Preparation and characterization of TiO2 hybrid sol for UV-curable high-refractive-index organic–inorganic hybrid thin films
In this study, UV-curable hybrid thin films were successfully prepared from TiO 2 and TiO 2 hybrid sols containing the acrylic monomer DPHA on PMMA substrates. The prepared TiO 2 and TiO 2 hybrid sols showed long-term storage stability and can provide operating control for the preparation of high-re...
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| Veröffentlicht in: | Journal of sol-gel science and technology 2010-08, Vol.55 (2), p.199-206 |
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| container_title | Journal of sol-gel science and technology |
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| creator | Chang, Chao-Ching Cheng, Liao-Ping Huang, Feng-Hsi Lin, Chia-Ying Hsieh, Chi-Fa Wang, Wei-Hong |
| description | In this study, UV-curable hybrid thin films were successfully prepared from TiO
2
and TiO
2
hybrid sols containing the acrylic monomer DPHA on PMMA substrates. The prepared TiO
2
and TiO
2
hybrid sols showed long-term storage stability and can provide operating control for the preparation of high-refractive-index hybrid thin films. The existence of interaction between the TiO
2
particle and the coupling agent was evidenced by FT-IR and UV–visible spectra. All hybrid thin films showed good adhesion to the PMMA substrate with refractive index falling over the range 1.64–1.77. These results suggested the potential application of present TiO
2
hybrid films in optical devices, such as anti-reflective coatings. |
| doi_str_mv | 10.1007/s10971-010-2233-6 |
| format | Article |
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2
and TiO
2
hybrid sols containing the acrylic monomer DPHA on PMMA substrates. The prepared TiO
2
and TiO
2
hybrid sols showed long-term storage stability and can provide operating control for the preparation of high-refractive-index hybrid thin films. The existence of interaction between the TiO
2
particle and the coupling agent was evidenced by FT-IR and UV–visible spectra. All hybrid thin films showed good adhesion to the PMMA substrate with refractive index falling over the range 1.64–1.77. These results suggested the potential application of present TiO
2
hybrid films in optical devices, such as anti-reflective coatings.</description><identifier>ISSN: 0928-0707</identifier><identifier>EISSN: 1573-4846</identifier><identifier>DOI: 10.1007/s10971-010-2233-6</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Adhesion ; Antireflection coatings ; Ceramics ; Chemistry ; Chemistry and Materials Science ; Colloidal gels. Colloidal sols ; Colloidal state and disperse state ; Composites ; Control stability ; Coupling agents ; Exact sciences and technology ; Falling ; General and physical chemistry ; Glass ; Inorganic Chemistry ; Materials Science ; Monomers ; Nanotechnology ; Natural Materials ; Optical and Electronic Materials ; Original Paper ; Polymethyl methacrylate ; Polymethyl methacrylates ; Refractivity ; Spectra ; Storage stability ; Substrates ; Thin films ; Titanium dioxide ; Ultraviolet radiation</subject><ispartof>Journal of sol-gel science and technology, 2010-08, Vol.55 (2), p.199-206</ispartof><rights>Springer Science+Business Media, LLC 2010</rights><rights>2015 INIST-CNRS</rights><rights>Journal of Sol-Gel Science and Technology is a copyright of Springer, (2010). All Rights Reserved.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c445t-9afc5fc8c76395b8ee1eb13e1cd0c7bed1043ccabac173fdd5ab8bee5162800b3</citedby><cites>FETCH-LOGICAL-c445t-9afc5fc8c76395b8ee1eb13e1cd0c7bed1043ccabac173fdd5ab8bee5162800b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10971-010-2233-6$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10971-010-2233-6$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=23089024$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Chang, Chao-Ching</creatorcontrib><creatorcontrib>Cheng, Liao-Ping</creatorcontrib><creatorcontrib>Huang, Feng-Hsi</creatorcontrib><creatorcontrib>Lin, Chia-Ying</creatorcontrib><creatorcontrib>Hsieh, Chi-Fa</creatorcontrib><creatorcontrib>Wang, Wei-Hong</creatorcontrib><title>Preparation and characterization of TiO2 hybrid sol for UV-curable high-refractive-index organic–inorganic hybrid thin films</title><title>Journal of sol-gel science and technology</title><addtitle>J Sol-Gel Sci Technol</addtitle><description>In this study, UV-curable hybrid thin films were successfully prepared from TiO
2
and TiO
2
hybrid sols containing the acrylic monomer DPHA on PMMA substrates. The prepared TiO
2
and TiO
2
hybrid sols showed long-term storage stability and can provide operating control for the preparation of high-refractive-index hybrid thin films. The existence of interaction between the TiO
2
particle and the coupling agent was evidenced by FT-IR and UV–visible spectra. All hybrid thin films showed good adhesion to the PMMA substrate with refractive index falling over the range 1.64–1.77. These results suggested the potential application of present TiO
2
