Determination of organotin compounds in marine mussel samples by using high-performance liquid chromatography-hydride generation inductively coupled plasma atomic emission spectrometry

Organotin compounds were determined in marine mussel samples using high-performance liquid chromatography (HPLC) and inductively-coupled plasma atomic emission spectrometry (ICP-AES), with a hydride generation gas-liquid separator inserted between the HPLC column and the ICP-AES detector. A detectio...

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Veröffentlicht in:Analyst (London) 1995, Vol.120 (7), p.1937-1939
Hauptverfasser: RIVARO, P, ZARATIN, L, FRACHE, R, MAZZUCOTTELLI, A
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container_end_page 1939
container_issue 7
container_start_page 1937
container_title Analyst (London)
container_volume 120
creator RIVARO, P
ZARATIN, L
FRACHE, R
MAZZUCOTTELLI, A
description Organotin compounds were determined in marine mussel samples using high-performance liquid chromatography (HPLC) and inductively-coupled plasma atomic emission spectrometry (ICP-AES), with a hydride generation gas-liquid separator inserted between the HPLC column and the ICP-AES detector. A detection limit of 7 ng was obtained for tin. The organotin species were completely separated within 7 minutes. Organometallic compounds were accurately determined in the marine mussel samples. The hydride generator allowed an increase in the sensitivity of the method and used organic solvents in high proportions without extinguishing the plasma torch.
doi_str_mv 10.1039/an9952001937
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source Royal Society of Chemistry Journals Archive (1841-2007); Royal Society Of Chemistry Journals 2008-; Alma/SFX Local Collection
subjects Animal, plant and microbial ecology
Biological and medical sciences
Fundamental and applied biological sciences. Psychology
General aspects. Techniques
Methods and techniques (sampling, tagging, trapping, modelling...)
title Determination of organotin compounds in marine mussel samples by using high-performance liquid chromatography-hydride generation inductively coupled plasma atomic emission spectrometry
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