Polymer Blend Nanoarchitectonics with Exfoliated Molybdenum Disulphide/Polyvinyl Chloride/Nitrocellulose
Inorganic fillers modified polymer blends are in demands for domestic as well as engineering applications. In the present investigation, polyvinylchloride (PVC)/Nitrocellulose (NC)/Molybdenum disulphide (MoS 2 ) polymer blend were prepared by solution blending. Chemical functionalities present in po...
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Veröffentlicht in: | Journal of inorganic and organometallic polymers and materials 2023-03, Vol.33 (3), p.680-693 |
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creator | Jadhav, Pratibha S. Humbe, Shankar S. Joshi, Girish M. Deshmukh, R. R. Kaleemulla, S. |
description | Inorganic fillers modified polymer blends are in demands for domestic as well as engineering applications. In the present investigation, polyvinylchloride (PVC)/Nitrocellulose (NC)/Molybdenum disulphide (MoS
2
) polymer blend were prepared by solution blending. Chemical functionalities present in polymer blends were confirmed the interaction of filler and polymer host system analysed by Fourier transform infrared spectrophotometer. E
2
g and A
1
g active mode of Raman scattering were analysed by Raman spectroscopy. Increased degree of crystallinity and crystallite size of polymer blends due to incorporation of MoS
2
was investigated by X-ray diffraction. Increased pore morphology of polymer blends was foreseen by Scanning electron microscopy. Intercalated layers of MoS
2
in polymer host system was confirmed by energy dispersive X-ray analysis. Dielectric properties of the modified blends were studied by impedance analyser. The hydrophobic to hydrophilic nature of polymer system was determined by measurement of contact angle and relative surface energy analysed by surface goniometer. Increased thermal conductivity due to interaction of filler and polymer host system mutually correlate to the increased degree of crystallinity were explored by Lee’s disc probe. We quantified the influence of MoS
2
modified polymer blends could be preferred excellent candidate for engineering domain. |
doi_str_mv | 10.1007/s10904-022-02518-3 |
format | Article |
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2
) polymer blend were prepared by solution blending. Chemical functionalities present in polymer blends were confirmed the interaction of filler and polymer host system analysed by Fourier transform infrared spectrophotometer. E
2
g and A
1
g active mode of Raman scattering were analysed by Raman spectroscopy. Increased degree of crystallinity and crystallite size of polymer blends due to incorporation of MoS
2
was investigated by X-ray diffraction. Increased pore morphology of polymer blends was foreseen by Scanning electron microscopy. Intercalated layers of MoS
2
in polymer host system was confirmed by energy dispersive X-ray analysis. Dielectric properties of the modified blends were studied by impedance analyser. The hydrophobic to hydrophilic nature of polymer system was determined by measurement of contact angle and relative surface energy analysed by surface goniometer. Increased thermal conductivity due to interaction of filler and polymer host system mutually correlate to the increased degree of crystallinity were explored by Lee’s disc probe. We quantified the influence of MoS
2
modified polymer blends could be preferred excellent candidate for engineering domain.</description><identifier>ISSN: 1574-1443</identifier><identifier>EISSN: 1574-1451</identifier><identifier>DOI: 10.1007/s10904-022-02518-3</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Cellulose esters ; Cellulose nitrate ; Chemistry ; Chemistry and Materials Science ; Contact angle ; Crystallinity ; Crystallites ; Degree of crystallinity ; Dielectric properties ; Disulfides ; Energy dispersive X ray analysis ; Fillers ; Fourier transforms ; Infrared analysis ; Infrared spectrophotometers ; Inorganic Chemistry ; Molybdenum ; Molybdenum disulfide ; Organic Chemistry ; Polymer blends ; Polymer Sciences ; Polymers ; Polyvinyl chloride ; Raman spectra ; Raman spectroscopy ; Solution blending ; Surface energy ; Thermal conductivity ; X ray analysis</subject><ispartof>Journal of inorganic and organometallic polymers and materials, 2023-03, Vol.33 (3), p.680-693</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c319t-feb457d001f70cc3178acf01667b25f12d80b0a8ed41c694e0fc026d7d8acd2d3</citedby><cites>FETCH-LOGICAL-c319t-feb457d001f70cc3178acf01667b25f12d80b0a8ed41c694e0fc026d7d8acd2d3</cites><orcidid>0000-0003-4583-1708</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10904-022-02518-3$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10904-022-02518-3$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>315,781,785,27929,27930,41493,42562,51324</link.rule.ids></links><search><creatorcontrib>Jadhav, Pratibha S.