Two methods for spirothiohydantoin synthesis

Two methods for spirothiohydantoin synthesis

Two methods for spirothiohydantoin synthesis are presented. The title compounds were prepared with reaction of the corresponding 1-aminocycloalkanecarboxylic acids and thiourea. These compounds were also prepared by a hydrolysis of the relevant spirodithiohydantoins with barium hydroxide. The struct...

Ausführliche Beschreibung

Gespeichert in:
Bibliographische Detailangaben
Veröffentlicht in:Acta chimica Slovenica 2012-09, Vol.59 (3), p.680-685
Hauptverfasser: Stoyanov, Neyko, Marinov, Marin
Format: Artikel
Sprache:eng
Online-Zugang:Volltext
Tags: Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
container_end_page 685
container_issue 3
container_start_page 680
container_title Acta chimica Slovenica
container_volume 59
creator Stoyanov, Neyko
Marinov, Marin
description Two methods for spirothiohydantoin synthesis are presented. The title compounds were prepared with reaction of the corresponding 1-aminocycloalkanecarboxylic acids and thiourea. These compounds were also prepared by a hydrolysis of the relevant spirodithiohydantoins with barium hydroxide. The structures of the compounds obtained were verified by comparison of 1H, and 13C NMR, IR and MS spectral data.
format Article
fullrecord <record><control><sourceid>proquest_pubme</sourceid><recordid>TN_cdi_proquest_miscellaneous_1436563849</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1436563849</sourcerecordid><originalsourceid>FETCH-LOGICAL-p211t-3c4e672162e725e9c8c3b18a6be35de71017763beeb82b33b17aa869f45110cb3</originalsourceid><addsrcrecordid>eNo1j81KxDAURrNQnHH0FaRLFxZykzRJlzL4MzDgZlyXpL2lkbapvSnSt3fAcXUW3-GDc8W2IMHmXHCzYbdEX5yLQilzwzZCcQ1S6C17Ov3EbMDUxYayNs4ZTWGOqQuxWxs3phjGjNYxdUiB7th163rC-wt37PP15bR_z48fb4f98zGfBEDKZa1QGwFaoBEFlrWtpQfrtEdZNGiAgzFaekRvhZfnzThnddmqAoDXXu7Y49_vNMfvBSlVQ6Aa-96NGBeqQEldaGlVeVYfLuriB2yqaQ6Dm9fqv1D-AlCxSww</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1436563849</pqid></control><display><type>article</type><title>Two methods for spirothiohydantoin synthesis</title><source>DOAJ Directory of Open Access Journals</source><source>EZB-FREE-00999 freely available EZB journals</source><source>Free Full-Text Journals in Chemistry</source><creator>Stoyanov, Neyko ; Marinov, Marin</creator><creatorcontrib>Stoyanov, Neyko ; Marinov, Marin</creatorcontrib><description>Two methods for spirothiohydantoin synthesis are presented. The title compounds were prepared with reaction of the corresponding 1-aminocycloalkanecarboxylic acids and thiourea. These compounds were also prepared by a hydrolysis of the relevant spirodithiohydantoins with barium hydroxide. The structures of the compounds obtained were verified by comparison of 1H, and 13C NMR, IR and MS spectral data.</description><identifier>ISSN: 1318-0207</identifier><identifier>PMID: 24061326</identifier><language>eng</language><publisher>Slovenia</publisher><ispartof>Acta chimica Slovenica, 2012-09, Vol.59 (3), p.680-685</ispartof><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/24061326$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Stoyanov, Neyko</creatorcontrib><creatorcontrib>Marinov, Marin</creatorcontrib><title>Two methods for spirothiohydantoin synthesis</title><title>Acta chimica Slovenica</title><addtitle>Acta Chim Slov</addtitle><description>Two methods for spirothiohydantoin synthesis are presented. The title compounds were prepared with reaction of the corresponding 1-aminocycloalkanecarboxylic acids and thiourea. These compounds were also prepared by a hydrolysis of the relevant spirodithiohydantoins with barium hydroxide. The structures of the compounds obtained were verified by comparison of 1H, and 13C NMR, IR and MS spectral data.</description><issn>1318-0207</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNo1j81KxDAURrNQnHH0FaRLFxZykzRJlzL4MzDgZlyXpL2lkbapvSnSt3fAcXUW3-GDc8W2IMHmXHCzYbdEX5yLQilzwzZCcQ1S6C17Ov3EbMDUxYayNs4ZTWGOqQuxWxs3phjGjNYxdUiB7th163rC-wt37PP15bR_z48fb4f98zGfBEDKZa1QGwFaoBEFlrWtpQfrtEdZNGiAgzFaekRvhZfnzThnddmqAoDXXu7Y49_vNMfvBSlVQ6Aa-96NGBeqQEldaGlVeVYfLuriB2yqaQ6Dm9fqv1D-AlCxSww</recordid><startdate>201209</startdate><enddate>201209</enddate><creator>Stoyanov, Neyko</creator><creator>Marinov, Marin</creator><scope>NPM</scope><scope>7X8</scope></search><sort><creationdate>201209</creationdate><title>Two methods for spirothiohydantoin synthesis</title><author>Stoyanov, Neyko ; Marinov, Marin</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-p211t-3c4e672162e725e9c8c3b18a6be35de71017763beeb82b33b17aa869f45110cb3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><toplevel>online_resources</toplevel><creatorcontrib>Stoyanov, Neyko</creatorcontrib><creatorcontrib>Marinov, Marin</creatorcontrib><collection>PubMed</collection><collection>MEDLINE - Academic</collection><jtitle>Acta chimica Slovenica</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Stoyanov, Neyko</au><au>Marinov, Marin</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Two methods for spirothiohydantoin synthesis</atitle><jtitle>Acta chimica Slovenica</jtitle><addtitle>Acta Chim Slov</addtitle><date>2012-09</date><risdate>2012</risdate><volume>59</volume><issue>3</issue><spage>680</spage><epage>685</epage><pages>680-685</pages><issn>1318-0207</issn><abstract>Two methods for spirothiohydantoin synthesis are presented. The title compounds were prepared with reaction of the corresponding 1-aminocycloalkanecarboxylic acids and thiourea. These compounds were also prepared by a hydrolysis of the relevant spirodithiohydantoins with barium hydroxide. The structures of the compounds obtained were verified by comparison of 1H, and 13C NMR, IR and MS spectral data.</abstract><cop>Slovenia</cop><pmid>24061326</pmid><tpages>6</tpages></addata></record>
fulltext fulltext
identifier ISSN: 1318-0207
ispartof Acta chimica Slovenica, 2012-09, Vol.59 (3), p.680-685
issn 1318-0207
language eng
recordid cdi_proquest_miscellaneous_1436563849
source DOAJ Directory of Open Access Journals; EZB-FREE-00999 freely available EZB journals; Free Full-Text Journals in Chemistry
title Two methods for spirothiohydantoin synthesis
url https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-27T21%3A05%3A28IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_pubme&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Two%20methods%20for%20spirothiohydantoin%20synthesis&rft.jtitle=Acta%20chimica%20Slovenica&rft.au=Stoyanov,%20Neyko&rft.date=2012-09&rft.volume=59&rft.issue=3&rft.spage=680&rft.epage=685&rft.pages=680-685&rft.issn=1318-0207&rft_id=info:doi/&rft_dat=%3Cproquest_pubme%3E1436563849%3C/proquest_pubme%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1436563849&rft_id=info:pmid/24061326&rfr_iscdi=true