The Effect of Anodization and Thermal Treatment on Mixed-Oxide Layer Formation on Ti–Zr Alloy
The anodization or thermal treatments applied to alloys of titanium and zirconium have a substantiated effect on the mixed-oxide layer formation compared to the naturally occurring one. A Ti–Zr 50%/50% alloy was chosen for a comparative study. Controlled, thermally treated, and anodized samples obta...
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| Veröffentlicht in: | Coatings (Basel) 2024-09, Vol.14 (9), p.1217 |
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| creator | Ciobotaru, Ioana-Alina Ismail, Fidan Bahtiar Budei, Roxana Cojocaru, Anca Vaireanu, Danut-Ionel |
| description | The anodization or thermal treatments applied to alloys of titanium and zirconium have a substantiated effect on the mixed-oxide layer formation compared to the naturally occurring one. A Ti–Zr 50%/50% alloy was chosen for a comparative study. Controlled, thermally treated, and anodized samples obtained with controlled procedures were analyzed in terms of morphological and compositional analysis (using SEM and EDX analysis) as well as for the determination of hardness variations. Substantial differences were observed depending on the applied functionalization method (compact of structured mixed-oxide nanotubes when the samples are subjected to the anodization procedure); there was an increase of more than six folds in the mixed-oxide layer hardness and D Shore scale, when subjected to thermal treatment, and hence, this lead to the conclusion that one may control the morphology, composition and/or the hardness of the mixed-oxide layer by applying one or another or a combination of functionalization methods. |
| doi_str_mv | 10.3390/coatings14091217 |
| format | Article |
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A Ti–Zr 50%/50% alloy was chosen for a comparative study. Controlled, thermally treated, and anodized samples obtained with controlled procedures were analyzed in terms of morphological and compositional analysis (using SEM and EDX analysis) as well as for the determination of hardness variations. Substantial differences were observed depending on the applied functionalization method (compact of structured mixed-oxide nanotubes when the samples are subjected to the anodization procedure); there was an increase of more than six folds in the mixed-oxide layer hardness and D Shore scale, when subjected to thermal treatment, and hence, this lead to the conclusion that one may control the morphology, composition and/or the hardness of the mixed-oxide layer by applying one or another or a combination of functionalization methods.</description><identifier>ISSN: 2079-6412</identifier><identifier>EISSN: 2079-6412</identifier><identifier>DOI: 10.3390/coatings14091217</identifier><language>eng</language><publisher>Basel: MDPI AG</publisher><subject>Alloys ; Analysis ; Anodizing ; Biocompatibility ; Cell adhesion & migration ; Comparative studies ; Corrosion resistance ; Electrolytes ; Hardness ; Heat treatment ; Lasers ; Mechanical properties ; Metals ; Mixed oxides ; Morphology ; Nanotubes ; Oxidation ; Pore size ; Scale (corrosion) ; Specialty metals industry ; Titanium ; Titanium base alloys ; Zirconium ; Zirconium base alloys</subject><ispartof>Coatings (Basel), 2024-09, Vol.14 (9), p.1217</ispartof><rights>COPYRIGHT 2024 MDPI AG</rights><rights>2024 by the authors. 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Ismail, Fidan Bahtiar ; Budei, Roxana ; Cojocaru, Anca ; Vaireanu, Danut-Ionel</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c235t-f31151d9c54c8c6966bbca56a7ab022f98bd596ccf861881052c1b11f7a31ae23</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Alloys</topic><topic>Analysis</topic><topic>Anodizing</topic><topic>Biocompatibility</topic><topic>Cell adhesion & migration</topic><topic>Comparative studies</topic><topic>Corrosion resistance</topic><topic>Electrolytes</topic><topic>Hardness</topic><topic>Heat treatment</topic><topic>Lasers</topic><topic>Mechanical properties</topic><topic>Metals</topic><topic>Mixed oxides</topic><topic>Morphology</topic><topic>Nanotubes</topic><topic>Oxidation</topic><topic>Pore size</topic><topic>Scale (corrosion)</topic><topic>Specialty metals industry</topic><topic>Titanium</topic><topic>Titanium base alloys</topic><topic>Zirconium</topic><topic>Zirconium base alloys</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Ciobotaru, Ioana-Alina</creatorcontrib><creatorcontrib>Ismail, Fidan Bahtiar</creatorcontrib><creatorcontrib>Budei, Roxana</creatorcontrib><creatorcontrib>Cojocaru, Anca</creatorcontrib><creatorcontrib>Vaireanu, Danut-Ionel</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>ProQuest Central China</collection><jtitle>Coatings (Basel)</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Ciobotaru, Ioana-Alina</au><au>Ismail, Fidan Bahtiar</au><au>Budei, Roxana</au><au>Cojocaru, Anca</au><au>Vaireanu, Danut-Ionel</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>The Effect of Anodization and Thermal Treatment on Mixed-Oxide Layer Formation on Ti–Zr Alloy</atitle><jtitle>Coatings (Basel)</jtitle><date>2024-09-01</date><risdate>2024</risdate><volume>14</volume><issue>9</issue><spage>1217</spage><pages>1217-</pages><issn>2079-6412</issn><eissn>2079-6412</eissn><abstract>The anodization or thermal treatments applied to alloys of titanium and zirconium have a substantiated effect on the mixed-oxide layer formation compared to the naturally occurring one. A Ti–Zr 50%/50% alloy was chosen for a comparative study. Controlled, thermally treated, and anodized samples obtained with controlled procedures were analyzed in terms of morphological and compositional analysis (using SEM and EDX analysis) as well as for the determination of hardness variations. Substantial differences were observed depending on the applied functionalization method (compact of structured mixed-oxide nanotubes when the samples are subjected to the anodization procedure); there was an increase of more than six folds in the mixed-oxide layer hardness and D Shore scale, when subjected to thermal treatment, and hence, this lead to the conclusion that one may control the morphology, composition and/or the hardness of the mixed-oxide layer by applying one or another or a combination of functionalization methods.</abstract><cop>Basel</cop><pub>MDPI AG</pub><doi>10.3390/coatings14091217</doi><orcidid>https://orcid.org/0000-0001-5402-9253</orcidid><orcidid>https://orcid.org/0000-0003-2737-2990</orcidid><orcidid>https://orcid.org/0000-0001-9109-488X</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | Alloys Analysis Anodizing Biocompatibility Cell adhesion & migration Comparative studies Corrosion resistance Electrolytes Hardness Heat treatment Lasers Mechanical properties Metals Mixed oxides Morphology Nanotubes Oxidation Pore size Scale (corrosion) Specialty metals industry Titanium Titanium base alloys Zirconium Zirconium base alloys |
| title | The Effect of Anodization and Thermal Treatment on Mixed-Oxide Layer Formation on Ti–Zr Alloy |
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