TILT-A-WHIRL: a texture analysis package for 3D rendering of pole figures using Matlab

A new Matlab-based software suite called Tilt-A-Whirl has been applied to XRD data from textured gold films electro-deposited onto nickel substrates. The software routines facilitate phase identification, texture analysis via pole figure visualization, and macrostrain determination. The use of princ...

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Veröffentlicht in:Powder diffraction 2013-06, Vol.28 (2), p.81-89
Hauptverfasser: Rodriguez, Mark A., Pearl, Megan R., Van Benthem, Mark H., Griego, James J. M., Pillars, Jamin R.
Format: Artikel
Sprache:eng
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Zusammenfassung:A new Matlab-based software suite called Tilt-A-Whirl has been applied to XRD data from textured gold films electro-deposited onto nickel substrates. The software routines facilitate phase identification, texture analysis via pole figure visualization, and macrostrain determination. The use of principal component analysis with multivariate curve resolution (PCA/MCR) revealed the extraction of texture components. The unusual hardness properties of one Au film (deposited from a 30% gold depleted BDT-200 bath) were found to be dependent on the (210) out-of-plane preferred orientation of the polycrystalline gold film. The progressive nucleation of Au crystallites during electro-plating has been tied to improved hardness properties of this film.
ISSN:0885-7156
1945-7413
DOI:10.1017/S0885715613000262