Identification of organic compounds in a mutagenic extract of a surface drinking water by a computerized gas chromatography/mass spectrometry system (GC/MS/COM)
The diethyl ether extract of the reverse osmosis concentrate of drinking water which was found to be mutagenic, was analysed. To obtain clearly resolved peaks on a gas chromatogram of individual organic compounds, present in trace amounts, the extract was partitioned into acid, methylated acid and b...
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| Veröffentlicht in: | Environ. Sci. Technol.; (United States) 1980-05, Vol.14 (5), p.576-588 |
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| container_title | Environ. Sci. Technol.; (United States) |
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| creator | Coleman, W. Emile Melton, Robert G Kopfler, Frederick C Barone, Karen A Aurand, Theresa A Jellison, Mark G |
| description | The diethyl ether extract of the reverse osmosis concentrate of drinking water which was found to be mutagenic, was analysed. To obtain clearly resolved peaks on a gas chromatogram of individual organic compounds, present in trace amounts, the extract was partitioned into acid, methylated acid and base/neutral fractions and the latter fraction was further partitioned on a silica gel microcolumn by elution with solvents of different polarities. The fractions were analysed on a computerized GC/MS system, equipped with glass capillary columns. Some 460 organic compounds were identified, including 41 polynuclear aromatic compounds and 15 PCB. |
| doi_str_mv | 10.1021/es60165a012 |
| format | Article |
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Emile</creatorcontrib><creatorcontrib>Melton, Robert G</creatorcontrib><creatorcontrib>Kopfler, Frederick C</creatorcontrib><creatorcontrib>Barone, Karen A</creatorcontrib><creatorcontrib>Aurand, Theresa A</creatorcontrib><creatorcontrib>Jellison, Mark G</creatorcontrib><creatorcontrib>EPA</creatorcontrib><collection>AGRIS</collection><collection>Istex</collection><collection>CrossRef</collection><collection>Aqualine</collection><collection>Environment Abstracts</collection><collection>Environmental Sciences and Pollution Management</collection><collection>Environment Abstracts</collection><collection>OSTI.GOV</collection><jtitle>Environ. Sci. Technol.; (United States)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Coleman, W. Emile</au><au>Melton, Robert G</au><au>Kopfler, Frederick C</au><au>Barone, Karen A</au><au>Aurand, Theresa A</au><au>Jellison, Mark G</au><aucorp>EPA</aucorp><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Identification of organic compounds in a mutagenic extract of a surface drinking water by a computerized gas chromatography/mass spectrometry system (GC/MS/COM)</atitle><jtitle>Environ. Sci. Technol.; (United States)</jtitle><addtitle>Environ. Sci. Technol</addtitle><date>1980-05-01</date><risdate>1980</risdate><volume>14</volume><issue>5</issue><spage>576</spage><epage>588</epage><pages>576-588</pages><issn>0013-936X</issn><eissn>1520-5851</eissn><abstract>The diethyl ether extract of the reverse osmosis concentrate of drinking water which was found to be mutagenic, was analysed. To obtain clearly resolved peaks on a gas chromatogram of individual organic compounds, present in trace amounts, the extract was partitioned into acid, methylated acid and base/neutral fractions and the latter fraction was further partitioned on a silica gel microcolumn by elution with solvents of different polarities. The fractions were analysed on a computerized GC/MS system, equipped with glass capillary columns. Some 460 organic compounds were identified, including 41 polynuclear aromatic compounds and 15 PCB.</abstract><cop>United States</cop><pub>American Chemical Society</pub><doi>10.1021/es60165a012</doi><tpages>13</tpages></addata></record> |
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| ispartof | Environ. Sci. Technol.; (United States), 1980-05, Vol.14 (5), p.576-588 |
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| source | ACS Publications |
| subjects | AMIDES AMINES AROMATICS CHROMATOGRAPHY DRINKING WATER ENVIRONMENTAL SCIENCES GAS CHROMATOGRAPHY HYDROCARBONS HYDROGEN COMPOUNDS MUTAGENS ORGANIC CHLORINE COMPOUNDS ORGANIC COMPOUNDS ORGANIC HALOGEN COMPOUNDS ORGANIC NITROGEN COMPOUNDS OXYGEN COMPOUNDS POLYCYCLIC AROMATIC HYDROCARBONS SEPARATION PROCESSES WATER 520200 -- Environment, Aquatic-- Chemicals Monitoring & Transport-- (-1989) |
| title | Identification of organic compounds in a mutagenic extract of a surface drinking water by a computerized gas chromatography/mass spectrometry system (GC/MS/COM) |
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