Dissipation and Residue Determination of Fluoroglycofen-Ethyl in Soybean and Soil by UPLC-MS–MS
A rapid, highly selective, and sensitive method was developed for detecting fluoroglycofen-ethyl in soybean seed, plant, and soil using UPLC-MS–MS. The detection limits of fluoroglycofen-ethyl in soybean seed, plant, and soil were 0.5, 1, and 1 μg kg −1 , respectively. Recoveries ranged from 83.4 %...
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| Veröffentlicht in: | Bulletin of environmental contamination and toxicology 2012-09, Vol.89 (3), p.669-673 |
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| creator | Geng, Yue Jia, Ran Li, Chongjiu Ma, Xiaodong Lin, Yan |
| description | A rapid, highly selective, and sensitive method was developed for detecting fluoroglycofen-ethyl in soybean seed, plant, and soil using UPLC-MS–MS. The detection limits of fluoroglycofen-ethyl in soybean seed, plant, and soil were 0.5, 1, and 1 μg kg
−1
, respectively. Recoveries ranged from 83.4 % to 99.2 %, in which intra-day RSDs were from 1.3 % to 6.7 % and inter-day RSDs were from 1.9 % to 7.0%. In the dissipation study, the half-lives of fluoroglycofen-ethyl were 34.8 (Shanxi) and 48.5 h (Heilongjiang) in soil and 43.3 h in soybean plant in both locations. The residues of fluoroglycofen-ethyl in all samples were below LODs 30 days before and during harvest. |
| doi_str_mv | 10.1007/s00128-012-0681-0 |
| format | Article |
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−1
, respectively. Recoveries ranged from 83.4 % to 99.2 %, in which intra-day RSDs were from 1.3 % to 6.7 % and inter-day RSDs were from 1.9 % to 7.0%. In the dissipation study, the half-lives of fluoroglycofen-ethyl were 34.8 (Shanxi) and 48.5 h (Heilongjiang) in soil and 43.3 h in soybean plant in both locations. The residues of fluoroglycofen-ethyl in all samples were below LODs 30 days before and during harvest.</description><identifier>ISSN: 0007-4861</identifier><identifier>EISSN: 1432-0800</identifier><identifier>DOI: 10.1007/s00128-012-0681-0</identifier><identifier>PMID: 22752219</identifier><language>eng</language><publisher>New York: Springer-Verlag</publisher><subject>Aquatic Pollution ; Chromatography, Liquid - methods ; Detection limits ; Earth and Environmental Science ; Ecotoxicology ; Environment ; Environmental Chemistry ; Environmental Health ; Glycine max - chemistry ; Herbicides ; Herbicides - analysis ; Hydrocarbons, Halogenated - analysis ; Nitrobenzoates - analysis ; Pollution ; Reproducibility of Results ; Residues ; Soil Pollutants - analysis ; Soil Science & Conservation ; Soils ; Soybeans ; Tandem Mass Spectrometry - methods ; Toxicology ; Waste Water Technology ; Water Management ; Water Pollution Control</subject><ispartof>Bulletin of environmental contamination and toxicology, 2012-09, Vol.89 (3), p.669-673</ispartof><rights>Springer Science+Business Media, LLC 2012</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c405t-ad152cbc25bb25095a4a889379ac3cd4d845d637b786e69656c565b6a2fbc86e3</citedby><cites>FETCH-LOGICAL-c405t-ad152cbc25bb25095a4a889379ac3cd4d845d637b786e69656c565b6a2fbc86e3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s00128-012-0681-0$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s00128-012-0681-0$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/22752219$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Geng, Yue</creatorcontrib><creatorcontrib>Jia, Ran</creatorcontrib><creatorcontrib>Li, Chongjiu</creatorcontrib><creatorcontrib>Ma, Xiaodong</creatorcontrib><creatorcontrib>Lin, Yan</creatorcontrib><title>Dissipation and Residue Determination of Fluoroglycofen-Ethyl in Soybean and Soil by UPLC-MS–MS</title><title>Bulletin of environmental contamination and toxicology</title><addtitle>Bull Environ Contam Toxicol</addtitle><addtitle>Bull Environ Contam Toxicol</addtitle><description>A rapid, highly selective, and sensitive method was developed for detecting fluoroglycofen-ethyl in soybean seed, plant, and soil using UPLC-MS–MS. The detection limits of fluoroglycofen-ethyl in soybean seed, plant, and soil were 0.5, 1, and 1 μg kg
−1
