Fabrication of BaTiO3–Bi(Mg0.5Ti0.5)O3–BiFeO3 ceramics at lower temperature by using citrate method

We fabricated 0.3BaTiO3–0.1Bi(Mg0.5Ti0.5)O3–0.6BiFeO3 (0.3BT–0.1BMT–0.6BF) ceramics prepared using powders synthesized using the citrate method (CM) and solid state method (SSM) and investigated their microstructure and electric properties. Compared with SSM, CM reduced calcination temperature by 30...

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Veröffentlicht in:	Journal of the Ceramic Society of Japan 2024/07/01, Vol.132(7), pp.358-363
Hauptverfasser:	Nakagawa, Shota, Fujii, Ichiro, Nam, Hyunwook, Ueno, Shintaro, Wada, Satoshi
Format:	Artikel
Sprache:	eng ; jpn
Schlagworte:	Barium titanates Ceramics Citrate method Ferroelectricity Ferroelectrics Piezoelectricity Piezoelectrics Roasting Sintering (powder metallurgy) Specific gravity Synthesis
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container_title	Journal of the Ceramic Society of Japan
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creator	Nakagawa, Shota Fujii, Ichiro Nam, Hyunwook Ueno, Shintaro Wada, Satoshi
description	We fabricated 0.3BaTiO3–0.1Bi(Mg0.5Ti0.5)O3–0.6BiFeO3 (0.3BT–0.1BMT–0.6BF) ceramics prepared using powders synthesized using the citrate method (CM) and solid state method (SSM) and investigated their microstructure and electric properties. Compared with SSM, CM reduced calcination temperature by 300 °C to synthesize 0.3BT–0.1BMT–0.6BF and reduced sintering temperature by 100 °C to densify the ceramics with a relative density of more than 95 %. The reduced calcination and sintering temperatures with CM were due to a smaller calcined powder. Improved ferroelectric and piezoelectric properties were observed for the ceramics prepared using this method. This could be attributed to reduced defects associated with the suppression of Bi volatilization.
doi_str_mv	10.2109/jcersj2.23215
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Compared with SSM, CM reduced calcination temperature by 300 °C to synthesize 0.3BT–0.1BMT–0.6BF and reduced sintering temperature by 100 °C to densify the ceramics with a relative density of more than 95 %. The reduced calcination and sintering temperatures with CM were due to a smaller calcined powder. Improved ferroelectric and piezoelectric properties were observed for the ceramics prepared using this method. 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Soc. Japan</addtitle><description>We fabricated 0.3BaTiO3–0.1Bi(Mg0.5Ti0.5)O3–0.6BiFeO3 (0.3BT–0.1BMT–0.6BF) ceramics prepared using powders synthesized using the citrate method (CM) and solid state method (SSM) and investigated their microstructure and electric properties. Compared with SSM, CM reduced calcination temperature by 300 °C to synthesize 0.3BT–0.1BMT–0.6BF and reduced sintering temperature by 100 °C to densify the ceramics with a relative density of more than 95 %. The reduced calcination and sintering temperatures with CM were due to a smaller calcined powder. Improved ferroelectric and piezoelectric properties were observed for the ceramics prepared using this method. 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subjects	Barium titanates Ceramics Citrate method Ferroelectricity Ferroelectrics Piezoelectricity Piezoelectrics Roasting Sintering (powder metallurgy) Specific gravity Synthesis
title	Fabrication of BaTiO3–Bi(Mg0.5Ti0.5)O3–BiFeO3 ceramics at lower temperature by using citrate method
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