Structure and mechanical performance of in situ synthesized hydroxyapatite/polyetheretherketone nanocomposite materials
Nano-hydroxyapatite (HA) particles were prepared by a sol–gel method and polyetheretherketone (PEEK) composite materials containing a various amount of lab-prepared HA fillers had been successfully synthesized via an in situ synthesis process. The materials structure was characterized by infrared sp...
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| Veröffentlicht in: | Journal of sol-gel science and technology 2012-04, Vol.62 (1), p.52-56 |
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| creator | Ma, Rui Weng, Luqian Fang, Lin Luo, Zhongkuan Song, Shenhua |
| description | Nano-hydroxyapatite (HA) particles were prepared by a sol–gel method and polyetheretherketone (PEEK) composite materials containing a various amount of lab-prepared HA fillers had been successfully synthesized via an in situ synthesis process. The materials structure was characterized by infrared spectroscopy, transmission electron microscopy, scanning electron microscopy, and energy dispersive X-ray spectroscopy and the mechanical performance was investigated by a tensile strength test. The tensile strength of HA/PEEK composites reaches an optimal 108 MPa at 6.1% HA content. The composites with HA content below 17.4% exhibit a plastic break mode, while a brittle break mode above 17.4%. The results exhibit that the strong bonding between hydroxyapatite fillers and PEEK matrix has been achieved. And it was proved that this strong bonding may be mainly attributed to the physical factors, such as mechanical interlock between PEEK molecules and HA surface. The study clearly demonstrates that in situ synthesized HA/PEEK composite materials have the potential for use as an alternative material for hard tissue replacement. |
| doi_str_mv | 10.1007/s10971-012-2682-1 |
| format | Article |
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The materials structure was characterized by infrared spectroscopy, transmission electron microscopy, scanning electron microscopy, and energy dispersive X-ray spectroscopy and the mechanical performance was investigated by a tensile strength test. The tensile strength of HA/PEEK composites reaches an optimal 108 MPa at 6.1% HA content. The composites with HA content below 17.4% exhibit a plastic break mode, while a brittle break mode above 17.4%. The results exhibit that the strong bonding between hydroxyapatite fillers and PEEK matrix has been achieved. And it was proved that this strong bonding may be mainly attributed to the physical factors, such as mechanical interlock between PEEK molecules and HA surface. The study clearly demonstrates that in situ synthesized HA/PEEK composite materials have the potential for use as an alternative material for hard tissue replacement.</description><identifier>ISSN: 0928-0707</identifier><identifier>EISSN: 1573-4846</identifier><identifier>DOI: 10.1007/s10971-012-2682-1</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Bonding strength ; Breaking ; Ceramics ; Chemistry ; Chemistry and Materials Science ; Colloidal gels. Colloidal sols ; Colloidal state and disperse state ; Composite materials ; Composites ; Energy dispersive X ray spectroscopy ; Energy transmission ; Exact sciences and technology ; Fillers ; General and physical chemistry ; Glass ; Hydroxyapatite ; Inorganic Chemistry ; Materials Science ; Mechanical properties ; Microscopy ; Nanocomposites ; Nanostructure ; Nanotechnology ; Natural Materials ; Optical and Electronic Materials ; Original Paper ; Particulate composites ; Physical factors ; Polyether ether ketones ; Polyetheretherketones ; Polymer matrix composites ; Scanning electron microscopy ; Sol-gel processes ; Spectrum analysis ; Tensile strength ; Transmission electron microscopy</subject><ispartof>Journal of sol-gel science and technology, 2012-04, Vol.62 (1), p.52-56</ispartof><rights>Springer Science+Business Media, LLC 2012</rights><rights>2015 INIST-CNRS</rights><rights>Journal of Sol-Gel Science and Technology is a copyright of Springer, (2012). