Preparation and characterization of Ag-added Bi1.84Pb0.4Sr2Ca2.2Cu3O10+x bulk tube conductors for cryogen free superconducting magnet

Bulk tube conductors of Bi1.84Pb0.4Sr2Ca2.2Cu3O10+xwith addition of silver varying from 0 to 25 wt% (not reported earlier) were systematically studied using X-ray diffraction (XRD), scanning electron microscopy (SEM), electrical transport and a.c. susceptibility techniques. The tube conductors forme...

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Veröffentlicht in:Bulletin of materials science 2001-01, Vol.24 (6), p.603-609
Hauptverfasser: Ekbote, S. N., Padam, G. K., Sharma, M., Arora, N. K., Khurana, B. S., Goel, R. C., Suri, D. K., Mehra, N., Das, B. K.
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container_end_page 609
container_issue 6
container_start_page 603
container_title Bulletin of materials science
container_volume 24
creator Ekbote, S. N.
Padam, G. K.
Sharma, M.
Arora, N. K.
Khurana, B. S.
Goel, R. C.
Suri, D. K.
Mehra, N.
Das, B. K.
description Bulk tube conductors of Bi1.84Pb0.4Sr2Ca2.2Cu3O10+xwith addition of silver varying from 0 to 25 wt% (not reported earlier) were systematically studied using X-ray diffraction (XRD), scanning electron microscopy (SEM), electrical transport and a.c. susceptibility techniques. The tube conductors formed by cold isostatic pressing (CIP) of the powders obtained from spray drying method have been made successfully. It was found that Ag addition has not only affected the formation of the desired Bi-2223 phase and the microstructure of these large bulk tube samples thereby influencing on the critical current (Ic),it also reduces the contact resistance to minimize the cryogen losses. These variations have been found to be Ag content dependent. An optimized value of 10 wt% Ag has been found to produce the best quality tubes showing reproducibleIcvalue > 120 Amp at 77 K which is in general a requirement to energies of the cryogen free conventional/HTSC superconducting magnets below 20 K.
doi_str_mv 10.1007/BF02704008
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subjects Bismuth strontium calcium copper oxide
Cold isostatic pressing
Cold pressing
Conductors
Contact resistance
Critical current (superconductivity)
Electric contacts
Scanning electron microscopy
Silver
Spray drying
Superconducting magnets
Superconductivity
Tubes
title Preparation and characterization of Ag-added Bi1.84Pb0.4Sr2Ca2.2Cu3O10+x bulk tube conductors for cryogen free superconducting magnet
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