Structure and properties development in poly(phenylene sulfide) fibers, part I: Effect of material and melt spinning process variables
The detailed research study of manufacturing PPS fibers using melt spinning and further enhancement of tensile properties by drawing and annealing experiments, a study lacking as of today in open scientific literature, was the focus of this research. This article discusses the effect of polymer mole...
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| Veröffentlicht in: | Journal of applied polymer science 2011-12, Vol.122 (5), p.3110-3121 |
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| container_title | Journal of applied polymer science |
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| creator | Gulgunje, Prabhakar Bhat, Gajanan Spruiell, Joseph |
| description | The detailed research study of manufacturing PPS fibers using melt spinning and further enhancement of tensile properties by drawing and annealing experiments, a study lacking as of today in open scientific literature, was the focus of this research. This article discusses the effect of polymer molecular weight (MW) and melt spinning process variables on the structure and properties development in melt spun fibers manufactured from proprietary Fortron® linear PPS resins. Structure‐properties relationship was studied using several characterization tools like tensile testing, differential scanning calorimetry, polarized light optical microscopy, and wide‐angle x‐ray scattering. Changes in dynamic mechanical behavior of as‐spun fibers manufactured from resins of varying MW and different melt spinning take‐up speeds were also studied. The study showed that by a combination of higher MW of the polymer and spinning at higher take‐up speeds, tensile properties of as‐spun PPS fibers can be improved. © 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2011 |
| doi_str_mv | 10.1002/app.34353 |
| format | Article |
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This article discusses the effect of polymer molecular weight (MW) and melt spinning process variables on the structure and properties development in melt spun fibers manufactured from proprietary Fortron® linear PPS resins. Structure‐properties relationship was studied using several characterization tools like tensile testing, differential scanning calorimetry, polarized light optical microscopy, and wide‐angle x‐ray scattering. Changes in dynamic mechanical behavior of as‐spun fibers manufactured from resins of varying MW and different melt spinning take‐up speeds were also studied. The study showed that by a combination of higher MW of the polymer and spinning at higher take‐up speeds, tensile properties of as‐spun PPS fibers can be improved. © 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2011</description><identifier>ISSN: 0021-8995</identifier><identifier>ISSN: 1097-4628</identifier><identifier>EISSN: 1097-4628</identifier><identifier>DOI: 10.1002/app.34353</identifier><identifier>CODEN: JAPNAB</identifier><language>eng</language><publisher>Hoboken: Wiley Subscription Services, Inc., A Wiley Company</publisher><subject>Applied sciences ; Exact sciences and technology ; extrusion ; Fibers ; Fibers and threads ; Forms of application and semi-finished materials ; high performance polymers ; Materials science ; Melt spinning ; Melt spun ; Polymer industry, paints, wood ; Polymers ; Polyphenylene sulfides ; Property development ; Resins ; structure-property relations ; Technology of polymers ; Tensile properties ; thermoplastics</subject><ispartof>Journal of applied polymer science, 2011-12, Vol.122 (5), p.3110-3121</ispartof><rights>Copyright © 2011 Wiley Periodicals, Inc.</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c4643-5d4fb4763cdf0eea6a62acf20f48d021622b1aa5dbc5eb61661152c17698a10b3</citedby><cites>FETCH-LOGICAL-c4643-5d4fb4763cdf0eea6a62acf20f48d021622b1aa5dbc5eb61661152c17698a10b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://onlinelibrary.wiley.com/doi/pdf/10.1002%2Fapp.34353$$EPDF$$P50$$Gwiley$$H</linktopdf><linktohtml>$$Uhttps://onlinelibrary.wiley.com/doi/full/10.1002%2Fapp.34353$$EHTML$$P50$$Gwiley$$H</linktohtml><link.rule.ids>314,780,784,1416,27923,27924,45573,45574</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=24567313$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Gulgunje, Prabhakar</creatorcontrib><creatorcontrib>Bhat, Gajanan</creatorcontrib><creatorcontrib>Spruiell, Joseph</creatorcontrib><title>Structure and properties development in poly(phenylene sulfide) fibers, part I: Effect of material and melt spinning process variables</title><title>Journal of applied polymer science</title><addtitle>J. Appl. Polym. Sci</addtitle><description>The detailed research study of manufacturing PPS fibers using melt spinning and further enhancement of tensile properties by drawing and annealing experiments, a study lacking as of today in open scientific literature, was the