Developing a Millifluidic Flow Analysis System for Asphaltene Content Reduction in Crude Oil via Liquid-Liquid Extraction with Variable Parameters

Solvent deasphalting (SDA) of the actual heavy crude oil is one of the most critical processes in the petroleum industry, which improves the specifications of low-quality crude oil. The work shows heavy crude oil with an asphaltene content of 2.49 wt % taken from the Samawah oil refinery in southern...

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Veröffentlicht in:Petroleum chemistry 2024, Vol.64 (8), p.1055-1062
Hauptverfasser: Hadi, Ahmed A., Ali, Ali A., Dakhil, Ihsan H., Khathi, Mohammed T., Khudair, Zainab J., Razzaq, Ali S., Hameed, Abdullah T., Al-Rudaini, Khudhair A.
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container_end_page 1062
container_issue 8
container_start_page 1055
container_title Petroleum chemistry
container_volume 64
creator Hadi, Ahmed A.
Ali, Ali A.
Dakhil, Ihsan H.
Khathi, Mohammed T.
Khudair, Zainab J.
Razzaq, Ali S.
Hameed, Abdullah T.
Al-Rudaini, Khudhair A.
description Solvent deasphalting (SDA) of the actual heavy crude oil is one of the most critical processes in the petroleum industry, which improves the specifications of low-quality crude oil. The work shows heavy crude oil with an asphaltene content of 2.49 wt % taken from the Samawah oil refinery in southern Iraq was deasphalted using a homemade flow system with several variables. The significant variables impacting the deasphalting process were identified using the central composite design (CCD) and response surface method (RSM). The optimum conditions of the deasphalting process are n -heptane solvent, a flow rate of 31 mL/min, a mixing coil length of 172 cm, a temperature of 32°C, and a time of 3 s. It was determined that the impact of using variables occurs in the following order: mixing coil length > temperature > solvent flow rate > time in n -heptane solvent. The experimental and theoretical efficiencies of the deasphalting technique for heavy crude oil were found to be 57.94 and 56.26%, respectively.
doi_str_mv 10.1134/S0965544124070120
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subjects Asphaltenes
Chemistry
Chemistry and Materials Science
Coils
Crude oil
Flow velocity
Heavy petroleum
Heptanes
Industrial Chemistry/Chemical Engineering
Industrial development
Liquid-liquid extraction
Parameter identification
Refineries
Response surface methodology
Solvents
Variables
title Developing a Millifluidic Flow Analysis System for Asphaltene Content Reduction in Crude Oil via Liquid-Liquid Extraction with Variable Parameters
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