibit up to 27.13, 13.51, and 21.99% improvement on flexural strength, flexural modulus, and maximum strain, respectively, over neat epoxy with only 0.2 wt % loading. Dynamic mechanical analysis (DMA), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) indicated improvement in storage modulus, Tg, inflection temperature, and residue content, respectively over neat SC‐1 epoxy. Thermal and mechanical properties at higher loading conditions were seen to either reduce or not significantly improve. This was attributed to high viscosity of nanocomposites as determined by rheological analysis which prevents good dispersion of MWNCTs into epoxy system at 0.4 wt % loading. © 2012 Wiley Periodicals, Inc. J. Appl. Polym. Sci., 2013 |
| doi_str_mv | 10.1002/app.37990 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_miscellaneous_1439780976</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1439780976</sourcerecordid><originalsourceid>FETCH-LOGICAL-c3980-6a82720a022d2ead972906985304949c5bfc827ff359d1daf25a80805d787dfa3</originalsourceid><addsrcrecordid>eNp1kEtLAzEUhYMoWKsL_8GACLqYNo-ZPJZSahVq7aI-diFmEjt1OhmTKbb_3tSqC8HVXdzvfBwOAKcI9hCEuK-apkeYEHAPdBAULM0o5vugE38o5ULkh-AohAWECOWQdsB0aK3RbeJs0ninTQhl_Zq0Rs_r8n1lQuLqpJ2bpDHeOr9UtTZbdti49aZ_9zSYzJJa1U67ZeNC2ZpwDA6sqoI5-b5d8HA9nA1u0vH96HZwNU41ERymVHHMMFQQ4wIbVQiGBaSC5wRmIhM6f7E6EtaSXBSoUBbnikMO84JxVlhFuuBi5421t0VbuSyDNlWlauNWQaKMCMbjAjSiZ3_QhVv5OraTCGeYE5oxEqnLHaW9C8EbKxtfLpXfSATldlsZt5Vf20b2_NuoglaV9XGXMvwGMBWI0i9nf8d9lJXZ_C-UV9PpjzndJcrQmvVvQvk3GYUsl0-TkcyyweT5cTaWI_IJhLmVtQ</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1242836473</pqid></control><display><type>article</type><title>Effect of processing techniques on the performance of Epoxy/MWCNT nanocomposites</title><source>Wiley Online Library Journals Frontfile Complete</source><creator>Hosur, Mahesh ; Barua, Rajib ; Zainuddin, Shaik ; Kumar, Ashok ; Trovillion, Jonathan ; Jeelani, Shaik</creator><creatorcontrib>Hosur, Mahesh ; Barua, Rajib ; Zainuddin, Shaik ; Kumar, Ashok ; Trovillion, Jonathan ; Jeelani, Shaik</creatorcontrib><description>The aim of this study is to investigate the optimum technique to disperse Multi‐Walled Carbon Nanotubes (MWCNTs) in SC‐1 epoxy uniformly and to evaluate the effect of processing technique on the performance of SC‐1 epoxy. To achieve better dispersion, MWCNT was mixed with SC‐1 resin directly or premixed with a solvent and then mixed with SC‐1 resin after evaporating the solvent using sonication, thinky mixing and three‐roll mill methods either in isolation or combination. Flexural tests were performed to evaluate mechanical performances and results exhibit up to 27.13, 13.51, and 21.99% improvement on flexural strength, flexural modulus, and maximum strain, respectively, over neat epoxy with only 0.2 wt % loading. Dynamic mechanical analysis (DMA), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) indicated improvement in storage modulus, Tg, inflection temperature, and residue content, respectively over neat SC‐1 epoxy. Thermal and mechanical properties at higher loading conditions were seen to either reduce or not significantly improve. This was attributed to high viscosity of nanocomposites as determined by rheological analysis which prevents good dispersion of MWNCTs into epoxy system at 0.4 wt % loading. © 2012 Wiley Periodicals, Inc. J. Appl. Polym. Sci., 2013</description><identifier>ISSN: 0021-8995</identifier><identifier>EISSN: 1097-4628</identifier><identifier>DOI: 10.1002/app.37990</identifier><identifier>CODEN: JAPNAB</identifier><language>eng</language><publisher>Hoboken: Wiley Subscription Services, Inc., A Wiley Company</publisher><subject>Applied sciences ; Composites ; Differential scanning calorimetry ; Dispersions ; Exact sciences and technology ; flexure ; Forms of application and semi-finished materials ; Materials science ; Modulus of rupture in bending ; multiwalled carbon nanotubes ; Nanocomposites ; Polymer industry, paints, wood ; Polymers ; Reproduction ; Resins ; rheology ; Solvents ; Technology of polymers ; thermal properties</subject><ispartof>Journal of applied polymer science, 2013-03, Vol.127 (6), p.4211-4224</ispartof><rights>Copyright © 2012 Wiley Periodicals, Inc.