focus of this research. This article discusses the effect of polymer molecular weight (MW) and melt spinning process variables on the structure and properties development in melt spun fibers manufactured from proprietary Fortron® linear PPS resins. Structure‐properties relationship was studied using several characterization tools like tensile testing, differential scanning calorimetry, polarized light optical microscopy, and wide‐angle x‐ray scattering. Changes in dynamic mechanical behavior of as‐spun fibers manufactured from resins of varying MW and different melt spinning take‐up speeds were also studied. The study showed that by a combination of higher MW of the polymer and spinning at higher take‐up speeds, tensile properties of as‐spun PPS fibers can be improved. © 2011 Wiley Periodicals, Inc. J Appl Polym Sci, 2011</description><subject>Applied sciences</subject><subject>Exact sciences and technology</subject><subject>extrusion</subject><subject>Fibers</subject><subject>Fibers and threads</subject><subject>Forms of application and semi-finished materials</subject><subject>high performance polymers</subject><subject>Materials science</subject><subject>Melt spinning</subject><subject>Melt spun</subject><subject>Polymer industry, paints, wood</subject><subject>Polymers</subject><subject>Polyphenylene sulfides</subject><subject>Property development</subject><subject>Resins</subject><subject>structure-property relations</subject><subject>Technology of polymers</subject><subject>Tensile properties</subject><subject>thermoplastics</subject><issn>0021-8995</issn><issn>1097-4628</issn><issn>1097-4628</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><recordid>eNp1kU1rFTEUhgdR8Fpd-A8CIrTgtPmYZGbcldIvKHqhisuQyZxoaiYTk0z1_oH-7ub21i4Es8kiz_vkHN6qekvwIcGYHqkQDlnDOHtWrQju27oRtHtercobqbu-5y-rVyndYEwIx2JV3V3nuOi8REDKjyjEOUDMFhIa4RbcHCbwGVmPwuw2--EH-I0DDygtztgRDpCxA8T0AQUVM7r8iE6NAZ3RbNCkMkSr3IN4ApdRCtZ7679vv9GQErpVBRgcpNfVC6NcgjeP91719ez0y8lFffX5_PLk-KrWjWhYzcfGDE0rmB4NBlBCCaq0odg03Vg2FJQORCk-DprDIIgQZU2qSSv6ThE8sL1qf-ctE_xaIGU52aTBOeVhXpIkmNKu423DCvruH_RmXqIv00nCiehxzzteqIMdpeOcUgQjQ7STipuikttGZGlEPjRS2PePRpW0ciYqr216CtCGi5aRLXe0435bB5v_C-Xxev3XXO8SNmX485RQ8acsypbLb5_O5Zpdn_Fy5AW7B15KqiM</recordid><startdate>20111205</startdate><enddate>20111205</enddate><creator>Gulgunje, Prabhakar</creator><creator>Bhat, Gajanan</creator><creator>Spruiell, Joseph</creator><general>Wiley Subscription Services, Inc., A Wiley Company</general><general>Wiley</general><general>Wiley Subscription Services, Inc</general><scope>BSCLL</scope><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20111205</creationdate><title>Structure and properties development in poly(phenylene sulfide) fibers, part I: Effect of material and melt spinning process variables</title><author>Gulgunje, Prabhakar ; Bhat, Gajanan ; Spruiell, Joseph</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c4643-5d4fb4763cdf0eea6a62acf20f48d021622b1aa5dbc5eb61661152c17698a10b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Applied sciences</topic><topic>Exact sciences and technology</topic><topic>extrusion</topic><topic>Fibers</topic><topic>Fibers and threads</topic><topic>Forms of application and semi-finished materials</topic><topic>high performance polymers</topic><topic>Materials science</topic><topic>Melt spinning</topic><topic>Melt spun</topic><topic>Polymer industry, paints, wood</topic><topic>Polymers</topic><topic>Polyphenylene sulfides</topic><topic>Property development</topic><topic>Resins</topic><topic>structure-property relations</topic><topic>Technology of polymers</topic><topic>Tensile properties</topic><topic>thermoplastics</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Gulgunje, Prabhakar</creatorcontrib><creatorcontrib>Bhat, Gajanan</creatorcontrib><creatorcontrib>Spruiell, Joseph</creatorcontrib><collection>Istex</collection><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Journal of applied polymer science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Gulgunje, Prabhakar</au><au>Bhat, Gajanan</au><au>Spruiell, Joseph</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Structure and properties development in poly(phenylene sulfide) fibers, part I: Effect of material and melt spinning process variables</atitle><jtitle>Journal of applied polymer science</jtitle><addtitle>J. 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| subjects | Applied sciences Exact sciences and technology extrusion Fibers Fibers and threads Forms of application and semi-finished materials high performance polymers Materials science Melt spinning Melt spun Polymer industry, paints, wood Polymers Polyphenylene sulfides Property development Resins structure-property relations Technology of polymers Tensile properties thermoplastics |
| title | Structure and properties development in poly(phenylene sulfide) fibers, part I: Effect of material and melt spinning process variables |
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