Flash heating in the diamond cell: melting curve of rhenium
A new method for measuring melting temperatures in the laser-heated diamond cell is described. This method circumvents previous problems associated with the sample instability, thermal runaway, and chemical reactions. Samples were heated with a single, 20 milliseconds rectangular pulse from a fiber...
Gespeichert in:
| Veröffentlicht in: | Rev. Sci. Instrum 2012-06, Vol.83 (6), p.063905-063905 |
|---|---|
| Hauptverfasser: | , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 063905 |
|---|---|
| container_issue | 6 |
| container_start_page | 063905 |
| container_title | Rev. Sci. Instrum |
| container_volume | 83 |
| creator | Yang, Liuxiang Karandikar, Amol Boehler, Reinhard |
| description | A new method for measuring melting temperatures in the laser-heated diamond cell is described. This method circumvents previous problems associated with the sample instability, thermal runaway, and chemical reactions. Samples were heated with a single, 20 milliseconds rectangular pulse from a fiber laser, monitoring their thermal response with a fast photomultiplier while measuring the steady state temperature with a CCD spectrometer. The samples were recovered and analyzed using scanning electron microscopy. Focused ion beam milling allowed to examine both the lateral and the vertical solid-liquid boundaries. Ambient pressure tests reproducibly yielded the known melting temperatures of rhenium and molybdenum. Melting of Re was measured to 50 GPa, a 5-fold extension of previous data. The refractory character of Re is drastically enhanced by pressure, in contrast to Mo. |
| doi_str_mv | 10.1063/1.4730595 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_osti_</sourceid><recordid>TN_cdi_proquest_miscellaneous_1429867042</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1023534259</sourcerecordid><originalsourceid>FETCH-LOGICAL-c411t-3e3f19f0b9cd42333a499ff342bdffc89f8461ee741b327079eaa21eb10e2b633</originalsourceid><addsrcrecordid>eNqF0D1PwzAQBmALgWj5GPgDyGKCIcVnO3YME0IUkCqxwBw5zpkY5QPiBIl_T0oLK15u8KO7Vy8hJ8AWwJS4hIXUgqUm3SFzYJlJtOJil8wZEzJRWmYzchDjG5teCrBPZpzrNFUS5uR6WdtY0QrtENpXGlo6VEjLYJuuLanDur6iDdY_n27sP5F2nvYVtmFsjsiet3XE4-08JC_Lu-fbh2T1dP94e7NKnAQYEoHCg_GsMK6UXAhhpTHeC8mL0nuXGZ9JBYhaQiG4ZtqgtRywAIa8UEIckrPN3i4OIY8uDOgq17UtuiGfClBGr9H5Br333ceIccibENf5bYvdGHOQ3GRKsynBv5RxkU7xUjPRiw11fRdjjz5_70Nj-68JrU-LHPJt95M93a4diwbLP_lbtvgGq_17SQ</addsrcrecordid><sourcetype>Open Access Repository</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1023534259</pqid></control><display><type>article</type><title>Flash heating in the diamond cell: melting curve of rhenium</title><source>AIP Journals Complete</source><source>AIP Digital Archive</source><source>Alma/SFX Local Collection</source><creator>Yang, Liuxiang ; Karandikar, Amol ; Boehler, Reinhard</creator><creatorcontrib>Yang, Liuxiang ; Karandikar, Amol ; Boehler, Reinhard ; Energy Frontier Research Centers (EFRC) ; Energy Frontier Research in Extreme Environments (EFree)</creatorcontrib><description>A new method for measuring melting temperatures in the laser-heated diamond cell is described. This method circumvents previous problems associated with the sample instability, thermal runaway, and chemical reactions. Samples were heated with a single, 20 milliseconds rectangular pulse from a fiber laser, monitoring their thermal response with a fast photomultiplier while measuring the steady state temperature with a CCD spectrometer. The samples were recovered and analyzed using scanning electron microscopy. Focused ion beam milling allowed to examine both the lateral and the vertical solid-liquid boundaries. Ambient pressure tests reproducibly yielded the known melting temperatures of rhenium and molybdenum. Melting of Re was measured to 50 GPa, a 5-fold extension of previous data. The refractory character of Re is drastically enhanced by pressure, in contrast to Mo.