Controlled synthesis of monodisperse silver nanocubes via a solvothermal method
Silver nanostructures have been synthesized via a simple solvothermal method by adding sodium sulfide (Na 2 S) into the solution. The morphologies of products are controlled by the concentration of Ag 2 S formed in the initial stage. A low-concentration Ag 2 S (12.5 ~ 50 μM) acts as the catalysis, l...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2011-12, Vol.22 (12), p.1788-1795 |
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| container_issue | 12 |
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| container_title | Journal of materials science. Materials in electronics |
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| creator | Chen, Dapeng Zhu, Gang Zhu, Xingong Qiao, Xueliang Chen, Jianguo |
| description | Silver nanostructures have been synthesized via a simple solvothermal method by adding sodium sulfide (Na
2
S) into the solution. The morphologies of products are controlled by the concentration of Ag
2
S formed in the initial stage. A low-concentration Ag
2
S (12.5 ~ 50 μM) acts as the catalysis, leading to the formation of silver nanocubes with controllable sizes. However, a high-concentration Ag
2
S (100 μM) mainly acts as the controlling agent. It facilitates the synthesis of silver nanowires. Reaction conditions, the reaction temperature and the molar ratio of the repeating unit of PVP to AgNO
3
(R), have also been investigated. A possible mechanism is proposed to interpret the synthesis of silver nanocubes and nanowires. Finally, our results indicate that this strategy provides a simple route to prepare silver nanocubes with adjustable sizes. |
| doi_str_mv | 10.1007/s10854-011-0364-3 |
| format | Article |
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2
S) into the solution. The morphologies of products are controlled by the concentration of Ag
2
S formed in the initial stage. A low-concentration Ag
2
S (12.5 ~ 50 μM) acts as the catalysis, leading to the formation of silver nanocubes with controllable sizes. However, a high-concentration Ag
2
S (100 μM) mainly acts as the controlling agent. It facilitates the synthesis of silver nanowires. Reaction conditions, the reaction temperature and the molar ratio of the repeating unit of PVP to AgNO
3
(R), have also been investigated. A possible mechanism is proposed to interpret the synthesis of silver nanocubes and nanowires. Finally, our results indicate that this strategy provides a simple route to prepare silver nanocubes with adjustable sizes.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-011-0364-3</identifier><language>eng</language><publisher>Boston: Springer US</publisher><subject>Catalytic methods ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Condensed matter: structure, mechanical and thermal properties ; Cross-disciplinary physics: materials science; rheology ; Exact sciences and technology ; Low-dimensional structures (superlattices, quantum well structures, multilayers): structure, and nonelectronic properties ; Materials Science ; Methods of nanofabrication ; Nanoscale materials and structures: fabrication and characterization ; Optical and Electronic Materials ; Physics ; Quantum wires ; Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</subject><ispartof>Journal of materials science. Materials in electronics, 2011-12, Vol.22 (12), p.1788-1795</ispartof><rights>Springer Science+Business Media, LLC 2011</rights><rights>2015 INIST-CNRS</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c345t-3a88cdc53623ef7f497a490acc96eab4c89d8b29b7dee93f488d3c66393d3d773</citedby><cites>FETCH-LOGICAL-c345t-3a88cdc53623ef7f497a490acc96eab4c89d8b29b7dee93f488d3c66393d3d773</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-011-0364-3$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-011-0364-3$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids><backlink>$$Uhttp://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=25233058$$DView record in Pascal Francis$$Hfree_for_read</backlink></links><search><creatorcontrib>Chen, Dapeng</creatorcontrib><creatorcontrib>Zhu, Gang</creatorcontrib><creatorcontrib>Zhu, Xingong</creatorcontrib><creatorcontrib>Qiao, Xueliang</creatorcontrib><creatorcontrib>Chen, Jianguo</creatorcontrib><title>Controlled synthesis of monodisperse silver nanocubes via a solvothermal method</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>Silver nanostructures have been synthesized via a simple solvothermal method by adding sodium sulfide (Na
2
S) into the solution. The morphologies of products are controlled by the concentration of Ag
2
S formed in the initial stage. A low-concentration Ag
2
S (12.5 ~ 50 μM) acts as the catalysis, leading to the formation of silver nanocubes with controllable sizes. However, a high-concentration Ag
2
S (100 μM) mainly acts as the controlling agent. It facilitates the synthesis of silver nanowires. Reaction conditions, the reaction temperature and the molar ratio of the repeating unit of PVP to AgNO
3
