Photocatalytic Degradation of Four Organic Dyes Present in Water Using ZnO Nanoparticles Synthesized with Green Synthesis Using Ambrosia ambrosioides Leaf and Root Extract
Currently, several organic dyes found in wastewater cause severe contamination problems for flora, fauna, and people in direct contact with them. This research proposes an alternative for the degradation of polluting dyes using ZnO nanoparticles (NPs) synthesized by an ecological route using leaf an...
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creator | Medina-Acosta, Martin Chinchillas-Chinchillas, Manuel J. Garrafa-Gálvez, Horacio E. Garcia-Maro, Caree A. Rosas-Casarez, Carlos A. Lugo-Medina, Eder Luque-Morales, Priscy A. Soto-Robles, Carlos A. |
description | Currently, several organic dyes found in wastewater cause severe contamination problems for flora, fauna, and people in direct contact with them. This research proposes an alternative for the degradation of polluting dyes using ZnO nanoparticles (NPs) synthesized by an ecological route using leaf and root extracts of Ambrosia ambrosioides as a reducing agent (with a weight/volume ratio = 4%). Scanning Electron Microscopy (SEM) was used to determine the morphology, showing an agglomeration of cluster-shaped NPs. Using Transmission Electron Microscopy (TEM), different sizes of NPs ranging from 5 to 56 nm were observed for both synthesized NPs. The composition and structure of the nanomaterial were analyzed by infrared spectroscopy (FT-IR) and X-ray diffraction (XRD), showing as a result that the NPs have a wurtzite-like crystalline structure with crystallite sizes around 32–37 nm for both samples. Additionally, the bandgap of the NPs was calculated using Ultraviolet Visible Spectroscopy (UV–Vis), determining values of 2.82 and 2.70 eV for the NPs synthesized with leaf and root, respectively. Finally, thermogravimetric analysis demonstrated that the nanoparticles contained an organic part after the green synthesis process, with high thermal stability for both samples. Photocatalytic analysis showed that these nanomaterials can degrade four dyes under UV irradiation, reaching 90% degradation for methylene blue (MB), methyl orange (MO) and Congo red (CR) at 60, 100 and 60 min, respectively, while for methyl red (MR) almost 90% degradation was achieved at 140 min of UV irradiation. These results demonstrate that it is effective to use Ambrosia ambrosioides root and leaf extracts as a reducing agent for the formation of ZnO NPs, also evidencing their favorable application in the photocatalytic degradation of these four organic dyes. |
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This research proposes an alternative for the degradation of polluting dyes using ZnO nanoparticles (NPs) synthesized by an ecological route using leaf and root extracts of Ambrosia ambrosioides as a reducing agent (with a weight/volume ratio = 4%). Scanning Electron Microscopy (SEM) was used to determine the morphology, showing an agglomeration of cluster-shaped NPs. Using Transmission Electron Microscopy (TEM), different sizes of NPs ranging from 5 to 56 nm were observed for both synthesized NPs. The composition and structure of the nanomaterial were analyzed by infrared spectroscopy (FT-IR) and X-ray diffraction (XRD), showing as a result that the NPs have a wurtzite-like crystalline structure with crystallite sizes around 32–37 nm for both samples. Additionally, the bandgap of the NPs was calculated using Ultraviolet Visible Spectroscopy (UV–Vis), determining values of 2.82 and 2.70 eV for the NPs synthesized with leaf and root, respectively. Finally, thermogravimetric analysis demonstrated that the nanoparticles contained an organic part after the green synthesis process, with high thermal stability for both samples. Photocatalytic analysis showed that these nanomaterials can degrade four dyes under UV irradiation, reaching 90% degradation for methylene blue (MB), methyl orange (MO) and Congo red (CR) at 60, 100 and 60 min, respectively, while for methyl red (MR) almost 90% degradation was achieved at 140 min of UV irradiation. These results demonstrate that it is effective to use Ambrosia ambrosioides root and leaf extracts as a reducing agent for the formation of ZnO NPs, also evidencing their favorable application in the photocatalytic degradation of these four organic dyes.