Diamine complexes of nickel(II) nitrate: X-ray single crystal structural analysis of trans-[NiL2(NO3)2] [L = 1-(2-aminoethyl)piperidine]

Diamine complexes of nickel(II) nitrate: X-ray single crystal structural analysis of trans-[NiL2(NO3)2] [L = 1-(2-aminoethyl)piperidine]

Trans-[NiL^sub 2^(H^sub 2^O)^sub 2^](NO^sub 3^)^sub 2^ (pale blue) (1), trans-[NiL^sub 2^(NO^sub 3^)^sub 2^] (dark blue) (2), [L = 1-(2-aminoethyl)piperidine] and trans-[NiL^sub 2^^sup '^(H^sub 2^O)^sub 2^](NO^sub 3^)^sub 2^ (blue) (3) [L = 1-(2-aminoethyl)pyrrolidine] have been prepared. Compl...

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Veröffentlicht in:Transition metal chemistry (Weinheim) 2001-08, Vol.26 (4-5), p.594
Hauptverfasser: Laskar, Inamur R, Das, Debasis, Wong, Wing-tak, Chaudhuri, N Ray
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container_title Transition metal chemistry (Weinheim)
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creator Laskar, Inamur R
Das, Debasis
Wong, Wing-tak
Chaudhuri, N Ray
description Trans-[NiL^sub 2^(H^sub 2^O)^sub 2^](NO^sub 3^)^sub 2^ (pale blue) (1), trans-[NiL^sub 2^(NO^sub 3^)^sub 2^] (dark blue) (2), [L = 1-(2-aminoethyl)piperidine] and trans-[NiL^sub 2^^sup '^(H^sub 2^O)^sub 2^](NO^sub 3^)^sub 2^ (blue) (3) [L = 1-(2-aminoethyl)pyrrolidine] have been prepared. Complexes (1) and (3) upon heating undergo deaquation-anation yielding trans-[NiL^sub 2^(NO^sub 3^)^sub 2^] (dark blue) (2) and cis-[NiL^sub 2^'(NO^sub 3^)](NO^sub 3^) (blue) (3a), respectively. The X-ray single crystal structure of complex (2) has been determined.[PUBLICATION ABSTRACT]
doi_str_mv 10.1023/A:1011003029546
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Complexes (1) and (3) upon heating undergo deaquation-anation yielding trans-[NiL^sub 2^(NO^sub 3^)^sub 2^] (dark blue) (2) and cis-[NiL^sub 2^'(NO^sub 3^)](NO^sub 3^) (blue) (3a), respectively. 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title Diamine complexes of nickel(II) nitrate: X-ray single crystal structural analysis of trans-[NiL2(NO3)2] [L = 1-(2-aminoethyl)piperidine]
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