Degree of conversion of simplified contemporary adhesive systems as influenced by extended air-activated or passive solvent volatilization modes
This study evaluated the effect of five methods of solvent volatilization on the degree of conversion (DC) of nine one-bottle adhesive systems using Fourier transform infrared/attenuated total reflectance (FTIR/ATR) analysis. Nine adhesives were tested: Adper Single Bond 2 (SB), Adper Easy One (EO),...
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| Veröffentlicht in: | Operative dentistry 2012-05, Vol.37 (3), p.246-252 |
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| creator | Borges, Boniek C D Souza-Junior, Eduardo Jose Brandt, William C Loguercio, Alessandro D Montes, Marcos A J R Puppin-Rontani, Regina M Sinhoreti, Mario Alexandre Coelho |
| description | This study evaluated the effect of five methods of solvent volatilization on the degree of conversion (DC) of nine one-bottle adhesive systems using Fourier transform infrared/attenuated total reflectance (FTIR/ATR) analysis. Nine adhesives were tested: Adper Single Bond 2 (SB), Adper Easy One (EO), One Up Bond F Plus (OUP), One Coat Bond SL (OC), XP Bond (XP), Ambar (AM), Natural Bond (NB), GO, and Stae. The adhesive systems were applied to a zinc-selenide pellet and 1) cured without solvent volatilization, 2) left undisturbed for 10 seconds before curing, 3) left undisturbed for 60 seconds before curing, 4) air-dried with an air stream for 10 seconds before curing, and 5) air-dried with an air stream for 60 seconds before curing. FTIR/ATR spectra were obtained, and the DC was calculated by comparing the aliphatic bonds/reference peaks before and after light activation for 10 seconds (FlashLite 1401). The DC means of each material were analyzed by one-way analysis of variance and post hoc Tukey test (p |
| doi_str_mv | 10.2341/11-248-L |
| format | Article |
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Nine adhesives were tested: Adper Single Bond 2 (SB), Adper Easy One (EO), One Up Bond F Plus (OUP), One Coat Bond SL (OC), XP Bond (XP), Ambar (AM), Natural Bond (NB), GO, and Stae. The adhesive systems were applied to a zinc-selenide pellet and 1) cured without solvent volatilization, 2) left undisturbed for 10 seconds before curing, 3) left undisturbed for 60 seconds before curing, 4) air-dried with an air stream for 10 seconds before curing, and 5) air-dried with an air stream for 60 seconds before curing. FTIR/ATR spectra were obtained, and the DC was calculated by comparing the aliphatic bonds/reference peaks before and after light activation for 10 seconds (FlashLite 1401). The DC means of each material were analyzed by one-way analysis of variance and post hoc Tukey test (p<0.05). The DC of GO and Stae adhesive systems was not affected by the five evaporation conditions. Air-drying for 60 seconds before curing yielded the highest DC for SB, EO, and OC. Extended solvent volatilization time (60 seconds) either with or without air-drying before curing provided the highest DC for AM, NB, XP, and OUP. Thus, the monomer conversion of adhesive systems was material dependent. In general, the 60-second passive or active air-drying modes to volatilize solvents before curing enhanced the degree of conversion for the one-bottle simplified adhesive systems.</description><identifier>ISSN: 0361-7734</identifier><identifier>EISSN: 1559-2863</identifier><identifier>DOI: 10.2341/11-248-L</identifier><identifier>PMID: 22313268</identifier><language>eng</language><publisher>United States</publisher><subject>Acetone ; Air ; Dentistry ; Ethanol ; Hardness ; Light-Curing of Dental Adhesives ; Polymerization ; Resin Cements - chemistry ; Solvents ; Spectroscopy, Fourier Transform Infrared ; Volatilization ; Water</subject><ispartof>Operative dentistry, 2012-05, Vol.37 (3), p.246-252</ispartof><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c317t-db301493eb2ca36d6338b79ab3b5638f2b8b4f74152b18394b01650e2eb251d13</citedby><cites>FETCH-LOGICAL-c317t-db301493eb2ca36d6338b79ab3b5638f2b8b4f74152b18394b01650e2eb251d13</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27901,27902</link.rule.ids><backlink>$$Uhttps://www.ncbi.nlm.nih.gov/pubmed/22313268$$D View this record in