hybrid films in optical devices, such as anti-reflective coatings.</description><subject>Adhesion</subject><subject>Antireflection coatings</subject><subject>Ceramics</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Colloidal gels. Colloidal sols</subject><subject>Colloidal state and disperse state</subject><subject>Composites</subject><subject>Control stability</subject><subject>Coupling agents</subject><subject>Exact sciences and technology</subject><subject>Falling</subject><subject>General and physical chemistry</subject><subject>Glass</subject><subject>Inorganic Chemistry</subject><subject>Materials Science</subject><subject>Monomers</subject><subject>Nanotechnology</subject><subject>Natural Materials</subject><subject>Optical and Electronic Materials</subject><subject>Original Paper</subject><subject>Polymethyl methacrylate</subject><subject>Polymethyl methacrylates</subject><subject>Refractivity</subject><subject>Spectra</subject><subject>Storage stability</subject><subject>Substrates</subject><subject>Thin films</subject><subject>Titanium dioxide</subject><subject>Ultraviolet radiation</subject><issn>0928-0707</issn><issn>1573-4846</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2010</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNp1kc-KFDEQxoMoOK4-gLeACF6iVUmn032UxX-wsB52vYYknZ7O0pOMSY_sehDfwTf0SczQo4LgKUnl931U1UfIU4SXCKBeFYReIQMExrkQrL1HNiiVYE3XtPfJBnreMVCgHpJHpdwAgGxQbci3j9nvTTZLSJGaOFA31ZdbfA5f12Ia6VW45HS6szkMtKSZjinT60_MHbKxs6dT2E4s-_GoC188C3HwtzTlrYnB_fz-I8TT_bfHMoVIxzDvymPyYDRz8U9O5xm5fvvm6vw9u7h89-H89QVzTSMX1pvRydF1TrWil7bzHr1F4dEN4JT1A0IjnDPWOFRiHAZpbGe9l9jyDsCKM_Ji9d3n9Pngy6J3oTg_zyb6dCgaUbRCKhCyos_-QW_SIcfaneZc9lJIFH2lcKVcTqXU4fU-h53JdxpBHxPRayK6JqKPiei2ap6fnE1xZq77ii6UP0IuoOuBN5XjK1fqV9z6_LeD_5v_Aqs7nnU</recordid><startdate>20100801</startdate><enddate>20100801</enddate><creator>Chang, Chao-Ching</creator><creator>Cheng, Liao-Ping</creator><creator>Huang, Feng-Hsi</creator><creator>Lin, Chia-Ying</creator><creator>Hsieh, Chi-Fa</creator><creator>Wang, Wei-Hong</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M7S</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20100801</creationdate><title>Preparation and characterization of TiO2 hybrid sol for UV-curable high-refractive-index organic–inorganic hybrid thin films</title><author>Chang, Chao-Ching ; Cheng, Liao-Ping ; Huang, Feng-Hsi ; Lin, Chia-Ying ; Hsieh, Chi-Fa ; Wang, Wei-Hong</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c445t-9afc5fc8c76395b8ee1eb13e1cd0c7bed1043ccabac173fdd5ab8bee5162800b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2010</creationdate><topic>Adhesion</topic><topic>Antireflection coatings</topic><topic>Ceramics</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Colloidal gels. Colloidal sols</topic><topic>Colloidal state and disperse state</topic><topic>Composites</topic><topic>Control stability</topic><topic>Coupling agents</topic><topic>Exact sciences and technology</topic><topic>Falling</topic><topic>General and physical chemistry</topic><topic>Glass</topic><topic>Inorganic Chemistry</topic><topic>Materials Science</topic><topic>Monomers</topic><topic>Nanotechnology</topic><topic>Natural Materials</topic><topic>Optical and Electronic Materials</topic><topic>Original Paper</topic><topic>Polymethyl methacrylate</topic><topic>Polymethyl methacrylates</topic><topic>Refractivity</topic><topic>Spectra</topic><topic>Storage stability</topic><topic>Substrates</topic><topic>Thin films</topic><topic>Titanium dioxide</topic><topic>Ultraviolet radiation</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Chang, Chao-Ching</creatorcontrib><creatorcontrib>Cheng, Liao-Ping</creatorcontrib><creatorcontrib>Huang, Feng-Hsi</creatorcontrib><creatorcontrib>Lin, Chia-Ying</creatorcontrib><creatorcontrib>Hsieh, Chi-Fa</creatorcontrib><creatorcontrib>Wang, Wei-Hong</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of sol-gel science and technology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Chang, Chao-Ching</au><au>Cheng, Liao-Ping</au><au>Huang, Feng-Hsi</au><au>Lin, Chia-Ying</au><au>Hsieh, Chi-Fa</au><au>Wang, Wei-Hong</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Preparation and characterization of TiO2 hybrid sol for UV-curable high-refractive-index organic–inorganic hybrid thin films</atitle><jtitle>Journal of sol-gel science and technology</jtitle><stitle>J Sol-Gel Sci Technol</stitle><date>2010-08-01</date><risdate>2010</risdate><volume>55</volume><issue>2</issue><spage>199</spage><epage>206</epage><pages>199-206</pages><issn>0928-0707</issn><eissn>1573-4846</eissn><abstract>In this study, UV-curable hybrid thin films were successfully prepared from TiO
2
and TiO
2
hybrid sols containing the acrylic monomer DPHA on PMMA substrates. The prepared TiO
2
and TiO
2
hybrid sols showed long-term storage stability and can provide operating control for the preparation of high-refractive-index hybrid thin films. The existence of interaction between the TiO
2
particle and the coupling agent was evidenced by FT-IR and UV–visible spectra. All hybrid thin films showed good adhesion to the PMMA substrate with refractive index falling over the range 1.64–1.77. These results suggested the potential application of present TiO
2
hybrid films in optical devices, such as anti-reflective coatings.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1007/s10971-010-2233-6</doi><tpages>8</tpages></addata></record> |
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| subjects | Adhesion Antireflection coatings Ceramics Chemistry Chemistry and Materials Science Colloidal gels. Colloidal sols Colloidal state and disperse state Composites Control stability Coupling agents Exact sciences and technology Falling General and physical chemistry Glass Inorganic Chemistry Materials Science Monomers Nanotechnology Natural Materials Optical and Electronic Materials Original Paper Polymethyl methacrylate Polymethyl methacrylates Refractivity Spectra Storage stability Substrates Thin films Titanium dioxide Ultraviolet radiation |
| title | Preparation and characterization of TiO2 hybrid sol for UV-curable high-refractive-index organic–inorganic hybrid thin films |
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