</creatorcontrib><creatorcontrib>Humbe, Shankar S.</creatorcontrib><creatorcontrib>Joshi, Girish M.</creatorcontrib><creatorcontrib>Deshmukh, R. R.</creatorcontrib><creatorcontrib>Kaleemulla, S.</creatorcontrib><title>Polymer Blend Nanoarchitectonics with Exfoliated Molybdenum Disulphide/Polyvinyl Chloride/Nitrocellulose</title><title>Journal of inorganic and organometallic polymers and materials</title><addtitle>J Inorg Organomet Polym</addtitle><description>Inorganic fillers modified polymer blends are in demands for domestic as well as engineering applications. In the present investigation, polyvinylchloride (PVC)/Nitrocellulose (NC)/Molybdenum disulphide (MoS
2
) polymer blend were prepared by solution blending. Chemical functionalities present in polymer blends were confirmed the interaction of filler and polymer host system analysed by Fourier transform infrared spectrophotometer. E
2
g and A
1
g active mode of Raman scattering were analysed by Raman spectroscopy. Increased degree of crystallinity and crystallite size of polymer blends due to incorporation of MoS
2
was investigated by X-ray diffraction. Increased pore morphology of polymer blends was foreseen by Scanning electron microscopy. Intercalated layers of MoS
2
in polymer host system was confirmed by energy dispersive X-ray analysis. Dielectric properties of the modified blends were studied by impedance analyser. The hydrophobic to hydrophilic nature of polymer system was determined by measurement of contact angle and relative surface energy analysed by surface goniometer. Increased thermal conductivity due to interaction of filler and polymer host system mutually correlate to the increased degree of crystallinity were explored by Lee’s disc probe. We quantified the influence of MoS
2
modified polymer blends could be preferred excellent candidate for engineering domain.</description><subject>Cellulose esters</subject><subject>Cellulose nitrate</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Contact angle</subject><subject>Crystallinity</subject><subject>Crystallites</subject><subject>Degree of crystallinity</subject><subject>Dielectric properties</subject><subject>Disulfides</subject><subject>Energy dispersive X ray analysis</subject><subject>Fillers</subject><subject>Fourier transforms</subject><subject>Infrared analysis</subject><subject>Infrared spectrophotometers</subject><subject>Inorganic Chemistry</subject><subject>Molybdenum</subject><subject>Molybdenum disulfide</subject><subject>Organic Chemistry</subject><subject>Polymer blends</subject><subject>Polymer Sciences</subject><subject>Polymers</subject><subject>Polyvinyl chloride</subject><subject>Raman spectra</subject><subject>Raman spectroscopy</subject><subject>Solution blending</subject><subject>Surface energy</subject><subject>Thermal conductivity</subject><subject>X ray analysis</subject><issn>1574-1443</issn><issn>1574-1451</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp9kElPwzAQhS0EEqXwBzhF4hw6trMeoZRFKssBzlbihbhy42I7QP89LkFw4zCa0ei9N5oPoVMM5xignHkMNWQpEBIrx1VK99AE52WW4izH-79zRg_RkfcrAFpBjieoe7Jmu5YuuTSyF8lD09vG8U4HyYPtNffJhw5dsvhU1ugmSJHcR0MrZD-skyvtB7PptJCzXcy77rcmmXfGut3qQQdnuTRmMNbLY3SgGuPlyU-fopfrxfP8Nl0-3tzNL5Ypp7gOqZJtlpcCAKsSeNyVVcMV4KIoW5IrTEQFLTSVFBnmRZ1JUBxIIUoRdYIIOkVnY-7G2bdB-sBWdnB9PMkoJkVNSfw8qsio4s5676RiG6fXjdsyDGxHlI1EWSTKvokyGk10NPko7l-l-4v-x_UFz2F7gQ</recordid><startdate>20230301</startdate><enddate>20230301</enddate><creator>Jadhav, Pratibha S.</creator><creator>Humbe, Shankar S.</creator><creator>Joshi, Girish M.</creator><creator>Deshmukh, R. R.</creator><creator>Kaleemulla, S.</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0000-0003-4583-1708</orcidid></search><sort><creationdate>20230301</creationdate><title>Polymer Blend Nanoarchitectonics with Exfoliated Molybdenum Disulphide/Polyvinyl Chloride/Nitrocellulose</title><author>Jadhav, Pratibha S. ; Humbe, Shankar S. ; Joshi, Girish M. ; Deshmukh, R. R. ; Kaleemulla, S.