, respectively. Recoveries ranged from 83.4 % to 99.2 %, in which intra-day RSDs were from 1.3 % to 6.7 % and inter-day RSDs were from 1.9 % to 7.0%. In the dissipation study, the half-lives of fluoroglycofen-ethyl were 34.8 (Shanxi) and 48.5 h (Heilongjiang) in soil and 43.3 h in soybean plant in both locations. The residues of fluoroglycofen-ethyl in all samples were below LODs 30 days before and during harvest.</description><subject>Aquatic Pollution</subject><subject>Chromatography, Liquid - methods</subject><subject>Detection limits</subject><subject>Earth and Environmental Science</subject><subject>Ecotoxicology</subject><subject>Environment</subject><subject>Environmental Chemistry</subject><subject>Environmental Health</subject><subject>Glycine max - chemistry</subject><subject>Herbicides</subject><subject>Herbicides - analysis</subject><subject>Hydrocarbons, Halogenated - analysis</subject><subject>Nitrobenzoates - analysis</subject><subject>Pollution</subject><subject>Reproducibility of Results</subject><subject>Residues</subject><subject>Soil Pollutants - analysis</subject><subject>Soil Science & Conservation</subject><subject>Soils</subject><subject>Soybeans</subject><subject>Tandem Mass Spectrometry - methods</subject><subject>Toxicology</subject><subject>Waste Water Technology</subject><subject>Water Management</subject><subject>Water Pollution Control</subject><issn>0007-4861</issn><issn>1432-0800</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><sourceid>BENPR</sourceid><recordid>eNp1kM1OxCAUhYnR6PjzAG5MEzduUKBAYWlm_EvGaBxdN0CpYjplhHbRne_gG_okYqrGmLi5N5f7nXPJAWAfo2OMUHESEcJEwFQg4gJDtAYmmOZpEgitgwlKEKSC4y2wHeNzopkgZBNsEVIwQrCcADVzMbqV6pxvM9VW2Z2NruptNrOdDUvXjhtfZ-dN74N_bAbja9vCs-5paDLXZgs_aKtG8cK7JtND9nA7n8Lrxfvr2_ViF2zUqol276vvgIfzs_vpJZzfXFxNT-fQUMQ6qCrMiNGGMK0JQ5IpqoSQeSGVyU1FK0FZxfNCF4JbLjnjhnGmuSK1Nukp3wFHo-8q-Jfexq5cumhs06jW-j6WGHGJpUC0SOjhH_TZ96FNv0tUXhAuqaSJwiNlgo8x2LpcBbdUYUhQ-Zl_OeZfplJ-5l-ipDn4cu710lY_iu_AE0BGIKZV-2jD79P_uX4AK12PcA</recordid><startdate>20120901</startdate><enddate>20120901</enddate><creator>Geng, Yue</creator><creator>Jia, Ran</creator><creator>Li, Chongjiu</creator><creator>Ma, Xiaodong</creator><creator>Lin, Yan</creator><general>Springer-Verlag</general><general>Springer Nature B.V</general><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7T7</scope><scope>7TK</scope><scope>7TV</scope><scope>7U7</scope><scope>7X7</scope><scope>7XB</scope><scope>88E</scope><scope>88I</scope><scope>8C1</scope><scope>8FD</scope><scope>8FI</scope><scope>8FJ</scope><scope>8FK</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BHPHI</scope><scope>C1K</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>FR3</scope><scope>FYUFA</scope><scope>GHDGH</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>K9.</scope><scope>M0S</scope><scope>M1P</scope><scope>M2P</scope><scope>P64</scope><scope>PATMY</scope><scope>PHGZM</scope><scope>PHGZT</scope><scope>PJZUB</scope><scope>PKEHL</scope><scope>PPXIY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PYCSY</scope><scope>Q9U</scope><scope>7ST</scope><scope>SOI</scope></search><sort><creationdate>20120901</creationdate><title>Dissipation and Residue Determination of Fluoroglycofen-Ethyl in Soybean and Soil by UPLC-MS–MS</title><author>Geng, Yue ; Jia, Ran ; Li, Chongjiu ; Ma, Xiaodong ; Lin, Yan</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c405t-ad152cbc25bb25095a4a889379ac3cd4d845d637b786e69656c565b6a2fbc86e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Aquatic Pollution</topic><topic>Chromatography, Liquid - methods</topic><topic>Detection limits</topic><topic>Earth and Environmental Science</topic><topic>Ecotoxicology</topic><topic>Environment</topic><topic>Environmental Chemistry</topic><topic>Environmental Health</topic><topic>Glycine max - chemistry</topic><topic>Herbicides</topic><topic>Herbicides - analysis</topic><topic>Hydrocarbons, Halogenated - analysis</topic><topic>Nitrobenzoates - analysis</topic><topic>Pollution</topic><topic>Reproducibility of Results</topic><topic>Residues</topic><topic>Soil Pollutants - analysis</topic><topic>Soil Science & Conservation</topic><topic>Soils</topic><topic>Soybeans</topic><topic>Tandem Mass Spectrometry - methods</topic><topic>Toxicology</topic><topic>Waste Water Technology</topic><topic>Water Management</topic><topic>Water Pollution Control</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Geng, Yue</creatorcontrib><creatorcontrib>Jia, Ran</creatorcontrib><creatorcontrib>Li, Chongjiu</creatorcontrib><creatorcontrib>Ma, Xiaodong</creatorcontrib><creatorcontrib>Lin, Yan</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Industrial