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c412t-9d22426029940b765b3740fd263243da9ca1ce01e6a574528d678912346dd8083</citedby><cites>FETCH-LOGICAL-c412t-9d22426029940b765b3740fd263243da9ca1ce01e6a574528d678912346dd8083</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10971-012-2682-1$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10971-012-2682-1$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27923,27924,41487,42556,51318</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=25604001$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Ma, Rui</creatorcontrib><creatorcontrib>Weng, Luqian</creatorcontrib><creatorcontrib>Fang, Lin</creatorcontrib><creatorcontrib>Luo, Zhongkuan</creatorcontrib><creatorcontrib>Song, Shenhua</creatorcontrib><title>Structure and mechanical performance of in situ synthesized hydroxyapatite/polyetheretherketone nanocomposite materials</title><title>Journal of sol-gel science and technology</title><addtitle>J Sol-Gel Sci Technol</addtitle><description>Nano-hydroxyapatite (HA) particles were prepared by a sol–gel method and polyetheretherketone (PEEK) composite materials containing a various amount of lab-prepared HA fillers had been successfully synthesized via an in situ synthesis process. The materials structure was characterized by infrared spectroscopy, transmission electron microscopy, scanning electron microscopy, and energy dispersive X-ray spectroscopy and the mechanical performance was investigated by a tensile strength test. The tensile strength of HA/PEEK composites reaches an optimal 108 MPa at 6.1% HA content. The composites with HA content below 17.4% exhibit a plastic break mode, while a brittle break mode above 17.4%. The results exhibit that the strong bonding between hydroxyapatite fillers and PEEK matrix has been achieved. And it was proved that this strong bonding may be mainly attributed to the physical factors, such as mechanical interlock between PEEK molecules and HA surface. The study clearly demonstrates that in situ synthesized HA/PEEK composite materials have the potential for use as an alternative material for hard tissue replacement.</description><subject>Bonding strength</subject><subject>Breaking</subject><subject>Ceramics</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Colloidal gels. Colloidal sols</subject><subject>Colloidal state and disperse state</subject><subject>Composite materials</subject><subject>Composites</subject><subject>Energy dispersive X ray spectroscopy</subject><subject>Energy transmission</subject><subject>Exact sciences and technology</subject><subject>Fillers</subject><subject>General and physical chemistry</subject><subject>Glass</subject><subject>Hydroxyapatite</subject><subject>Inorganic Chemistry</subject><subject>Materials Science</subject><subject>Mechanical properties</subject><subject>Microscopy</subject><subject>Nanocomposites</subject><subject>Nanostructure</subject><subject>Nanotechnology</subject><subject>Natural Materials</subject><subject>Optical and Electronic Materials</subject><subject>Original Paper</subject><subject>Particulate composites</subject><subject>Physical factors</subject><subject>Polyether ether ketones</subject><subject>Polyetheretherketones</subject><subject>Polymer matrix composites</subject><subject>Scanning electron microscopy</subject><subject>Sol-gel processes</subject><subject>Spectrum analysis</subject><subject>Tensile strength</subject><subject>Transmission electron microscopy</subject><issn>0928-0707</issn><issn>1573-4846</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNqFkU1rFTEUhgdR8Nr2B3QXEMHNtCdn8jVLKVYLBRfW9ZBmzninziRjkkHHX2-utygI4iZncZ73JclTVeccLjiAvkwcWs1r4FijMljzJ9WOS93Uwgj1tNpBi6YGDfp59SKlBwCQgutd9e1jjqvLayRmfc9mcnvrR2cntlAcQpytd8TCwEbP0phXljaf95TGH9Sz_dbH8H2zi81jpsslTBuVZfx1fKEcPDFvfXBhXkJJE5ttpjjaKZ1Wz4Yy6OxxnlSfrt_eXb2vbz-8u7l6c1s7wTHXbY8oUAG2rYB7reR9owUMPaoGRdPb1lnuCDgpK7WQaHqlTcuxEarvDZjmpHp97F1i-LpSyt08JkfTZD2FNXUckRsjNTb_R8EUWCghCvryL_QhrNGXh3SIspWN1CALxY-UiyGlSEO3xHG2cStV3cFad7TWFWvdwVrHS-bVY7NNxcIQy_-P6XcQpQIBcODwyKWy8p8p_rnBv8t_Ano5p_o</recordid><startdate>20120401</startdate><enddate>20120401</enddate><creator>Ma, Rui</creator><creator>Weng, Luqian</creator><creator>Fang, Lin</creator><creator>Luo, Zhongkuan</creator><creator>Song, Shenhua</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>PTHSS</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20120401</creationdate><title>Structure and mechanical performance of in situ synthesized hydroxyapatite/polyetheretherketone nanocomposite materials</title><author>Ma, Rui ; Weng, Luqian ; Fang, Lin ; Luo, Zhongkuan ; Song, Shenhua</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c412t-9d22426029940b765b3740fd263243da9ca1ce01e6a574528d678912346dd8083</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Bonding