</description><identifier>ISSN: 2227-9717</identifier><identifier>EISSN: 2227-9717</identifier><identifier>DOI: 10.3390/pr12112456</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Ambrosia ambrosioides ; Analysis ; Aqueous solutions ; Azo compounds ; Crystallites ; Crystals ; Degradation ; Dyes ; Electron microscopy ; Flavonoids ; Infrared analysis ; Infrared spectroscopy ; Irradiation ; Leaves ; Methylene blue ; Nanomaterials ; Nanoparticles ; Nanotechnology ; Oxidation ; Photocatalysis ; Photodegradation ; Plant extracts ; Pollutants ; Reducing agents ; Scanning electron microscopy ; Spectrum analysis ; Structure ; Synthesis ; Thermal stability ; Thermogravimetric analysis ; Transmission electron microscopy ; Ultraviolet radiation ; Wastewater ; Wurtzite ; X-ray diffraction ; Zinc oxide</subject><ispartof>Processes, 2024-11, Vol.12 (11), p.2456</ispartof><rights>COPYRIGHT 2024 MDPI AG</rights><rights>2024 by the authors. Licensee MDPI, Basel, Switzerland. This article is an open access article distributed under the terms and conditions of the Creative Commons Attribution (CC BY) license (https://creativecommons.org/licenses/by/4.0/). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c251t-2a777d0e98f9c35ce87d4f54b893afba5757aa6fe2fd8d509ff68625343930b3</cites><orcidid>0000-0001-5516-4393 ; 0000-0002-6171-0773 ; 0000-0002-9081-7836</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><link.rule.ids>314,776,780,27903,27904</link.rule.ids></links><search><creatorcontrib>Medina-Acosta, Martin</creatorcontrib><creatorcontrib>Chinchillas-Chinchillas, Manuel J.</creatorcontrib><creatorcontrib>Garrafa-Gálvez, Horacio E.</creatorcontrib><creatorcontrib>Garcia-Maro, Caree A.</creatorcontrib><creatorcontrib>Rosas-Casarez, Carlos A.</creatorcontrib><creatorcontrib>Lugo-Medina, Eder</creatorcontrib><creatorcontrib>Luque-Morales, Priscy A.</creatorcontrib><creatorcontrib>Soto-Robles, Carlos A.</creatorcontrib><title>Photocatalytic Degradation of Four Organic Dyes Present in Water Using ZnO Nanoparticles Synthesized with Green Synthesis Using Ambrosia ambrosioides Leaf and Root Extract</title><title>Processes</title><description>Currently, several organic dyes found in wastewater cause severe contamination problems for flora, fauna, and people in direct contact with them. This research proposes an alternative for the degradation of polluting dyes using ZnO nanoparticles (NPs) synthesized by an ecological route using leaf and root extracts of Ambrosia ambrosioides as a reducing agent (with a weight/volume ratio = 4%). Scanning Electron Microscopy (SEM) was used to determine the morphology, showing an agglomeration of cluster-shaped NPs. Using Transmission Electron Microscopy (TEM), different sizes of NPs ranging from 5 to 56 nm were observed for both synthesized NPs. The composition and structure of the nanomaterial were analyzed by infrared spectroscopy (FT-IR) and X-ray diffraction (XRD), showing as a result that the NPs have a wurtzite-like crystalline structure with crystallite sizes around 32–37 nm for both samples. Additionally, the bandgap of the NPs was calculated using Ultraviolet Visible Spectroscopy (UV–Vis), determining values of 2.82 and 2.70 eV for the NPs synthesized with leaf and root, respectively. Finally, thermogravimetric analysis demonstrated that the nanoparticles contained an organic part after the green synthesis process, with high thermal stability for both samples. Photocatalytic analysis showed that these nanomaterials can degrade four dyes under UV irradiation, reaching 90% degradation for methylene blue (MB), methyl orange (MO) and Congo red (CR) at 60, 100 and 60 min, respectively, while for methyl red (MR) almost 90% degradation was achieved at 140 min of UV irradiation. These results demonstrate that it is effective to use Ambrosia ambrosioides root and leaf extracts as a reducing agent for the formation of ZnO NPs, also evidencing their favorable application in the photocatalytic degradation of these four organic dyes.