Morphology, structure and chemistry of extracted diesel sootaPart I: Transmission electron microscopy, Raman spectroscopy, X-ray photoelectron spectroscopy and synchrotron X-ray diffraction study
Inclusion of soot in lubricating oil can result in increased wear and decreased lubricity. In this study we have attempted to gain fundamental insight into the morphology, structure and chemistry of diesel soot. Energy dispersive spectroscopy using TEM suggests interaction between lubrication additi...
Gespeichert in:
| Veröffentlicht in: | Tribology international 2012-08, Vol.52, p.29-39 |
|---|---|
| Hauptverfasser: | , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 39 |
|---|---|
| container_issue | |
| container_start_page | 29 |
| container_title | Tribology international |
| container_volume | 52 |
| creator | Patel, Mihir Azanza Ricardo, Cristy Leonor Scardi, Paolo Aswath, Pranesh B |
| description | Inclusion of soot in lubricating oil can result in increased wear and decreased lubricity. In this study we have attempted to gain fundamental insight into the morphology, structure and chemistry of diesel soot. Energy dispersive spectroscopy using TEM suggests interaction between lubrication additives and crankcase soot resulting in the presence of C, Ca, S, P, O and Zn. Synchrotron X-ray diffraction indicates the presence of different sulfates of calcium as well as the presence of amorphous zinc based compounds. Raman spectroscopy and selected area diffraction using TEM indicates that the turbostratic structures of the carbon in both are very similar. |
| doi_str_mv | 10.1016/j.triboint.2012.03.004 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest</sourceid><recordid>TN_cdi_proquest_miscellaneous_1038249304</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>1038249304</sourcerecordid><originalsourceid>FETCH-proquest_miscellaneous_10382493043</originalsourceid><addsrcrecordid>eNqVTrtOxDAQdAESx-MXkEsKEtZJdCG0CATFSQhdcd3JOA7xKfEG70Yi38eP4QsnREu1o3nsjBCXClIFanmzSzm4N3Se0wxUlkKeAhRHYgE5qGRZVpsTcUq0A4CyqMqF-FphGFrs8H26lsRhNDwGK7WvpWlt7yI1SWyk_eSgDdta1s6S7SQhsn7RgeXznVwH7SmayaGXtrOGQwS9MwHJ4BBfv-pee0nDLB24TRL0JGM742_mr2NeQZM3bcBZ_AnUrmn2W_ZdxGM9nYvjRndkLw73TFw9Pqzvn5Ih4MdoibdxmrFdp73FkbYK8tusqHIo8n9YvwGj63ei</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>1038249304</pqid></control><display><type>article</type><title>Morphology, structure and chemistry of extracted diesel sootaPart I: Transmission electron microscopy, Raman spectroscopy, X-ray photoelectron spectroscopy and synchrotron X-ray diffraction study</title><source>ScienceDirect Freedom Collection (Elsevier)</source><creator>Patel, Mihir ; Azanza Ricardo, Cristy Leonor ; Scardi, Paolo ; Aswath, Pranesh B</creator><creatorcontrib>Patel, Mihir ; Azanza Ricardo, Cristy Leonor ; Scardi, Paolo ; Aswath, Pranesh B</creatorcontrib><description>Inclusion of soot in lubricating oil can result in increased wear and decreased lubricity. In this study we have attempted to gain fundamental insight into the morphology, structure and chemistry of diesel soot. Energy dispersive spectroscopy using TEM suggests interaction between lubrication additives and crankcase soot resulting in the presence of C, Ca, S, P, O and Zn. Synchrotron X-ray diffraction indicates the presence of different sulfates of calcium as well as the presence of amorphous zinc based compounds. Raman spectroscopy and selected area diffraction using TEM indicates that the turbostratic structures of the carbon in both are very similar.</description><identifier>ISSN: 0301-679X</identifier><identifier>DOI: 10.1016/j.triboint.2012.03.004</identifier><language>eng</language><subject>Diesel ; Diesel fuels ; Diffraction ; Lubrication ; Soot ; Transmission electron microscopy ; X-rays ; Zinc</subject><ispartof>Tribology international, 2012-08, Vol.52, p.29-39</ispartof><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,780,784,27924,27925</link.rule.ids></links><search><creatorcontrib>Patel, Mihir</creatorcontrib><creatorcontrib>Azanza Ricardo, Cristy Leonor</creatorcontrib><creatorcontrib>Scardi, Paolo</creatorcontrib><creatorcontrib>Aswath, Pranesh B</creatorcontrib><title>Morphology, structure and chemistry of extracted diesel sootaPart I: Transmission electron microscopy, Raman spectroscopy, X-ray photoelectron spectroscopy and synchrotron X-ray diffraction study</title><title>Tribology international</title><description>Inclusion of soot in lubricating oil can result in increased wear and decreased lubricity. In this study we have attempted to gain fundamental insight into the morphology, structure and chemistry of diesel soot. Energy dispersive spectroscopy using TEM suggests interaction between lubrication additives and crankcase soot resulting in the presence of C, Ca, S, P, O and Zn. Synchrotron X-ray diffraction indicates the presence of different sulfates of calcium as well as the presence of amorphous zinc based compounds. Raman spectroscopy and selected area diffraction using TEM indicates that the turbostratic structures of the carbon in both are very similar.