The Analysis of the ZnO/Por-Si Hierarchical Surface by Studying Fractal Properties with High Accuracy and the Behavior of the EPR Spectra Components in the Ordering of Structure
A hierarchical surface that includes objects with different sizes, as a result of creating local fields, initiates a large number of effects. Micropores in the composition of macropores, as well as nanoclusters of the substance, were detected by scanning electron and atomic force microscopies on the...
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| Veröffentlicht in: | Processes 2024-11, Vol.12 (11), p.2541 |
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| creator | Seredavina, Tatyana Zhapakov, Rashid Murzalinov, Danatbek Spivak, Yulia Ussipov, Nurzhan Chepushtanova, Tatyana Bolysbay, Aslan Mamyrbayeva, Kulzira Merkibayev, Yerik Moshnikov, Vyacheslav Altmyshbayeva, Aliya Tulegenov, Azamat |
| description | A hierarchical surface that includes objects with different sizes, as a result of creating local fields, initiates a large number of effects. Micropores in the composition of macropores, as well as nanoclusters of the substance, were detected by scanning electron and atomic force microscopies on the surface of ZnO/Por-Si samples. An identical fractal dimension for all levels of the hierarchy was determined for these structures, which is associated with the same response to external excitation. Photoluminescence studies have shown the presence of localized levels in the band gap, with the probability of capturing both electrons and holes, which ensures charge transitions between energy bands. Decomposition of the electron paramagnetic resonance (EPR) signal into components made it possible to determine the manifestations of various types of interaction between paramagnetic particles, including the hyperfine structure of the spectrum. The ordering of the structure of the substance as a result of sequential annealing in the range from 300 to 500 °C was revealed in the EPR spectrum. This fact, as well as photo- and gas sensitivity for all types of samples studied, confirms the prospects of using these structures as sensors. |
| doi_str_mv | 10.3390/pr12112541 |
| format | Article |
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Micropores in the composition of macropores, as well as nanoclusters of the substance, were detected by scanning electron and atomic force microscopies on the surface of ZnO/Por-Si samples. An identical fractal dimension for all levels of the hierarchy was determined for these structures, which is associated with the same response to external excitation. Photoluminescence studies have shown the presence of localized levels in the band gap, with the probability of capturing both electrons and holes, which ensures charge transitions between energy bands. Decomposition of the electron paramagnetic resonance (EPR) signal into components made it possible to determine the manifestations of various types of interaction between paramagnetic particles, including the hyperfine structure of the spectrum. The ordering of the structure of the substance as a result of sequential annealing in the range from 300 to 500 °C was revealed in the EPR spectrum. This fact, as well as photo- and gas sensitivity for all types of samples studied, confirms the prospects of using these structures as sensors.</description><identifier>ISSN: 2227-9717</identifier><identifier>EISSN: 2227-9717</identifier><identifier>DOI: 10.3390/pr12112541</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Atomic force microscopy ; Atomic properties ; Banded structure ; Composition effects ; Electron paramagnetic resonance ; Electron spin resonance ; Electrons ; Energy bands ; Energy charge ; Fractal analysis ; Fractal geometry ; Hierarchies ; Hyperfine structure ; Nanoclusters ; Neural networks ; Photoluminescence ; Photons ; Sensors ; Zinc oxide ; Zinc oxides</subject><ispartof>Processes, 2024-11, Vol.12 (11), p.2541</ispartof><rights>COPYRIGHT 2024 MDPI AG</rights><rights>2024 by the authors. Licensee MDPI, Basel, Switzerland. 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This fact, as well as photo- and gas sensitivity for all types of samples studied, confirms the prospects of using these structures as sensors.