MEDLINE/PubMed$$Hfree_for_read</backlink></links><search><creatorcontrib>Borges, Boniek C D</creatorcontrib><creatorcontrib>Souza-Junior, Eduardo Jose</creatorcontrib><creatorcontrib>Brandt, William C</creatorcontrib><creatorcontrib>Loguercio, Alessandro D</creatorcontrib><creatorcontrib>Montes, Marcos A J R</creatorcontrib><creatorcontrib>Puppin-Rontani, Regina M</creatorcontrib><creatorcontrib>Sinhoreti, Mario Alexandre Coelho</creatorcontrib><title>Degree of conversion of simplified contemporary adhesive systems as influenced by extended air-activated or passive solvent volatilization modes</title><title>Operative dentistry</title><addtitle>Oper Dent</addtitle><description>This study evaluated the effect of five methods of solvent volatilization on the degree of conversion (DC) of nine one-bottle adhesive systems using Fourier transform infrared/attenuated total reflectance (FTIR/ATR) analysis. Nine adhesives were tested: Adper Single Bond 2 (SB), Adper Easy One (EO), One Up Bond F Plus (OUP), One Coat Bond SL (OC), XP Bond (XP), Ambar (AM), Natural Bond (NB), GO, and Stae. The adhesive systems were applied to a zinc-selenide pellet and 1) cured without solvent volatilization, 2) left undisturbed for 10 seconds before curing, 3) left undisturbed for 60 seconds before curing, 4) air-dried with an air stream for 10 seconds before curing, and 5) air-dried with an air stream for 60 seconds before curing. FTIR/ATR spectra were obtained, and the DC was calculated by comparing the aliphatic bonds/reference peaks before and after light activation for 10 seconds (FlashLite 1401). The DC means of each material were analyzed by one-way analysis of variance and post hoc Tukey test (p<0.05). The DC of GO and Stae adhesive systems was not affected by the five evaporation conditions. Air-drying for 60 seconds before curing yielded the highest DC for SB, EO, and OC. Extended solvent volatilization time (60 seconds) either with or without air-drying before curing provided the highest DC for AM, NB, XP, and OUP. Thus, the monomer conversion of adhesive systems was material dependent. In general, the 60-second passive or active air-drying modes to volatilize solvents before curing enhanced the degree of conversion for the one-bottle simplified adhesive systems.</description><subject>Acetone</subject><subject>Air</subject><subject>Dentistry</subject><subject>Ethanol</subject><subject>Hardness</subject><subject>Light-Curing of Dental Adhesives</subject><subject>Polymerization</subject><subject>Resin Cements - chemistry</subject><subject>Solvents</subject><subject>Spectroscopy, Fourier Transform Infrared</subject><subject>Volatilization</subject><subject>Water</subject><issn>0361-7734</issn><issn>1559-2863</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2012</creationdate><recordtype>article</recordtype><sourceid>EIF</sourceid><recordid>eNpFkMtu1TAQhi0EoqcFqU9Qeckmrcdj57KsSrlIR-oG1pGdTMAoiVNPTsThKXhkfNQCm7l-_4z0C3EJ6lqjgRuAQpu62L8QO7C2KXRd4kuxU1hCUVVozsQ58w-ljDXWvhZnWiOgLuud-P2eviUiGQfZxXmjxCHOp47DtIxhCNSfFitNS0wuHaXrvxOHjSQfOU9ZOpZhHsYDzV1m_VHSz5XmPtcupMJ1a9jcmruY5OL4SRrHjeZVbnF0axjDrxzz1yn2xG_Eq8GNTG-f84X4-uH-y92nYv_w8fPd7b7oEKq16D0qMA2S153Dsi8Ra181zqO3JdaD9rU3Q2XAag81NsYrKK0inQUWesAL8e7p7pLi44F4bafAHY2jmykeuAUFWqtKN-o_2qXInGholxSmbEaG2pP_LUCb_W_3Gb16vnrwE_X_wL-G4x9BtYLT</recordid><startdate>201205</startdate><enddate>201205</enddate><creator>Borges, Boniek C D</creator><creator>Souza-Junior, Eduardo Jose</creator><creator>Brandt, William C</creator><creator>Loguercio, Alessandro D</creator><creator>Montes, Marcos A J R</creator><creator>Puppin-Rontani, Regina M</creator><creator>Sinhoreti, Mario Alexandre Coelho</creator><scope>CGR</scope><scope>CUY</scope><scope>CVF</scope><scope>ECM</scope><scope>EIF</scope><scope>NPM</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7X8</scope></search><sort><creationdate>201205</creationdate><title>Degree of conversion of simplified contemporary adhesive systems as influenced by extended air-activated or passive solvent volatilization modes</title><author>Borges, Boniek C D ; Souza-Junior, Eduardo Jose ; Brandt, William C ; Loguercio, Alessandro D ; Montes, Marcos A J R ; Puppin-Rontani, Regina M ; Sinhoreti, Mario Alexandre