and Applied Microbiology Abstracts (Microbiology A)</collection><collection>Neurosciences Abstracts</collection><collection>Pollution Abstracts</collection><collection>Toxicology Abstracts</collection><collection>Health & Medical Collection</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Medical Database (Alumni Edition)</collection><collection>Science Database (Alumni Edition)</collection><collection>Public Health Database</collection><collection>Technology Research Database</collection><collection>Hospital Premium Collection</collection><collection>Hospital Premium Collection (Alumni Edition)</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Natural Science Collection</collection><collection>Environmental Sciences and Pollution Management</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>Engineering Research Database</collection><collection>Health Research Premium Collection</collection><collection>Health Research Premium Collection (Alumni)</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Health & Medical Complete (Alumni)</collection><collection>Health & Medical Collection (Alumni Edition)</collection><collection>Medical Database</collection><collection>Science Database</collection><collection>Biotechnology and BioEngineering Abstracts</collection><collection>Environmental Science Database</collection><collection>ProQuest Central (New)</collection><collection>ProQuest One Academic (New)</collection><collection>ProQuest Health & Medical Research Collection</collection><collection>ProQuest One Academic Middle East (New)</collection><collection>ProQuest One Health & Nursing</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Environmental Science Collection</collection><collection>ProQuest Central Basic</collection><collection>Environment Abstracts</collection><collection>Environment Abstracts</collection><jtitle>Bulletin of environmental contamination and toxicology</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Geng, Yue</au><au>Jia, Ran</au><au>Li, Chongjiu</au><au>Ma, Xiaodong</au><au>Lin, Yan</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Dissipation and Residue Determination of Fluoroglycofen-Ethyl in Soybean and Soil by UPLC-MS–MS</atitle><jtitle>Bulletin of environmental contamination and toxicology</jtitle><stitle>Bull Environ Contam Toxicol</stitle><addtitle>Bull Environ Contam Toxicol</addtitle><date>2012-09-01</date><risdate>2012</risdate><volume>89</volume><issue>3</issue><spage>669</spage><epage>673</epage><pages>669-673</pages><issn>0007-4861</issn><eissn>1432-0800</eissn><abstract>A rapid, highly selective, and sensitive method was developed for detecting fluoroglycofen-ethyl in soybean seed, plant, and soil using UPLC-MS–MS. The detection limits of fluoroglycofen-ethyl in soybean seed, plant, and soil were 0.5, 1, and 1 μg kg
−1
, respectively. Recoveries ranged from 83.4 % to 99.2 %, in which intra-day RSDs were from 1.3 % to 6.7 % and inter-day RSDs were from 1.9 % to 7.0%. In the dissipation study, the half-lives of fluoroglycofen-ethyl were 34.8 (Shanxi) and 48.5 h (Heilongjiang) in soil and 43.3 h in soybean plant in both locations. The residues of fluoroglycofen-ethyl in all samples were below LODs 30 days before and during harvest.</abstract><cop>New York</cop><pub>Springer-Verlag</pub><pmid>22752219</pmid><doi>10.1007/s00128-012-0681-0</doi><tpages>5</tpages></addata></record> |
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| ispartof | Bulletin of environmental contamination and toxicology, 2012-09, Vol.89 (3), p.669-673 |
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| subjects | Aquatic Pollution Chromatography, Liquid - methods Detection limits Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Glycine max - chemistry Herbicides Herbicides - analysis Hydrocarbons, Halogenated - analysis Nitrobenzoates - analysis Pollution Reproducibility of Results Residues Soil Pollutants - analysis Soil Science & Conservation Soils Soybeans Tandem Mass Spectrometry - methods Toxicology Waste Water Technology Water Management Water Pollution Control |
| title | Dissipation and Residue Determination of Fluoroglycofen-Ethyl in Soybean and Soil by UPLC-MS–MS |
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