strength</topic><topic>Breaking</topic><topic>Ceramics</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Colloidal gels. Colloidal sols</topic><topic>Colloidal state and disperse state</topic><topic>Composite materials</topic><topic>Composites</topic><topic>Energy dispersive X ray spectroscopy</topic><topic>Energy transmission</topic><topic>Exact sciences and technology</topic><topic>Fillers</topic><topic>General and physical chemistry</topic><topic>Glass</topic><topic>Hydroxyapatite</topic><topic>Inorganic Chemistry</topic><topic>Materials Science</topic><topic>Mechanical properties</topic><topic>Microscopy</topic><topic>Nanocomposites</topic><topic>Nanostructure</topic><topic>Nanotechnology</topic><topic>Natural Materials</topic><topic>Optical and Electronic Materials</topic><topic>Original Paper</topic><topic>Particulate composites</topic><topic>Physical factors</topic><topic>Polyether ether ketones</topic><topic>Polyetheretherketones</topic><topic>Polymer matrix composites</topic><topic>Scanning electron microscopy</topic><topic>Sol-gel processes</topic><topic>Spectrum analysis</topic><topic>Tensile strength</topic><topic>Transmission electron microscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ma, Rui</creatorcontrib><creatorcontrib>Weng, Luqian</creatorcontrib><creatorcontrib>Fang, Lin</creatorcontrib><creatorcontrib>Luo, Zhongkuan</creatorcontrib><creatorcontrib>Song, Shenhua</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>Engineering Collection</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of sol-gel science and technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ma, Rui</au><au>Weng, Luqian</au><au>Fang, Lin</au><au>Luo, Zhongkuan</au><au>Song, Shenhua</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Structure and mechanical performance of in situ synthesized hydroxyapatite/polyetheretherketone nanocomposite materials</atitle><jtitle>Journal of sol-gel science and technology</jtitle><stitle>J Sol-Gel Sci Technol</stitle><date>2012-04-01</date><risdate>2012</risdate><volume>62</volume><issue>1</issue><spage>52</spage><epage>56</epage><pages>52-56</pages><issn>0928-0707</issn><eissn>1573-4846</eissn><abstract>Nano-hydroxyapatite (HA) particles were prepared by a sol–gel method and polyetheretherketone (PEEK) composite materials containing a various amount of lab-prepared HA fillers had been successfully synthesized via an in situ synthesis process. The materials structure was characterized by infrared spectroscopy, transmission electron microscopy, scanning electron microscopy, and energy dispersive X-ray spectroscopy and the mechanical performance was investigated by a tensile strength test. The tensile strength of HA/PEEK composites reaches an optimal 108 MPa at 6.1% HA content. The composites with HA content below 17.4% exhibit a plastic break mode, while a brittle break mode above 17.4%. The results exhibit that the strong bonding between hydroxyapatite fillers and PEEK matrix has been achieved. And it was proved that this strong bonding may be mainly attributed to the physical factors, such as mechanical interlock between PEEK molecules and HA surface. The study clearly demonstrates that in situ synthesized HA/PEEK composite materials have the potential for use as an alternative material for hard tissue replacement.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1007/s10971-012-2682-1</doi><tpages>5</tpages></addata></record> |
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| subjects | Bonding strength Breaking Ceramics Chemistry Chemistry and Materials Science Colloidal gels. Colloidal sols Colloidal state and disperse state Composite materials Composites Energy dispersive X ray spectroscopy Energy transmission Exact sciences and technology Fillers General and physical chemistry Glass Hydroxyapatite Inorganic Chemistry Materials Science Mechanical properties Microscopy Nanocomposites Nanostructure Nanotechnology Natural Materials Optical and Electronic Materials Original Paper Particulate composites Physical factors Polyether ether ketones Polyetheretherketones Polymer matrix composites Scanning electron microscopy Sol-gel processes Spectrum analysis Tensile strength Transmission electron microscopy |
| title | Structure and mechanical performance of in situ synthesized hydroxyapatite/polyetheretherketone nanocomposite materials |
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