Kinetic Study of the Crystallization of Free and Contact Surfaces of Fe77Ni1Si9B13 Amorphous-Alloy Ribbons under Low-Temperature Annealing
This study examines the differences in the crystallization kinetics of the free and contact sides of an Fe 77 Ni 1 Si 9 B 13 amorphous-alloy ribbon at 400°C. X-ray phase analysis reveals that crystals based on α-Fe form on the contact side after just 5 min of annealing. In contrast, on the free side...
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| Veröffentlicht in: | Surface investigation, x-ray, synchrotron and neutron techniques x-ray, synchrotron and neutron techniques, 2024-10, Vol.18 (5), p.1249-1254 |
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| container_title | Surface investigation, x-ray, synchrotron and neutron techniques |
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| creator | Konovalov, M. S. Lad’yanov, V. I. Mokrushina, M. I. Suslov, A. A. Shilyaev, A. I. Tereshkina, S. A. Ivanov, V. B. |
| description | This study examines the differences in the crystallization kinetics of the free and contact sides of an Fe
77
Ni
1
Si
9
B
13
amorphous-alloy ribbon at 400°C. X-ray phase analysis reveals that crystals based on α-Fe form on the contact side after just 5 min of annealing. In contrast, on the free side, reflections corresponding to α-Fe crystals are only detectable after 30 min of annealing. The relative content of the crystalline phase is determined using X-ray diffraction data, based on the relationship between the integral intensity of the reflection of the analyzed phase and its volume fraction. We explore the possible reasons for the observed differences in crystallization. Crystallization in the surface layers of both the contact and free sides of the ribbon occurs in two stages: the isotropic growth of existing nuclei with a decreasing rate of crystal formation, followed by the slowed anisotropic growth of already formed crystals. The first stage is satisfactorily described by the Johnson–Mehl–Avrami–Kolmogorov (JMAK) thermodynamic formalism, whereas applying a kinetic equation to describe the second stage is not appropriate. |
| doi_str_mv | 10.1134/S102745102470109X |
| format | Article |
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77
Ni
1
Si
9
B
13
amorphous-alloy ribbon at 400°C. X-ray phase analysis reveals that crystals based on α-Fe form on the contact side after just 5 min of annealing. In contrast, on the free side, reflections corresponding to α-Fe crystals are only detectable after 30 min of annealing. The relative content of the crystalline phase is determined using X-ray diffraction data, based on the relationship between the integral intensity of the reflection of the analyzed phase and its volume fraction. We explore the possible reasons for the observed differences in crystallization. Crystallization in the surface layers of both the contact and free sides of the ribbon occurs in two stages: the isotropic growth of existing nuclei with a decreasing rate of crystal formation, followed by the slowed anisotropic growth of already formed crystals. The first stage is satisfactorily described by the Johnson–Mehl–Avrami–Kolmogorov (JMAK) thermodynamic formalism, whereas applying a kinetic equation to describe the second stage is not appropriate.</description><identifier>ISSN: 1027-4510</identifier><identifier>EISSN: 1819-7094</identifier><identifier>DOI: 10.1134/S102745102470109X</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Alpha iron ; Amorphous alloys ; Annealing ; Chemistry and Materials Science ; Crystal growth ; Crystallization ; Crystals ; Kinetic equations ; Low temperature ; Materials Science ; Surface layers ; Surfaces and Interfaces ; Thin Films ; X ray reflection</subject><ispartof>Surface investigation, x-ray, synchrotron and neutron techniques, 2024-10, Vol.18 (5), p.1249-1254</ispartof><rights>Pleiades Publishing, Ltd. 2024 ISSN 1027-4510, Journal of Surface Investigation: X-ray, Synchrotron and Neutron Techniques, 2024, Vol. 18, No. 5, pp. 1249–1254. © Pleiades Publishing, Ltd., 2024.