AlN homoepitaxial growth on sublimation-AlN substrate by low-pressure HVPE

Crack-free thick AlN layers with low impurity concentrations were grown on free-standing AlN substrates fabricated by a sublimation method. Cracks due to tensile stresses were generated in the overgrowth layer when using on-axis AlN (0001) substrates, as indicated by Raman scattering spectroscopy. I...

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Veröffentlicht in:Journal of crystal growth 2012-07, Vol.350 (1), p.69-71
Hauptverfasser: Nomura, Takuya, Okumura, Kenta, Miyake, Hideto, Hiramatsu, Kazumasa, Eryu, Osamu, Yamada, Yoichi
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container_end_page 71
container_issue 1
container_start_page 69
container_title Journal of crystal growth
container_volume 350
creator Nomura, Takuya
Okumura, Kenta
Miyake, Hideto
Hiramatsu, Kazumasa
Eryu, Osamu
Yamada, Yoichi
description Crack-free thick AlN layers with low impurity concentrations were grown on free-standing AlN substrates fabricated by a sublimation method. Cracks due to tensile stresses were generated in the overgrowth layer when using on-axis AlN (0001) substrates, as indicated by Raman scattering spectroscopy. In contrast, cracks were not generated when using 5° off-angle AlN (0001) substrates. High crystalline quality was indicated by X-ray rocking curve (XRC) analysis. The full width at half maximum (FWHM) values of the (0002) and (10–10) diffractions were 277 and 306arcsec, respectively. Secondary ion mass spectrometry (SIMS) measurements indicated that the Si and C impurity concentrations were reduced to half of those in the sublimation-grown AlN substrates.
doi_str_mv 10.1016/j.jcrysgro.2011.12.025
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source ScienceDirect Journals (5 years ago - present)
subjects A2. Homoepitaxial growth
A3. HVPE
Aluminum nitride
B1. AlN
Condensed matter: structure, mechanical and thermal properties
Cracks
Cross-disciplinary physics: materials science
rheology
Crystal growth
Diffraction
Exact sciences and technology
Growth from vapor
Impurities
Materials science
Methods of crystal growth
physics of crystal growth
Methods of deposition of films and coatings
film growth and epitaxy
Physics
Secondary ion mass spectrometry
Silicon substrates
Structure of solids and liquids
crystallography
Structure of specific crystalline solids
Tensile stress
Vapor phase epitaxy
growth from vapor phase
title AlN homoepitaxial growth on sublimation-AlN substrate by low-pressure HVPE
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