</description><subject>Ambrosia ambrosioides</subject><subject>Analysis</subject><subject>Aqueous solutions</subject><subject>Azo compounds</subject><subject>Crystallites</subject><subject>Crystals</subject><subject>Degradation</subject><subject>Dyes</subject><subject>Electron microscopy</subject><subject>Flavonoids</subject><subject>Infrared analysis</subject><subject>Infrared spectroscopy</subject><subject>Irradiation</subject><subject>Leaves</subject><subject>Methylene blue</subject><subject>Nanomaterials</subject><subject>Nanoparticles</subject><subject>Nanotechnology</subject><subject>Oxidation</subject><subject>Photocatalysis</subject><subject>Photodegradation</subject><subject>Plant extracts</subject><subject>Pollutants</subject><subject>Reducing agents</subject><subject>Scanning electron microscopy</subject><subject>Spectrum analysis</subject><subject>Structure</subject><subject>Synthesis</subject><subject>Thermal stability</subject><subject>Thermogravimetric analysis</subject><subject>Transmission electron microscopy</subject><subject>Ultraviolet radiation</subject><subject>Wastewater</subject><subject>Wurtzite</subject><subject>X-ray diffraction</subject><subject>Zinc oxide</subject><issn>2227-9717</issn><issn>2227-9717</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><sourceid>BENPR</sourceid><recordid>eNptUV1rWzEMvYwNVrq-7BcY9jZId21ffz2Gru0GYSn9YLCXi2LLiUtiZ7bLlv2l_ck5pKwrTHqQkM45ElLXvaX9Keem_7DNlFHKBiFfdEeMMTUxiqqX_-Svu5NS7vtmhnIt5FH3-2qVarJQYb2rwZKPuMzgoIYUSfLkIj1kMs9LiPveDgu5ylgwVhIi-QoVM7krIS7JtzgnXyCmLeQms27Am12sKyzhFzryI9QVucyI8W-5PBKnm0VOJQCBQ5KCa-QZgicQHblOqZLznzWDrW-6Vx7WBU8e43F3e3F-e_ZpMptffj6bziaWCVonDJRSrkejvbFcWNTKDV4MC204-AUIJRSA9Mi80070xnupJRN84Ib3C37cvTvIbnP6_oCljvftCrFNHDnlnCszSP2EWsIaxxB92u-4CcWOU031IGXPZUOd_gfV3OEm2BTRh1Z_Rnh_INh2jJLRj9scNpB3I-3H_ZfHpy_zP2x2m18</recordid><startdate>20241101</startdate><enddate>20241101</enddate><creator>Medina-Acosta, Martin</creator><creator>Chinchillas-Chinchillas, Manuel J.</creator><creator>Garrafa-Gálvez, Horacio E.</creator><creator>Garcia-Maro, Caree A.</creator><creator>Rosas-Casarez, Carlos A.</creator><creator>Lugo-Medina, Eder</creator><creator>Luque-Morales, Priscy A.</creator><creator>Soto-Robles, Carlos A.</creator><general>MDPI AG</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>8FH</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>AZQEC</scope><scope>BBNVY</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>LK8</scope><scope>M7P</scope><scope>PDBOC</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PRINS</scope><orcidid>https://orcid.org/0000-0001-5516-4393</orcidid><orcidid>https://orcid.org/0000-0002-6171-0773</orcidid><orcidid>https://orcid.org/0000-0002-9081-7836</orcidid></search><sort><creationdate>20241101</creationdate><title>Photocatalytic Degradation of Four Organic Dyes Present in Water Using ZnO Nanoparticles Synthesized with Green Synthesis Using Ambrosia ambrosioides Leaf and Root Extract</title><author>Medina-Acosta, Martin ; Chinchillas-Chinchillas, Manuel J. ; Garrafa-Gálvez, Horacio E. ; Garcia-Maro, Caree A. ; Rosas-Casarez, Carlos A. ; Lugo-Medina, Eder ; Luque-Morales, Priscy A. ; Soto-Robles, Carlos A.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c251t-2a777d0e98f9c35ce87d4f54b893afba5757aa6fe2fd8d509ff68625343930b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Ambrosia ambrosioides</topic><topic>Analysis</topic><topic>Aqueous solutions</topic><topic>Azo compounds</topic><topic>Crystallites</topic><topic>Crystals</topic><topic>Degradation</topic><topic>Dyes</topic><topic>Electron microscopy</topic><topic>Flavonoids</topic><topic>Infrared analysis</topic><topic>Infrared spectroscopy</topic><topic>Irradiation</topic><topic>Leaves</topic><topic>Methylene blue</topic><topic>Nanomaterials</topic><topic>Nanoparticles</topic><topic>Nanotechnology</topic><topic>Oxidation</topic><topic>Photocatalysis</topic><topic>Photodegradation</topic><topic>Plant extracts</topic><topic>Pollutants</topic><topic>Reducing agents</topic><topic>Scanning electron microscopy</topic><topic>Spectrum analysis</topic><topic>Structure</topic><topic>Synthesis</topic><topic>Thermal stability</topic><topic>Thermogravimetric analysis</topic><topic>Transmission electron microscopy</topic><topic>Ultraviolet radiation</topic><topic>Wastewater</topic><topic>Wurtzite</topic><topic>X-ray diffraction</topic><topic>Zinc oxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Medina-Acosta, Martin</creatorcontrib><creatorcontrib>Chinchillas-Chinchillas, Manuel J.