</rights><rights>2014 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c3980-6a82720a022d2ead972906985304949c5bfc827ff359d1daf25a80805d787dfa3</citedby><cites>FETCH-LOGICAL-c3980-6a82720a022d2ead972906985304949c5bfc827ff359d1daf25a80805d787dfa3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fapp.37990$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fapp.37990$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,777,781,1412,27905,27906,45555,45556</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=26916673$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Hosur, Mahesh</creatorcontrib><creatorcontrib>Barua, Rajib</creatorcontrib><creatorcontrib>Zainuddin, Shaik</creatorcontrib><creatorcontrib>Kumar, Ashok</creatorcontrib><creatorcontrib>Trovillion, Jonathan</creatorcontrib><creatorcontrib>Jeelani, Shaik</creatorcontrib><title>Effect of processing techniques on the performance of Epoxy/MWCNT nanocomposites</title><title>Journal of applied polymer science</title><addtitle>J. Appl. Polym. Sci</addtitle><description>The aim of this study is to investigate the optimum technique to disperse Multi‐Walled Carbon Nanotubes (MWCNTs) in SC‐1 epoxy uniformly and to evaluate the effect of processing technique on the performance of SC‐1 epoxy. To achieve better dispersion, MWCNT was mixed with SC‐1 resin directly or premixed with a solvent and then mixed with SC‐1 resin after evaporating the solvent using sonication, thinky mixing and three‐roll mill methods either in isolation or combination. Flexural tests were performed to evaluate mechanical performances and results exhibit up to 27.13, 13.51, and 21.99% improvement on flexural strength, flexural modulus, and maximum strain, respectively, over neat epoxy with only 0.2 wt % loading. Dynamic mechanical analysis (DMA), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) indicated improvement in storage modulus, Tg, inflection temperature, and residue content, respectively over neat SC‐1 epoxy. Thermal and mechanical properties at higher loading conditions were seen to either reduce or not significantly improve. This was attributed to high viscosity of nanocomposites as determined by rheological analysis which prevents good dispersion of MWNCTs into epoxy system at 0.4 wt % loading. © 2012 Wiley Periodicals, Inc. J. Appl. Polym. Sci., 2013</description><subject>Applied sciences</subject><subject>Composites</subject><subject>Differential scanning calorimetry</subject><subject>Dispersions</subject><subject>Exact sciences and technology</subject><subject>flexure</subject><subject>Forms of application and semi-finished materials</subject><subject>Materials science</subject><subject>Modulus of rupture in bending</subject><subject>multiwalled carbon nanotubes</subject><subject>Nanocomposites</subject><subject>Polymer industry, paints, wood</subject><subject>Polymers</subject><subject>Reproduction</subject><subject>Resins</subject><subject>rheology</subject><subject>Solvents</subject><subject>Technology of polymers</subject><subject>thermal properties</subject><issn>0021-8995</issn><issn>1097-4628</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><recordid>eNp1kEtLAzEUhYMoWKsL_8GACLqYNo-ZPJZSahVq7aI-diFmEjt1OhmTKbb_3tSqC8HVXdzvfBwOAKcI9hCEuK-apkeYEHAPdBAULM0o5vugE38o5ULkh-AohAWECOWQdsB0aK3RbeJs0ninTQhl_Zq0Rs_r8n1lQuLqpJ2bpDHeOr9UtTZbdti49aZ_9zSYzJJa1U67ZeNC2ZpwDA6sqoI5-b5d8HA9nA1u0vH96HZwNU41ERymVHHMMFQQ4wIbVQiGBaSC5wRmIhM6f7E6EtaSXBSoUBbnikMO84JxVlhFuuBi5421t0VbuSyDNlWlauNWQaKMCMbjAjSiZ3_QhVv5OraTCGeYE5oxEqnLHaW9C8EbKxtfLpXfSATldlsZt5Vf20b2_NuoglaV9XGXMvwGMBWI0i9nf8d9lJXZ_C-UV9PpjzndJcrQmvVvQvk3GYUsl0-TkcyyweT5cTaWI_IJhLmVtQ</recordid><startdate>20130315</startdate><enddate>20130315</enddate><creator>Hosur, Mahesh</creator><creator>Barua, Rajib</creator><creator>Zainuddin, Shaik</creator><creator>Kumar, Ashok</creator><creator>Trovillion, Jonathan</creator><creator>Jeelani, Shaik</creator><general>Wiley Subscription Services, Inc., A Wiley Company</general><general>Wiley</general><general>Wiley Subscription Services, Inc</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20130315</creationdate><title>Effect of processing techniques on the performance of Epoxy/MWCNT nanocomposites</title><author>Hosur, Mahesh ; Barua, Rajib ; Zainuddin, Shaik ; Kumar, Ashok ; Trovillion, Jonathan ; Jeelani, Shaik</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c3980-6a82720a022d2ead972906985304949c5bfc827ff359d1daf25a80805d787dfa3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Applied sciences</topic><topic>Composites</topic><topic>Differential scanning calorimetry</topic><topic>Dispersions</topic><topic>Exact