Coelho</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c317t-db301493eb2ca36d6338b79ab3b5638f2b8b4f74152b18394b01650e2eb251d13</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2012</creationdate><topic>Acetone</topic><topic>Air</topic><topic>Dentistry</topic><topic>Ethanol</topic><topic>Hardness</topic><topic>Light-Curing of Dental Adhesives</topic><topic>Polymerization</topic><topic>Resin Cements - chemistry</topic><topic>Solvents</topic><topic>Spectroscopy, Fourier Transform Infrared</topic><topic>Volatilization</topic><topic>Water</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Borges, Boniek C D</creatorcontrib><creatorcontrib>Souza-Junior, Eduardo Jose</creatorcontrib><creatorcontrib>Brandt, William C</creatorcontrib><creatorcontrib>Loguercio, Alessandro D</creatorcontrib><creatorcontrib>Montes, Marcos A J R</creatorcontrib><creatorcontrib>Puppin-Rontani, Regina M</creatorcontrib><creatorcontrib>Sinhoreti, Mario Alexandre Coelho</creatorcontrib><collection>Medline</collection><collection>MEDLINE</collection><collection>MEDLINE (Ovid)</collection><collection>MEDLINE</collection><collection>MEDLINE</collection><collection>PubMed</collection><collection>CrossRef</collection><collection>MEDLINE - Academic</collection><jtitle>Operative dentistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Borges, Boniek C D</au><au>Souza-Junior, Eduardo Jose</au><au>Brandt, William C</au><au>Loguercio, Alessandro D</au><au>Montes, Marcos A J R</au><au>Puppin-Rontani, Regina M</au><au>Sinhoreti, Mario Alexandre Coelho</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Degree of conversion of simplified contemporary adhesive systems as influenced by extended air-activated or passive solvent volatilization modes</atitle><jtitle>Operative dentistry</jtitle><addtitle>Oper Dent</addtitle><date>2012-05</date><risdate>2012</risdate><volume>37</volume><issue>3</issue><spage>246</spage><epage>252</epage><pages>246-252</pages><issn>0361-7734</issn><eissn>1559-2863</eissn><abstract>This study evaluated the effect of five methods of solvent volatilization on the degree of conversion (DC) of nine one-bottle adhesive systems using Fourier transform infrared/attenuated total reflectance (FTIR/ATR) analysis. Nine adhesives were tested: Adper Single Bond 2 (SB), Adper Easy One (EO), One Up Bond F Plus (OUP), One Coat Bond SL (OC), XP Bond (XP), Ambar (AM), Natural Bond (NB), GO, and Stae. The adhesive systems were applied to a zinc-selenide pellet and 1) cured without solvent volatilization, 2) left undisturbed for 10 seconds before curing, 3) left undisturbed for 60 seconds before curing, 4) air-dried with an air stream for 10 seconds before curing, and 5) air-dried with an air stream for 60 seconds before curing. FTIR/ATR spectra were obtained, and the DC was calculated by comparing the aliphatic bonds/reference peaks before and after light activation for 10 seconds (FlashLite 1401). The DC means of each material were analyzed by one-way analysis of variance and post hoc Tukey test (p<0.05). The DC of GO and Stae adhesive systems was not affected by the five evaporation conditions. Air-drying for 60 seconds before curing yielded the highest DC for SB, EO, and OC. Extended solvent volatilization time (60 seconds) either with or without air-drying before curing provided the highest DC for AM, NB, XP, and OUP. Thus, the monomer conversion of adhesive systems was material dependent. In general, the 60-second passive or active air-drying modes to volatilize solvents before curing enhanced the degree of conversion for the one-bottle simplified adhesive systems.</abstract><cop>United States</cop><pmid>22313268</pmid><doi>10.2341/11-248-L</doi><tpages>7</tpages><oa>free_for_read</oa></addata></record> |
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| source | MEDLINE; Allen Press Journals; EZB-FREE-00999 freely available EZB journals; Alma/SFX Local Collection |
| subjects | Acetone Air Dentistry Ethanol Hardness Light-Curing of Dental Adhesives Polymerization Resin Cements - chemistry Solvents Spectroscopy, Fourier Transform Infrared Volatilization Water |
| title | Degree of conversion of simplified contemporary adhesive systems as influenced by extended air-activated or passive solvent volatilization modes |
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