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c319t-feb457d001f70cc3178acf01667b25f12d80b0a8ed41c694e0fc026d7d8acd2d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Cellulose esters</topic><topic>Cellulose nitrate</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Contact angle</topic><topic>Crystallinity</topic><topic>Crystallites</topic><topic>Degree of crystallinity</topic><topic>Dielectric properties</topic><topic>Disulfides</topic><topic>Energy dispersive X ray analysis</topic><topic>Fillers</topic><topic>Fourier transforms</topic><topic>Infrared analysis</topic><topic>Infrared spectrophotometers</topic><topic>Inorganic Chemistry</topic><topic>Molybdenum</topic><topic>Molybdenum disulfide</topic><topic>Organic Chemistry</topic><topic>Polymer blends</topic><topic>Polymer Sciences</topic><topic>Polymers</topic><topic>Polyvinyl chloride</topic><topic>Raman spectra</topic><topic>Raman spectroscopy</topic><topic>Solution blending</topic><topic>Surface energy</topic><topic>Thermal conductivity</topic><topic>X ray analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Jadhav, Pratibha S.</creatorcontrib><creatorcontrib>Humbe, Shankar S.</creatorcontrib><creatorcontrib>Joshi, Girish M.</creatorcontrib><creatorcontrib>Deshmukh, R. R.</creatorcontrib><creatorcontrib>Kaleemulla, S.</creatorcontrib><collection>CrossRef</collection><jtitle>Journal of inorganic and organometallic polymers and materials</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Jadhav, Pratibha S.</au><au>Humbe, Shankar S.</au><au>Joshi, Girish M.</au><au>Deshmukh, R. R.</au><au>Kaleemulla, S.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Polymer Blend Nanoarchitectonics with Exfoliated Molybdenum Disulphide/Polyvinyl Chloride/Nitrocellulose</atitle><jtitle>Journal of inorganic and organometallic polymers and materials</jtitle><stitle>J Inorg Organomet Polym</stitle><date>2023-03-01</date><risdate>2023</risdate><volume>33</volume><issue>3</issue><spage>680</spage><epage>693</epage><pages>680-693</pages><issn>1574-1443</issn><eissn>1574-1451</eissn><abstract>Inorganic fillers modified polymer blends are in demands for domestic as well as engineering applications. In the present investigation, polyvinylchloride (PVC)/Nitrocellulose (NC)/Molybdenum disulphide (MoS
2
) polymer blend were prepared by solution blending. Chemical functionalities present in polymer blends were confirmed the interaction of filler and polymer host system analysed by Fourier transform infrared spectrophotometer. E
2
g and A
1
g active mode of Raman scattering were analysed by Raman spectroscopy. Increased degree of crystallinity and crystallite size of polymer blends due to incorporation of MoS
2
was investigated by X-ray diffraction. Increased pore morphology of polymer blends was foreseen by Scanning electron microscopy. Intercalated layers of MoS
2
in polymer host system was confirmed by energy dispersive X-ray analysis. Dielectric properties of the modified blends were studied by impedance analyser. The hydrophobic to hydrophilic nature of polymer system was determined by measurement of contact angle and relative surface energy analysed by surface goniometer. Increased thermal conductivity due to interaction of filler and polymer host system mutually correlate to the increased degree of crystallinity were explored by Lee’s disc probe. We quantified the influence of MoS
2
modified polymer blends could be preferred excellent candidate for engineering domain.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10904-022-02518-3</doi><tpages>14</tpages><orcidid>https://orcid.org/0000-0003-4583-1708</orcidid></addata></record> |
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subjects | Cellulose esters Cellulose nitrate Chemistry Chemistry and Materials Science Contact angle Crystallinity Crystallites Degree of crystallinity Dielectric properties Disulfides Energy dispersive X ray analysis Fillers Fourier transforms Infrared analysis Infrared spectrophotometers Inorganic Chemistry Molybdenum Molybdenum disulfide Organic Chemistry Polymer blends Polymer Sciences Polymers Polyvinyl chloride Raman spectra Raman spectroscopy Solution blending Surface energy Thermal conductivity X ray analysis |
title | Polymer Blend Nanoarchitectonics with Exfoliated Molybdenum Disulphide/Polyvinyl Chloride/Nitrocellulose |
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