</description><subject>Diesel</subject><subject>Diesel fuels</subject><subject>Diffraction</subject><subject>Lubrication</subject><subject>Soot</subject><subject>Transmission electron microscopy</subject><subject>X-rays</subject><subject>Zinc</subject><issn>0301-679X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNqVTrtOxDAQdAESx-MXkEsKEtZJdCG0CATFSQhdcd3JOA7xKfEG70Yi38eP4QsnREu1o3nsjBCXClIFanmzSzm4N3Se0wxUlkKeAhRHYgE5qGRZVpsTcUq0A4CyqMqF-FphGFrs8H26lsRhNDwGK7WvpWlt7yI1SWyk_eSgDdta1s6S7SQhsn7RgeXznVwH7SmayaGXtrOGQwS9MwHJ4BBfv-pee0nDLB24TRL0JGM742_mr2NeQZM3bcBZ_AnUrmn2W_ZdxGM9nYvjRndkLw73TFw9Pqzvn5Ih4MdoibdxmrFdp73FkbYK8tusqHIo8n9YvwGj63ei</recordid><startdate>20120801</startdate><enddate>20120801</enddate><creator>Patel, Mihir</creator><creator>Azanza Ricardo, Cristy Leonor</creator><creator>Scardi, Paolo</creator><creator>Aswath, Pranesh B</creator><scope>7SR</scope><scope>7TB</scope><scope>7U5</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope></search><sort><creationdate>20120801</creationdate><title>Morphology, structure and chemistry of extracted diesel sootaPart I: Transmission electron microscopy, Raman spectroscopy, X-ray photoelectron spectroscopy and synchrotron X-ray diffraction study</title><author>Patel, Mihir ; Azanza Ricardo, Cristy Leonor ; Scardi, Paolo ; Aswath, Pranesh B</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-proquest_miscellaneous_10382493043</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Diesel</topic><topic>Diesel fuels</topic><topic>Diffraction</topic><topic>Lubrication</topic><topic>Soot</topic><topic>Transmission electron microscopy</topic><topic>X-rays</topic><topic>Zinc</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Patel, Mihir</creatorcontrib><creatorcontrib>Azanza Ricardo, Cristy Leonor</creatorcontrib><creatorcontrib>Scardi, Paolo</creatorcontrib><creatorcontrib>Aswath, Pranesh B</creatorcontrib><collection>Engineered Materials Abstracts</collection><collection>Mechanical & Transportation Engineering Abstracts</collection><collection>Solid State and Superconductivity Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Tribology international</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Patel, Mihir</au><au>Azanza Ricardo, Cristy Leonor</au><au>Scardi, Paolo</au><au>Aswath, Pranesh B</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Morphology, structure and chemistry of extracted diesel sootaPart I: Transmission electron microscopy, Raman spectroscopy, X-ray photoelectron spectroscopy and synchrotron X-ray diffraction study</atitle><jtitle>Tribology international</jtitle><date>2012-08-01</date><risdate>2012</risdate><volume>52</volume><spage>29</spage><epage>39</epage><pages>29-39</pages><issn>0301-679X</issn><abstract>Inclusion of soot in lubricating oil can result in increased wear and decreased lubricity. In this study we have attempted to gain fundamental insight into the morphology, structure and chemistry of diesel soot. Energy dispersive spectroscopy using TEM suggests interaction between lubrication additives and crankcase soot resulting in the presence of C, Ca, S, P, O and Zn. Synchrotron X-ray diffraction indicates the presence of different sulfates of calcium as well as the presence of amorphous zinc based compounds. Raman spectroscopy and selected area diffraction using TEM indicates that the turbostratic structures of the carbon in both are very similar.</abstract><doi>10.1016/j.triboint.2012.03.004</doi></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 0301-679X |
| ispartof | Tribology international, 2012-08, Vol.52, p.29-39 |
| issn | 0301-679X |
| language | eng |
| recordid | cdi_proquest_miscellaneous_1038249304 |
| source | ScienceDirect Freedom Collection (Elsevier) |
| subjects | Diesel Diesel fuels Diffraction Lubrication Soot Transmission electron microscopy X-rays Zinc |
| title | Morphology, structure and chemistry of extracted diesel sootaPart I: Transmission electron microscopy, Raman spectroscopy, X-ray photoelectron spectroscopy and synchrotron X-ray diffraction study |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2024-12-24T07%3A03%3A58IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Morphology,%20structure%20and%20chemistry%20of%20extracted%20diesel%20sootaPart%20I:%20Transmission%20electron%20microscopy,%20Raman%20spectroscopy,%20X-ray%20photoelectron%20spectroscopy%20and%20synchrotron%20X-ray%20diffraction%20study&rft.jtitle=Tribology%20international&rft.au=Patel,%20Mihir&rft.date=2012-08-01&rft.volume=52&rft.spage=29&rft.epage=39&rft.pages=29-39&rft.issn=0301-679X&rft_id=info:doi/10.1016/j.triboint.2012.03.004&rft_dat=%3Cproquest%3E1038249304%3C/proquest%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=1038249304&rft_id=info:pmid/&rfr_iscdi=true |