Hollow-fiber liquid-phase microextraction and gas chromatography-mass spectrometry of barbiturates in whole blood samples

Here, we present a method for measuring barbiturates (butalbital, secobarbital, pentobarbital, and phenobarbital) in whole blood samples. To accomplish these measurements, analytes were extracted by means of hollow‐fiber liquid‐phase microextraction in the three‐phase mode. Hollow‐fiber pores were f...

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Veröffentlicht in:	Journal of separation science 2012-12, Vol.35 (23), p.3361-3368
Hauptverfasser:	Menck, Rafael Almeida, de Lima, Diógenes Saulo, Seulin, Saskia Carolina, Leyton, Vilma, Pasqualucci, Carlos Augusto, Muñoz, Daniel Romero, Osselton, Michael David, Yonamine, Mauricio
Format:	Artikel
Sprache:	eng
Schlagworte:	Analysis Analytical chemistry Barbiturates Barbiturates - blood Barbiturates - chemistry Biological and medical sciences Blood Chromatography Decanol Extraction Fibers Gas chromatography Gas Chromatography-Mass Spectrometry - methods GC-MS General pharmacology Humans Injectors Liquid Phase Microextraction - instrumentation Liquid Phase Microextraction - methods Liquid-phase microextraction Mass spectrometry Medical sciences Methylation Molecular Structure Pharmacology Pharmacology. Drug treatments Whole blood
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