Rapid synthesis of pure DD3R zeolite using ball-milled Sigma-1 seeds under static conditions
Deca-Dodecasil 3 Rhombohedral (DD3R) zeolite has great potential applications in the separation of gases with small molecular size; however, the extremely long crystallization time and the generated impure phases such as Sigma-Two (SGT) and Dodecasil 1H (DOH) have been the main obstacles for commerc...
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| Veröffentlicht in: | Journal of materials science 2013-09, Vol.48 (18), p.6286-6292 |
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| container_title | Journal of materials science |
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| creator | Zheng, Fangyuan Jing, Wenheng Gu, Xuehong Xu, Nanping Dong, Junhang |
| description | Deca-Dodecasil 3 Rhombohedral (DD3R) zeolite has great potential applications in the separation of gases with small molecular size; however, the extremely long crystallization time and the generated impure phases such as Sigma-Two (SGT) and Dodecasil 1H (DOH) have been the main obstacles for commercial utilization. In this work, ball-milled Sigma-1 was used as seeds for the first time to induce the crystallization of DD3R crystals. Pure DD3R zeolite was successfully produced under static conditions with drastically reduced crystallization time of ca. 9 h. The new synthesis approach showed 100 % of repeatability to obtain pure DD3R zeolite. |
| doi_str_mv | 10.1007/s10853-013-7428-0 |
| format | Article |
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In this work, ball-milled Sigma-1 was used as seeds for the first time to induce the crystallization of DD3R crystals. Pure DD3R zeolite was successfully produced under static conditions with drastically reduced crystallization time of ca. 9 h. 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In this work, ball-milled Sigma-1 was used as seeds for the first time to induce the crystallization of DD3R crystals. Pure DD3R zeolite was successfully produced under static conditions with drastically reduced crystallization time of ca. 9 h. The new synthesis approach showed 100 % of repeatability to obtain pure DD3R zeolite.</description><subject>Ball milling</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Classical Mechanics</subject><subject>Crystallization</subject><subject>Crystallography and Scattering Methods</subject><subject>Crystals</subject><subject>Materials Science</subject><subject>Phases</subject><subject>Polymer Sciences</subject><subject>Reproducibility</subject><subject>Seeds</subject><subject>Silica</subject><subject>Solid Mechanics</subject><subject>Synthesis</subject><subject>Zeolites</subject><issn>0022-2461</issn><issn>1573-4803</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2013</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kV1rFTEQhoMoeDz6A7wLeKMXqZOP_chlaastFIRTvRNCNpldU_bjmGSh9debwwpSQeZiYHieYYaXkLcczjhA8zFxaCvJgEvWKNEyeEZ2vGokUy3I52QHIAQTquYvyauU7gGgagTfke8Hewyepsc5_8AUEl16elwj0stLeaC_cBlDRrqmMA-0s-PIpjCO6OldGCbLOE2IPtF19hhpyjYHR90y-5DDMqfX5EVvx4Rv_vQ9-fbp6uvFNbv98vnm4vyWOdW2mbWd1673reo5FxrA1i3v6h619HUnre4676SuwXotfAdtg43lzmvLLTqwvdyT99veY1x-rpiymUJyOI52xmVNhiupm0qCqgv67h_0flnjXK4zQlS6UXVd6D0526jBjmjC3C85WlfK4xTKf9iHMj-XSmmlBYcifHgiFCbjQx7smpK5uTs8ZfnGurikFLE3xxgmGx8NB3MK02xhmhKmOYVpTo7YnFTYecD49-z_S78BbNKgew</recordid><startdate>20130901</startdate><enddate>20130901</enddate><creator>Zheng, Fangyuan</creator><creator>Jing, Wenheng</creator><creator>Gu, Xuehong</creator><creator>Xu, Nanping</creator><creator>Dong, Junhang</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>ISR</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20130901</creationdate><title>Rapid synthesis of pure DD3R zeolite using ball-milled Sigma-1 seeds under static conditions</title><author>Zheng, Fangyuan ; Jing, Wenheng ; Gu, Xuehong ; Xu, Nanping ; Dong, Junhang</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c488t-8bd9cfd84f112900a681b6fe93d6b3a9bbdc3960ad92db087e7a1cd9a1aec0af3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2013</creationdate><topic>Ball milling</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Classical Mechanics</topic><topic>Crystallization</topic><topic>Crystallography and Scattering Methods</topic><topic>Crystals</topic><topic>Materials Science</topic><topic>Phases</topic><topic>Polymer Sciences</topic><topic>Reproducibility</topic><topic>Seeds</topic><topic>Silica</topic><topic>Solid Mechanics</topic><topic>Synthesis</topic><topic>Zeolites</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zheng, Fangyuan</creatorcontrib><creatorcontrib>Jing, Wenheng</creatorcontrib><creatorcontrib>Gu, Xuehong</creatorcontrib><creatorcontrib>Xu, Nanping</creatorcontrib><creatorcontrib>Dong, Junhang</creatorcontrib><collection>CrossRef</collection><collection>Gale In Context: Science</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zheng, Fangyuan</au><au>Jing, Wenheng</au><au>Gu, Xuehong</au><au>Xu, Nanping</au><au>Dong, Junhang</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Rapid synthesis of pure DD3R zeolite using ball-milled Sigma-1 seeds under static conditions</atitle><jtitle>Journal of materials science</jtitle><stitle>J Mater Sci</stitle><date>2013-09-01</date><risdate>2013</risdate><volume>48</volume><issue>18</issue><spage>6286</spage><epage>6292</epage><pages>6286-6292</pages><issn>0022-2461</issn><eissn>1573-4803</eissn><abstract>Deca-Dodecasil 3 Rhombohedral (DD3R) zeolite has great potential applications in the separation of gases with small molecular size; however, the extremely long crystallization time and the generated impure phases such as Sigma-Two (SGT) and Dodecasil 1H (DOH) have been the main obstacles for commercial utilization. In this work, ball-milled Sigma-1 was used as seeds for the first time to induce the crystallization of DD3R crystals. Pure DD3R zeolite was successfully produced under static conditions with drastically reduced crystallization time of ca. 9 h. The new synthesis approach showed 100 % of repeatability to obtain pure DD3R zeolite.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1007/s10853-013-7428-0</doi><tpages>7</tpages></addata></record> |
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| subjects | Ball milling Characterization and Evaluation of Materials Chemistry and Materials Science Classical Mechanics Crystallization Crystallography and Scattering Methods Crystals Materials Science Phases Polymer Sciences Reproducibility Seeds Silica Solid Mechanics Synthesis Zeolites |
| title | Rapid synthesis of pure DD3R zeolite using ball-milled Sigma-1 seeds under static conditions |
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