</rights><rights>Copyright Springer Nature B.V. 2024</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c1494-a549b0b3920f0fe2c4a4a86c57b11c1e7630e9daaab19fcb7db06720a53da6263</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S102745102470109X$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S102745102470109X$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27923,27924,41487,42556,51318</link.rule.ids></links><search><creatorcontrib>Konovalov, M. S.</creatorcontrib><creatorcontrib>Lad’yanov, V. I.</creatorcontrib><creatorcontrib>Mokrushina, M. I.</creatorcontrib><creatorcontrib>Suslov, A. A.</creatorcontrib><creatorcontrib>Shilyaev, A. I.</creatorcontrib><creatorcontrib>Tereshkina, S. A.</creatorcontrib><creatorcontrib>Ivanov, V. B.</creatorcontrib><title>Kinetic Study of the Crystallization of Free and Contact Surfaces of Fe77Ni1Si9B13 Amorphous-Alloy Ribbons under Low-Temperature Annealing</title><title>Surface investigation, x-ray, synchrotron and neutron techniques</title><addtitle>J. Surf. Investig</addtitle><description>This study examines the differences in the crystallization kinetics of the free and contact sides of an Fe
77
Ni
1
Si
9
B
13
amorphous-alloy ribbon at 400°C. X-ray phase analysis reveals that crystals based on α-Fe form on the contact side after just 5 min of annealing. In contrast, on the free side, reflections corresponding to α-Fe crystals are only detectable after 30 min of annealing. The relative content of the crystalline phase is determined using X-ray diffraction data, based on the relationship between the integral intensity of the reflection of the analyzed phase and its volume fraction. We explore the possible reasons for the observed differences in crystallization. Crystallization in the surface layers of both the contact and free sides of the ribbon occurs in two stages: the isotropic growth of existing nuclei with a decreasing rate of crystal formation, followed by the slowed anisotropic growth of already formed crystals. The first stage is satisfactorily described by the Johnson–Mehl–Avrami–Kolmogorov (JMAK) thermodynamic formalism, whereas applying a kinetic equation to describe the second stage is not appropriate.</description><subject>Alpha iron</subject><subject>Amorphous alloys</subject><subject>Annealing</subject><subject>Chemistry and Materials Science</subject><subject>Crystal growth</subject><subject>Crystallization</subject><subject>Crystals</subject><subject>Kinetic equations</subject><subject>Low temperature</subject><subject>Materials Science</subject><subject>Surface layers</subject><subject>Surfaces and Interfaces</subject><subject>Thin Films</subject><subject>X ray reflection</subject><issn>1027-4510</issn><issn>1819-7094</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp1UM1KxDAQLqKgrj6At4DnaqZNm81xXfzDRcFV8Fam6VQj3WRNUmR9BJ_arit4EC8zw3x_8CXJEfATgFyczoFnUhTDFJIDV09byR6MQaWSK7E93AOcrvHdZD-EV84LmRflXvJ5YyxFo9k89s2KuZbFF2JTvwoRu858YDTOrt8XnoihbdjU2Yg6snnvW9QUvkGS8tbA3KgzyNlk4fzyxfUhnXSdW7F7U9fOBtbbhjybuff0gRZL8hh7T2xiLWFn7PNBstNiF-jwZ4-Sx4vzh-lVOru7vJ5OZqkGoUSKhVA1r3OV8Za3lGmBAselLmQNoIFkmXNSDSLWoFpdy6bmpcw4FnmDZVbmo-R447v07q2nEKtX13s7RFY5DO3JMZRqYMGGpb0LwVNbLb1ZoF9VwKt15dWfygdNttGEgWufyf86_y_6Ap9Tg2g</recordid><startdate>20241001</startdate><enddate>20241001</enddate><creator>Konovalov, M. S.</creator><creator>Lad’yanov, V. I.</creator><creator>Mokrushina, M. I.</creator><creator>Suslov, A. A.</creator><creator>Shilyaev, A. I.</creator><creator>Tereshkina, S. A.</creator><creator>Ivanov, V. B.