(R), have also been investigated. A possible mechanism is proposed to interpret the synthesis of silver nanocubes and nanowires. Finally, our results indicate that this strategy provides a simple route to prepare silver nanocubes with adjustable sizes.</description><subject>Catalytic methods</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Condensed matter: structure, mechanical and thermal properties</subject><subject>Cross-disciplinary physics: materials science; rheology</subject><subject>Exact sciences and technology</subject><subject>Low-dimensional structures (superlattices, quantum well structures, multilayers): structure, and nonelectronic properties</subject><subject>Materials Science</subject><subject>Methods of nanofabrication</subject><subject>Nanoscale materials and structures: fabrication and characterization</subject><subject>Optical and Electronic Materials</subject><subject>Physics</subject><subject>Quantum wires</subject><subject>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2011</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kE1LxDAQhoMouK7-AG9B8FhNOmmaHGXxCxb2ouAtpEnqdmmbNdNd8N_bpYuePM1hnved4SHkmrM7zlh5j5ypQmSM84yBFBmckBkvSsiEyj9OyYzposxEkefn5AJxwxiTAtSMrBaxH1Js2-ApfvfDOmCDNNa0i330DW5DwkCxafch0d720e2qgHTfWGopxnYfx0jqbEu7MKyjvyRntW0xXB3nnLw_Pb4tXrLl6vl18bDMHIhiyMAq5bwrQOYQ6rIWurRCM-uclsFWwintVZXrqvQhaKiFUh6clKDBgy9LmJObqXeb4tcu4GA2cZf68aTRjCvBpZYjxCfIpYiYQm22qels-jacmYM2M2kzozZz0GZgzNweiy0629bJ9q7B32Be5ACsUCOXTxyOq_4zpL8H_i__AaZZfh8</recordid><startdate>20111201</startdate><enddate>20111201</enddate><creator>Chen, Dapeng</creator><creator>Zhu, Gang</creator><creator>Zhu, Xingong</creator><creator>Qiao, Xueliang</creator><creator>Chen, Jianguo</creator><general>Springer US</general><general>Springer</general><general>Springer Nature B.V</general><scope>IQODW</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>F28</scope><scope>FR3</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>L7M</scope><scope>P5Z</scope><scope>P62</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><scope>S0W</scope></search><sort><creationdate>20111201</creationdate><title>Controlled synthesis of monodisperse silver nanocubes via a solvothermal method</title><author>Chen, Dapeng ; Zhu, Gang ; Zhu, Xingong ; Qiao, Xueliang ; Chen, Jianguo</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c345t-3a88cdc53623ef7f497a490acc96eab4c89d8b29b7dee93f488d3c66393d3d773</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2011</creationdate><topic>Catalytic methods</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Condensed matter: structure, mechanical and thermal properties</topic><topic>Cross-disciplinary physics: materials science; rheology</topic><topic>Exact sciences and technology</topic><topic>Low-dimensional structures (superlattices, quantum well structures, multilayers): structure, and nonelectronic properties</topic><topic>Materials Science</topic><topic>Methods of nanofabrication</topic><topic>Nanoscale materials and structures: fabrication and characterization</topic><topic>Optical and Electronic Materials</topic><topic>Physics</topic><topic>Quantum wires</topic><topic>Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties)</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Chen, Dapeng</creatorcontrib><creatorcontrib>Zhu, Gang</creatorcontrib><creatorcontrib>Zhu, Xingong</creatorcontrib><creatorcontrib>Qiao, Xueliang</creatorcontrib><creatorcontrib>Chen, Jianguo</creatorcontrib><collection>Pascal-Francis</collection><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Advanced Technologies Database with Aerospace</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><collection>DELNET Engineering & Technology Collection</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Chen, Dapeng</au><au>Zhu, Gang</au><au>Zhu, Xingong</au><au>Qiao, Xueliang</au><au>Chen, Jianguo</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Controlled synthesis of monodisperse silver nanocubes via a solvothermal method</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2011-12-01</date><risdate>2011</risdate><volume>22</volume><issue>12</issue><spage>1788</spage><epage>1795</epage><pages>1788-1795</pages><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>Silver nanostructures have been synthesized via a simple solvothermal method by adding sodium sulfide (Na
2
S) into the solution. The morphologies of products are controlled by the concentration of Ag
2
S formed in the initial stage. A low-concentration Ag
2
S (12.5 ~ 50 μM) acts as the catalysis, leading to the formation of silver nanocubes with controllable sizes. However, a high-concentration Ag
2
S (100 μM) mainly acts as the controlling agent. It facilitates the synthesis of silver nanowires. Reaction conditions, the reaction temperature and the molar ratio of the repeating unit of PVP to AgNO
3
(R), have also been investigated. A possible mechanism is proposed to interpret the synthesis of silver nanocubes and nanowires. Finally, our results indicate that this strategy provides a simple route to prepare silver nanocubes with adjustable sizes.</abstract><cop>Boston</cop><pub>Springer US</pub><doi>10.1007/s10854-011-0364-3</doi><tpages>8</tpages></addata></record> |
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| subjects | Catalytic methods Characterization and Evaluation of Materials Chemistry and Materials Science Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science rheology Exact sciences and technology Low-dimensional structures (superlattices, quantum well structures, multilayers): structure, and nonelectronic properties Materials Science Methods of nanofabrication Nanoscale materials and structures: fabrication and characterization Optical and Electronic Materials Physics Quantum wires Surfaces and interfaces thin films and whiskers (structure and nonelectronic properties) |
| title | Controlled synthesis of monodisperse silver nanocubes via a solvothermal method |
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