</description><identifier>ISSN: 0034-6748</identifier><identifier>EISSN: 1089-7623</identifier><identifier>DOI: 10.1063/1.4730595</identifier><identifier>PMID: 22755641</identifier><language>eng</language><publisher>United States</publisher><subject>catalysis (heterogeneous), solar (photovoltaic), phonons, thermoelectric, energy storage (including batteries and capacitors), hydrogen and fuel cells, superconductivity, charge transport, mesostructured materials, materials and chemistry by design, synthesis (novel materials) ; Charge coupled devices ; Diamonds ; Heating ; Instability ; Melting ; Molybdenum ; Rhenium ; Spectrometers</subject><ispartof>Rev. Sci. Instrum, 2012-06, Vol.83 (6), p.063905-063905</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c411t-3e3f19f0b9cd42333a499ff342bdffc89f8461ee741b327079eaa21eb10e2b633</citedby><cites>FETCH-LOGICAL-c411t-3e3f19f0b9cd42333a499ff342bdffc89f8461ee741b327079eaa21eb10e2b633</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,885,27924,27925</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/22755641$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink><backlink>$$Uhttps://www.osti.gov/biblio/1066973$$D View this record in Osti.gov$$Hfree_for_read</backlink></links><search><creatorcontrib>Yang, Liuxiang</creatorcontrib><creatorcontrib>Karandikar, Amol</creatorcontrib><creatorcontrib>Boehler, Reinhard</creatorcontrib><creatorcontrib>Energy Frontier Research Centers (EFRC)</creatorcontrib><creatorcontrib>Energy Frontier Research in Extreme Environments (EFree)</creatorcontrib><title>Flash heating in the diamond cell: melting curve of rhenium</title><title>Rev. Sci. Instrum</title><addtitle>Rev Sci Instrum</addtitle><description>A new method for measuring melting temperatures in the laser-heated diamond cell is described. This method circumvents previous problems associated with the sample instability, thermal runaway, and chemical reactions. Samples were heated with a single, 20 milliseconds rectangular pulse from a fiber laser, monitoring their thermal response with a fast photomultiplier while measuring the steady state temperature with a CCD spectrometer. The samples were recovered and analyzed using scanning electron microscopy. Focused ion beam milling allowed to examine both the lateral and the vertical solid-liquid boundaries. Ambient pressure tests reproducibly yielded the known melting temperatures of rhenium and molybdenum. Melting of Re was measured to 50 GPa, a 5-fold extension of previous data. The refractory character of Re is drastically enhanced by pressure, in contrast to Mo.</description><subject>catalysis (heterogeneous), solar (photovoltaic), phonons, thermoelectric, energy storage (including batteries and capacitors), hydrogen and fuel cells, superconductivity, charge transport, mesostructured materials, materials and chemistry by design, synthesis (novel materials)</subject><subject>Charge coupled devices</subject><subject>Diamonds</subject><subject>Heating</subject><subject>Instability</subject><subject>Melting</subject><subject>Molybdenum</subject><subject>Rhenium</subject><subject>Spectrometers</subject><issn>0034-6748</issn><issn>1089-7623</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqF0D1PwzAQBmALgWj5GPgDyGKCIcVnO3YME0IUkCqxwBw5zpkY5QPiBIl_T0oLK15u8KO7Vy8hJ8AWwJS4hIXUgqUm3SFzYJlJtOJil8wZEzJRWmYzchDjG5teCrBPZpzrNFUS5uR6WdtY0QrtENpXGlo6VEjLYJuuLanDur6iDdY_n27sP5F2nvYVtmFsjsiet3XE4-08JC_Lu-fbh2T1dP94e7NKnAQYEoHCg_GsMK6UXAhhpTHeC8mL0nuXGZ9JBYhaQiG4ZtqgtRywAIa8UEIckrPN3i4OIY8uDOgq17UtuiGfClBGr9H5Br333ceIccibENf5bYvdGHOQ3GRKsynBv5RxkU7xUjPRiw11fRdjjz5_70Nj-68JrU-LHPJt95M93a4diwbLP_lbtvgGq_17SQ</recordid><startdate>20120601</startdate><enddate>20120601</enddate><creator>Yang, Liuxiang</creator><creator>Karandikar, Amol</creator><creator>Boehler, Reinhard</creator><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope><scope>7U5</scope><scope>8FD</scope><scope>L7M</scope><scope>OTOTI</scope></search><sort><creationdate>20120601</creationdate><title>Flash heating in the diamond cell: melting curve of rhenium</title><author>Yang, Liuxiang ; Karandikar, Amol ; Boehler, Reinhard</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c411t-3e3f19f0b9cd42333a499ff342bdffc89f8461ee741b327079eaa21eb10e2b633</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>catalysis (heterogeneous), solar (photovoltaic), phonons, thermoelectric, energy storage (including batteries and capacitors), hydrogen and fuel cells, superconductivity, charge transport, mesostructured materials, materials and chemistry by design, synthesis (novel materials)</topic><topic>Charge coupled devices</topic><topic>Diamonds</topic><topic>Heating</topic><topic>Instability</topic><topic>Melting</topic><topic>Molybdenum</topic><topic>Rhenium</topic><topic>Spectrometers</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Yang, Liuxiang</creatorcontrib><creatorcontrib>Karandikar, Amol</creatorcontrib><creatorcontrib>Boehler, Reinhard</creatorcontrib><creatorcontrib>Energy Frontier Research Centers (EFRC)</creatorcontrib><creatorcontrib>Energy Frontier Research in Extreme Environments (EFree)</creatorcontrib><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>Technology Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>OSTI.GOV</collection><jtitle>Rev. Sci. Instrum</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Yang, Liuxiang</au><au>Karandikar, Amol</au><au>Boehler, Reinhard</au><aucorp>Energy Frontier Research Centers (EFRC)</aucorp><aucorp>Energy Frontier Research in Extreme Environments (EFree)</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Flash heating in the diamond cell: melting curve of rhenium</atitle><jtitle>Rev. Sci. Instrum</jtitle><addtitle>Rev Sci Instrum</addtitle><date>2012-06-01</date><risdate>2012</risdate><volume>83</volume><issue>6</issue><spage>063905</spage><epage>063905</epage><pages>063905-063905</pages><issn>0034-6748</issn><eissn>1089-7623</eissn><abstract>A new method for measuring melting temperatures in the laser-heated diamond cell is described. This method circumvents previous problems associated with the sample instability, thermal runaway, and chemical reactions. Samples were heated with a single, 20 milliseconds rectangular pulse from a fiber laser, monitoring their thermal response with a fast photomultiplier while measuring the steady state temperature with a CCD spectrometer. The samples were recovered and analyzed using scanning electron microscopy. Focused ion beam milling allowed to examine both the lateral and the vertical solid-liquid boundaries. Ambient pressure tests reproducibly yielded the known melting temperatures of rhenium and molybdenum. Melting of Re was measured to 50 GPa, a 5-fold extension of previous data. The refractory character of Re is drastically enhanced by pressure, in contrast to Mo.</abstract><cop>United States</cop><pmid>22755641</pmid><doi>10.1063/1.4730595</doi><tpages>1</tpages></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0034-6748 |
| ispartof | Rev. Sci. Instrum, 2012-06, Vol.83 (6), p.063905-063905 |
| issn | 0034-6748 1089-7623 |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1429867042 |
| source | AIP Journals Complete; AIP Digital Archive; Alma/SFX Local Collection |
| subjects | catalysis (heterogeneous), solar (photovoltaic), phonons, thermoelectric, energy storage (including batteries and capacitors), hydrogen and fuel cells, superconductivity, charge transport, mesostructured materials, materials and chemistry by design, synthesis (novel materials) Charge coupled devices Diamonds Heating Instability Melting Molybdenum Rhenium Spectrometers |
| title | Flash heating in the diamond cell: melting curve of rhenium |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-02T11%3A22%3A08IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_osti_&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Flash%20heating%20in%20the%20diamond%20cell:%20melting%20curve%20of%20rhenium&rft.jtitle=Rev.%20Sci.%20Instrum&rft.au=Yang,%20Liuxiang&rft.aucorp=Energy%20Frontier%20Research%20Centers%20(EFRC)&rft.date=2012-06-01&rft.volume=83&rft.issue=6&rft.spage=063905&rft.epage=063905&rft.pages=063905-063905&rft.issn=0034-6748&rft.eissn=1089-7623&rft_id=info:doi/10.1063/1.4730595&rft_dat=%3Cproquest_osti_%3E1023534259%3C/proquest_osti_%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1023534259&rft_id=info:pmid/22755641&rfr_iscdi=true |