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope></search><sort><creationdate>20241001</creationdate><title>Kinetic Study of the Crystallization of Free and Contact Surfaces of Fe77Ni1Si9B13 Amorphous-Alloy Ribbons under Low-Temperature Annealing</title><author>Konovalov, M. S. ; Lad’yanov, V. I. ; Mokrushina, M. I. ; Suslov, A. A. ; Shilyaev, A. I. ; Tereshkina, S. A. ; Ivanov, V. B.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c1494-a549b0b3920f0fe2c4a4a86c57b11c1e7630e9daaab19fcb7db06720a53da6263</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Alpha iron</topic><topic>Amorphous alloys</topic><topic>Annealing</topic><topic>Chemistry and Materials Science</topic><topic>Crystal growth</topic><topic>Crystallization</topic><topic>Crystals</topic><topic>Kinetic equations</topic><topic>Low temperature</topic><topic>Materials Science</topic><topic>Surface layers</topic><topic>Surfaces and Interfaces</topic><topic>Thin Films</topic><topic>X ray reflection</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Konovalov, M. S.</creatorcontrib><creatorcontrib>Lad’yanov, V. I.</creatorcontrib><creatorcontrib>Mokrushina, M. I.</creatorcontrib><creatorcontrib>Suslov, A. A.</creatorcontrib><creatorcontrib>Shilyaev, A. I.</creatorcontrib><creatorcontrib>Tereshkina, S. A.</creatorcontrib><creatorcontrib>Ivanov, V. B.</creatorcontrib><collection>CrossRef</collection><jtitle>Surface investigation, x-ray, synchrotron and neutron techniques</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Konovalov, M. S.</au><au>Lad’yanov, V. I.</au><au>Mokrushina, M. I.</au><au>Suslov, A. A.</au><au>Shilyaev, A. I.</au><au>Tereshkina, S. A.</au><au>Ivanov, V. B.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Kinetic Study of the Crystallization of Free and Contact Surfaces of Fe77Ni1Si9B13 Amorphous-Alloy Ribbons under Low-Temperature Annealing</atitle><jtitle>Surface investigation, x-ray, synchrotron and neutron techniques</jtitle><stitle>J. Surf. Investig</stitle><date>2024-10-01</date><risdate>2024</risdate><volume>18</volume><issue>5</issue><spage>1249</spage><epage>1254</epage><pages>1249-1254</pages><issn>1027-4510</issn><eissn>1819-7094</eissn><abstract>This study examines the differences in the crystallization kinetics of the free and contact sides of an Fe
77
Ni
1
Si
9
B
13
amorphous-alloy ribbon at 400°C. X-ray phase analysis reveals that crystals based on α-Fe form on the contact side after just 5 min of annealing. In contrast, on the free side, reflections corresponding to α-Fe crystals are only detectable after 30 min of annealing. The relative content of the crystalline phase is determined using X-ray diffraction data, based on the relationship between the integral intensity of the reflection of the analyzed phase and its volume fraction. We explore the possible reasons for the observed differences in crystallization. Crystallization in the surface layers of both the contact and free sides of the ribbon occurs in two stages: the isotropic growth of existing nuclei with a decreasing rate of crystal formation, followed by the slowed anisotropic growth of already formed crystals. The first stage is satisfactorily described by the Johnson–Mehl–Avrami–Kolmogorov (JMAK) thermodynamic formalism, whereas applying a kinetic equation to describe the second stage is not appropriate.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S102745102470109X</doi><tpages>6</tpages></addata></record> |
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| subjects | Alpha iron Amorphous alloys Annealing Chemistry and Materials Science Crystal growth Crystallization Crystals Kinetic equations Low temperature Materials Science Surface layers Surfaces and Interfaces Thin Films X ray reflection |
| title | Kinetic Study of the Crystallization of Free and Contact Surfaces of Fe77Ni1Si9B13 Amorphous-Alloy Ribbons under Low-Temperature Annealing |
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