</creatorcontrib><creatorcontrib>Garrafa-Gálvez, Horacio E.</creatorcontrib><creatorcontrib>Garcia-Maro, Caree A.</creatorcontrib><creatorcontrib>Rosas-Casarez, Carlos A.</creatorcontrib><creatorcontrib>Lugo-Medina, Eder</creatorcontrib><creatorcontrib>Luque-Morales, Priscy A.</creatorcontrib><creatorcontrib>Soto-Robles, Carlos A.</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>Biological Science Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>ProQuest Biological Science Collection</collection><collection>Biological Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><jtitle>Processes</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Medina-Acosta, Martin</au><au>Chinchillas-Chinchillas, Manuel J.</au><au>Garrafa-Gálvez, Horacio E.</au><au>Garcia-Maro, Caree A.</au><au>Rosas-Casarez, Carlos A.</au><au>Lugo-Medina, Eder</au><au>Luque-Morales, Priscy A.</au><au>Soto-Robles, Carlos A.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Photocatalytic Degradation of Four Organic Dyes Present in Water Using ZnO Nanoparticles Synthesized with Green Synthesis Using Ambrosia ambrosioides Leaf and Root Extract</atitle><jtitle>Processes</jtitle><date>2024-11-01</date><risdate>2024</risdate><volume>12</volume><issue>11</issue><spage>2456</spage><pages>2456-</pages><issn>2227-9717</issn><eissn>2227-9717</eissn><abstract>Currently, several organic dyes found in wastewater cause severe contamination problems for flora, fauna, and people in direct contact with them. This research proposes an alternative for the degradation of polluting dyes using ZnO nanoparticles (NPs) synthesized by an ecological route using leaf and root extracts of Ambrosia ambrosioides as a reducing agent (with a weight/volume ratio = 4%). Scanning Electron Microscopy (SEM) was used to determine the morphology, showing an agglomeration of cluster-shaped NPs. Using Transmission Electron Microscopy (TEM), different sizes of NPs ranging from 5 to 56 nm were observed for both synthesized NPs. The composition and structure of the nanomaterial were analyzed by infrared spectroscopy (FT-IR) and X-ray diffraction (XRD), showing as a result that the NPs have a wurtzite-like crystalline structure with crystallite sizes around 32–37 nm for both samples. Additionally, the bandgap of the NPs was calculated using Ultraviolet Visible Spectroscopy (UV–Vis), determining values of 2.82 and 2.70 eV for the NPs synthesized with leaf and root, respectively. Finally, thermogravimetric analysis demonstrated that the nanoparticles contained an organic part after the green synthesis process, with high thermal stability for both samples. Photocatalytic analysis showed that these nanomaterials can degrade four dyes under UV irradiation, reaching 90% degradation for methylene blue (MB), methyl orange (MO) and Congo red (CR) at 60, 100 and 60 min, respectively, while for methyl red (MR) almost 90% degradation was achieved at 140 min of UV irradiation. These results demonstrate that it is effective to use Ambrosia ambrosioides root and leaf extracts as a reducing agent for the formation of ZnO NPs, also evidencing their favorable application in the photocatalytic degradation of these four organic dyes.</abstract><cop>Basel</cop><pub>MDPI AG</pub><doi>10.3390/pr12112456</doi><orcidid>https://orcid.org/0000-0001-5516-4393</orcidid><orcidid>https://orcid.org/0000-0002-6171-0773</orcidid><orcidid>https://orcid.org/0000-0002-9081-7836</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Ambrosia ambrosioides Analysis Aqueous solutions Azo compounds Crystallites Crystals Degradation Dyes Electron microscopy Flavonoids Infrared analysis Infrared spectroscopy Irradiation Leaves Methylene blue Nanomaterials Nanoparticles Nanotechnology Oxidation Photocatalysis Photodegradation Plant extracts Pollutants Reducing agents Scanning electron microscopy Spectrum analysis Structure Synthesis Thermal stability Thermogravimetric analysis Transmission electron microscopy Ultraviolet radiation Wastewater Wurtzite X-ray diffraction Zinc oxide |
title | Photocatalytic Degradation of Four Organic Dyes Present in Water Using ZnO Nanoparticles Synthesized with Green Synthesis Using Ambrosia ambrosioides Leaf and Root Extract |
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