Synthesis and Characterization of Zinc(II) Oxide Nanoparticles by Thermal Decomposition of Two Zinc(II) Nitrite Coordination Polymer Precursors
Two zinc(II) coordination polymers, {[Zn(3-bpdb)(NO 2 )]·0.5H 2 O} n ( 1 ) and [Zn(4-bpdb)(NO 2 ) 2 ] n ( 2 ), 3-bpdb = 1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene}, have been synthesized and characterized by elemental analyses and IR spectrosco...
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| Veröffentlicht in: | Journal of inorganic and organometallic polymers and materials 2012-03, Vol.22 (2), p.526-529 |
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| creator | Aghabeygi, Shokufeh Bigdeli, Fahime Morsali, Ali |
| description | Two zinc(II) coordination polymers, {[Zn(3-bpdb)(NO
2
)]·0.5H
2
O}
n
(
1
) and [Zn(4-bpdb)(NO
2
)
2
]
n
(
2
), 3-bpdb = 1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene}, have been synthesized and characterized by elemental analyses and IR spectroscopy. Nanoparticles of zinc(II) oxide have been prepared by thermolyses of two different zinc(II) coordination polymers,
1
–
2
. The nano-materials were characterized by scanning electron microscopy, X-ray powder diffraction and IR spectroscopy. The thermal stability of ZnO nano-particles was studied by thermal gravimetric and differential thermal analysis and showed that there is no loss of weight, which indicates that the products were zinc(II) oxide. This study demonstrates the coordination polymers may be suitable precursors for the preparation of nanoscale materials. |
| doi_str_mv | 10.1007/s10904-011-9575-6 |
| format | Article |
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2
)]·0.5H
2
O}
n
(
1
) and [Zn(4-bpdb)(NO
2
)
2
]
n
(
2
), 3-bpdb = 1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene}, have been synthesized and characterized by elemental analyses and IR spectroscopy. Nanoparticles of zinc(II) oxide have been prepared by thermolyses of two different zinc(II) coordination polymers,
1
–
2
. The nano-materials were characterized by scanning electron microscopy, X-ray powder diffraction and IR spectroscopy. The thermal stability of ZnO nano-particles was studied by thermal gravimetric and differential thermal analysis and showed that there is no loss of weight, which indicates that the products were zinc(II) oxide. This study demonstrates the coordination polymers may be suitable precursors for the preparation of nanoscale materials.</description><identifier>ISSN: 1574-1443</identifier><identifier>EISSN: 1574-1451</identifier><identifier>DOI: 10.1007/s10904-011-9575-6</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Chemistry ; Chemistry and Materials Science ; Communication ; Coordination polymers ; Infrared radiation ; Inorganic Chemistry ; Nanocomposites ; Nanomaterials ; Nanostructure ; Organic Chemistry ; Oxides ; Polymer Sciences ; Precursors ; Spectroscopy</subject><ispartof>Journal of inorganic and organometallic polymers and materials, 2012-03, Vol.22 (2), p.526-529</ispartof><rights>Springer Science+Business Media, LLC 2011</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c321t-131f82dd87e96c4e2e3bf35a9788b31b0fd0286e6d206feefeff13df3255a083</citedby><cites>FETCH-LOGICAL-c321t-131f82dd87e96c4e2e3bf35a9788b31b0fd0286e6d206feefeff13df3255a083</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10904-011-9575-6$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10904-011-9575-6$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Aghabeygi, Shokufeh</creatorcontrib><creatorcontrib>Bigdeli, Fahime</creatorcontrib><creatorcontrib>Morsali, Ali</creatorcontrib><title>Synthesis and Characterization of Zinc(II) Oxide Nanoparticles by Thermal Decomposition of Two Zinc(II) Nitrite Coordination Polymer Precursors</title><title>Journal of inorganic and organometallic polymers and materials</title><addtitle>J Inorg Organomet Polym</addtitle><description>Two zinc(II) coordination polymers, {[Zn(3-bpdb)(NO
2
)]·0.5H
2
O}
n
(
1
) and [Zn(4-bpdb)(NO
2
)
2
]
n
(
2
), 3-bpdb = 1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene}, have been synthesized and characterized by elemental analyses and IR spectroscopy. Nanoparticles of zinc(II) oxide have been prepared by thermolyses of two different zinc(II) coordination polymers,
1
–
2