</description><subject>Atomic force microscopy</subject><subject>Atomic properties</subject><subject>Banded structure</subject><subject>Composition effects</subject><subject>Electron paramagnetic resonance</subject><subject>Electron spin resonance</subject><subject>Electrons</subject><subject>Energy bands</subject><subject>Energy charge</subject><subject>Fractal analysis</subject><subject>Fractal geometry</subject><subject>Hierarchies</subject><subject>Hyperfine structure</subject><subject>Nanoclusters</subject><subject>Neural networks</subject><subject>Photoluminescence</subject><subject>Photons</subject><subject>Sensors</subject><subject>Zinc oxide</subject><subject>Zinc oxides</subject><issn>2227-9717</issn><issn>2227-9717</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNpNUc1u1DAQjhBIVKUXnsASN6S0_kni7HFZtRSp0q5IuXCJnMl442o3DmOnKI_FG-LtgsA-eDzfz2hmsuy94NdKrfjNREIKIctCvMoupJQ6X2mhX_8Xv82uQnji6ayEqsvqIvv1OCBbj-awBBeYtyym__dxe7PzlDeO3TskQzA4MAfWzGQNIOsW1sS5X9y4Z3dkICZsR35Cig4D--nikIT7ga0B5oQvzIz9i_MnHMyz8_S30u3uK2smhEiGbfxx8iOOMTA3vqBb6pFORRK7iTRDnAnfZW-sOQS8-vNeZt_ubh839_nD9vOXzfohB1HrmMuaW8mNqqrOmN5UEqS2wHUtRKk71Yuu41CgFFCB1rwsbKdBoVUCQXaSq8vsw9l3Iv9jxhDbJz9TmlRolVCqLErBT6zrM2tvDti60frUCqTb49FBase6lF_Xoi6qUvJVEnw8C4B8CIS2ncgdDS2t4O1pje2_NarfIbqQiQ</recordid><startdate>20241101</startdate><enddate>20241101</enddate><creator>Seredavina, Tatyana</creator><creator>Zhapakov, Rashid</creator><creator>Murzalinov, Danatbek</creator><creator>Spivak, Yulia</creator><creator>Ussipov, Nurzhan</creator><creator>Chepushtanova, Tatyana</creator><creator>Bolysbay, Aslan</creator><creator>Mamyrbayeva, Kulzira</creator><creator>Merkibayev, Yerik</creator><creator>Moshnikov, Vyacheslav</creator><creator>Altmyshbayeva, Aliya</creator><creator>Tulegenov, Azamat</creator><general>MDPI AG</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FH</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BBNVY</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>LK8</scope><scope>M7P</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><orcidid>https://orcid.org/0000-0002-6194-3518</orcidid><orcidid>https://orcid.org/0000-0002-2512-3280</orcidid><orcidid>https://orcid.org/0000-0002-6526-0044</orcidid><orcidid>https://orcid.org/0000-0002-5852-999X</orcidid><orcidid>https://orcid.org/0000-0001-6500-5492</orcidid><orcidid>https://orcid.org/0000-0002-2570-8190</orcidid><orcidid>https://orcid.org/0000-0001-6519-1969</orcidid><orcidid>https://orcid.org/0009-0007-5171-8767</orcidid><orcidid>https://orcid.org/0000-0002-4483-4635</orcidid><orcidid>https://orcid.org/0000-0001-9689-160X</orcidid></search><sort><creationdate>20241101</creationdate><title>The Analysis of the ZnO/Por-Si Hierarchical Surface by Studying Fractal Properties with High Accuracy and the Behavior of the EPR Spectra Components in the Ordering of Structure</title><author>Seredavina, Tatyana ; 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Micropores in the composition of macropores, as well as nanoclusters of the substance, were detected by scanning electron and atomic force microscopies on the surface of ZnO/Por-Si samples. An identical fractal dimension for all levels of the hierarchy was determined for these structures, which is associated with the same response to external excitation. Photoluminescence studies have shown the presence of localized levels in the band gap, with the probability of capturing both electrons and holes, which ensures charge transitions between energy bands. Decomposition of the electron paramagnetic resonance (EPR) signal into components made it possible to determine the manifestations of various types of interaction between paramagnetic particles, including the hyperfine structure of the spectrum. The ordering of the structure of the substance as a result of sequential annealing in the range from 300 to 500 °C was revealed in the EPR spectrum. 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| subjects | Atomic force microscopy Atomic properties Banded structure Composition effects Electron paramagnetic resonance Electron spin resonance Electrons Energy bands Energy charge Fractal analysis Fractal geometry Hierarchies Hyperfine structure Nanoclusters Neural networks Photoluminescence Photons Sensors Zinc oxide Zinc oxides |
| title | The Analysis of the ZnO/Por-Si Hierarchical Surface by Studying Fractal Properties with High Accuracy and the Behavior of the EPR Spectra Components in the Ordering of Structure |
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