sciences and technology</topic><topic>flexure</topic><topic>Forms of application and semi-finished materials</topic><topic>Materials science</topic><topic>Modulus of rupture in bending</topic><topic>multiwalled carbon nanotubes</topic><topic>Nanocomposites</topic><topic>Polymer industry, paints, wood</topic><topic>Polymers</topic><topic>Reproduction</topic><topic>Resins</topic><topic>rheology</topic><topic>Solvents</topic><topic>Technology of polymers</topic><topic>thermal properties</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Hosur, Mahesh</creatorcontrib><creatorcontrib>Barua, Rajib</creatorcontrib><creatorcontrib>Zainuddin, Shaik</creatorcontrib><creatorcontrib>Kumar, Ashok</creatorcontrib><creatorcontrib>Trovillion, Jonathan</creatorcontrib><creatorcontrib>Jeelani, Shaik</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of applied polymer science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Hosur, Mahesh</au><au>Barua, Rajib</au><au>Zainuddin, Shaik</au><au>Kumar, Ashok</au><au>Trovillion, Jonathan</au><au>Jeelani, Shaik</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Effect of processing techniques on the performance of Epoxy/MWCNT nanocomposites</atitle><jtitle>Journal of applied polymer science</jtitle><addtitle>J. Appl. Polym. Sci</addtitle><date>2013-03-15</date><risdate>2013</risdate><volume>127</volume><issue>6</issue><spage>4211</spage><epage>4224</epage><pages>4211-4224</pages><issn>0021-8995</issn><eissn>1097-4628</eissn><coden>JAPNAB</coden><abstract>The aim of this study is to investigate the optimum technique to disperse Multi‐Walled Carbon Nanotubes (MWCNTs) in SC‐1 epoxy uniformly and to evaluate the effect of processing technique on the performance of SC‐1 epoxy. To achieve better dispersion, MWCNT was mixed with SC‐1 resin directly or premixed with a solvent and then mixed with SC‐1 resin after evaporating the solvent using sonication, thinky mixing and three‐roll mill methods either in isolation or combination. Flexural tests were performed to evaluate mechanical performances and results exhibit up to 27.13, 13.51, and 21.99% improvement on flexural strength, flexural modulus, and maximum strain, respectively, over neat epoxy with only 0.2 wt % loading. Dynamic mechanical analysis (DMA), differential scanning calorimetry (DSC), thermogravimetric analysis (TGA) indicated improvement in storage modulus, Tg, inflection temperature, and residue content, respectively over neat SC‐1 epoxy. Thermal and mechanical properties at higher loading conditions were seen to either reduce or not significantly improve. This was attributed to high viscosity of nanocomposites as determined by rheological analysis which prevents good dispersion of MWNCTs into epoxy system at 0.4 wt % loading. © 2012 Wiley Periodicals, Inc. J. Appl. Polym. Sci., 2013</abstract><cop>Hoboken</cop><pub>Wiley Subscription Services, Inc., A Wiley Company</pub><doi>10.1002/app.37990</doi><tpages>14</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0021-8995 |
| ispartof | Journal of applied polymer science, 2013-03, Vol.127 (6), p.4211-4224 |
| issn | 0021-8995 1097-4628 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1439780976 |
| source | Wiley Online Library Journals Frontfile Complete |
| subjects | Applied sciences Composites Differential scanning calorimetry Dispersions Exact sciences and technology flexure Forms of application and semi-finished materials Materials science Modulus of rupture in bending multiwalled carbon nanotubes Nanocomposites Polymer industry, paints, wood Polymers Reproduction Resins rheology Solvents Technology of polymers thermal properties |
| title | Effect of processing techniques on the performance of Epoxy/MWCNT nanocomposites |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-19T22%3A09%3A25IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_cross&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Effect%20of%20processing%20techniques%20on%20the%20performance%20of%20Epoxy/MWCNT%20nanocomposites&rft.jtitle=Journal%20of%20applied%20polymer%20science&rft.au=Hosur,%20Mahesh&rft.date=2013-03-15&rft.volume=127&rft.issue=6&rft.spage=4211&rft.epage=4224&rft.pages=4211-4224&rft.issn=0021-8995&rft.eissn=1097-4628&rft.coden=JAPNAB&rft_id=info:doi/10.1002/app.37990&rft_dat=%3Cproquest_cross%3E1439780976%3C/proquest_cross%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1242836473&rft_id=info:pmid/&rfr_iscdi=true |