. The nano-materials were characterized by scanning electron microscopy, X-ray powder diffraction and IR spectroscopy. The thermal stability of ZnO nano-particles was studied by thermal gravimetric and differential thermal analysis and showed that there is no loss of weight, which indicates that the products were zinc(II) oxide. This study demonstrates the coordination polymers may be suitable precursors for the preparation of nanoscale materials.</description><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Communication</subject><subject>Coordination polymers</subject><subject>Infrared radiation</subject><subject>Inorganic Chemistry</subject><subject>Nanocomposites</subject><subject>Nanomaterials</subject><subject>Nanostructure</subject><subject>Organic Chemistry</subject><subject>Oxides</subject><subject>Polymer Sciences</subject><subject>Precursors</subject><subject>Spectroscopy</subject><issn>1574-1443</issn><issn>1574-1451</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><recordid>eNp9kMlOwzAQQCMEEqXwAdx8hEPAE2c9orJVQoBET1ws1xlTV4ldxqmg_AS_TKqw3DjNHN4baV4UHQM_A86L8wC84mnMAeIqK7I434lGkBVpDGkGu797KvajgxCWnIuSZzCKPp82rltgsIEpV7PJQpHSHZL9UJ31jnnDnq3TJ9PpKXt4tzWye-X8SlFndYOBzTdstkBqVcMuUft25YP9EWdv_k--tx3ZDtnEe6qtG64_-mbTIrFHQr2m4CkcRntGNQGPvuc4ml1fzSa38d3DzXRycRdrkUAXgwBTJnVdFljlOsUExdyITFVFWc4FzLmpeVLmmNcJzw2iQWNA1EYkWaZ4KcbRyXB2Rf51jaGTrQ0am0Y59OsggQsQvCrSLQoDqsmHQGjkimyraNNDctteDu1l315u28u8d5LBCT3rXpDk0q_J9Q_9I30Brq6JZA</recordid><startdate>20120301</startdate><enddate>20120301</enddate><creator>Aghabeygi, Shokufeh</creator><creator>Bigdeli, Fahime</creator><creator>Morsali, Ali</creator><general>Springer US</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20120301</creationdate><title>Synthesis and Characterization of Zinc(II) Oxide Nanoparticles by Thermal Decomposition of Two Zinc(II) Nitrite Coordination Polymer Precursors</title><author>Aghabeygi, Shokufeh ; Bigdeli, Fahime ; Morsali, Ali</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c321t-131f82dd87e96c4e2e3bf35a9788b31b0fd0286e6d206feefeff13df3255a083</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Communication</topic><topic>Coordination polymers</topic><topic>Infrared radiation</topic><topic>Inorganic Chemistry</topic><topic>Nanocomposites</topic><topic>Nanomaterials</topic><topic>Nanostructure</topic><topic>Organic Chemistry</topic><topic>Oxides</topic><topic>Polymer Sciences</topic><topic>Precursors</topic><topic>Spectroscopy</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Aghabeygi, Shokufeh</creatorcontrib><creatorcontrib>Bigdeli, Fahime</creatorcontrib><creatorcontrib>Morsali, Ali</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of inorganic and organometallic polymers and materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Aghabeygi, Shokufeh</au><au>Bigdeli, Fahime</au><au>Morsali, Ali</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and Characterization of Zinc(II) Oxide Nanoparticles by Thermal Decomposition of Two Zinc(II) Nitrite Coordination Polymer Precursors</atitle><jtitle>Journal of inorganic and organometallic polymers and materials</jtitle><stitle>J Inorg Organomet Polym</stitle><date>2012-03-01</date><risdate>2012</risdate><volume>22</volume><issue>2</issue><spage>526</spage><epage>529</epage><pages>526-529</pages><issn>1574-1443</issn><eissn>1574-1451</eissn><abstract>Two zinc(II) coordination polymers, {[Zn(3-bpdb)(NO
2
)]·0.5H
2
O}
n
(
1
) and [Zn(4-bpdb)(NO
2
)
2
]
n
(
2
), 3-bpdb = 1,4-bis(3-pyridyl)-2,3-diaza-1,3-butadiene and 4-bpdb = 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene}, have been synthesized and characterized by elemental analyses and IR spectroscopy. Nanoparticles of zinc(II) oxide have been prepared by thermolyses of two different zinc(II) coordination polymers,
1
–
2
. The nano-materials were characterized by scanning electron microscopy, X-ray powder diffraction and IR spectroscopy. The thermal stability of ZnO nano-particles was studied by thermal gravimetric and differential thermal analysis and showed that there is no loss of weight, which indicates that the products were zinc(II) oxide. This study demonstrates the coordination polymers may be suitable precursors for the preparation of nanoscale materials.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1007/s10904-011-9575-6</doi><tpages>4</tpages></addata></record> |
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| source | SpringerNature Complete Journals |
| subjects | Chemistry Chemistry and Materials Science Communication Coordination polymers Infrared radiation Inorganic Chemistry Nanocomposites Nanomaterials Nanostructure Organic Chemistry Oxides Polymer Sciences Precursors Spectroscopy |
| title | Synthesis and Characterization of Zinc(II) Oxide Nanoparticles by Thermal Decomposition of Two Zinc(II) Nitrite Coordination Polymer Precursors |
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