Tuning crystal size and inhibiting aggregation by adding guanidinoacetic acid in ZSM-5 zeolite synthesis for catalysing methanol-to-olefin reaction
Nanosized ZSM-5 zeolite with high-quality is highly desired in industrial application. This paper reports an approach of rapid synthesis of this type zeolite, being realized by crystallizing gels with the Si/Al atomic ratio of 12.5–80 at 170 ℃ for 12 h under assistance of guanidinoacetic acid (GAA)....
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| Veröffentlicht in: | Journal of porous materials 2024-08, Vol.31 (4), p.1477-1488 |
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| container_title | Journal of porous materials |
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| creator | Dong, Cunmei Li, Hongjiang Li, Shenmin Cui, Yingna Wang, Xinping |
| description | Nanosized ZSM-5 zeolite with high-quality is highly desired in industrial application. This paper reports an approach of rapid synthesis of this type zeolite, being realized by crystallizing gels with the Si/Al atomic ratio of 12.5–80 at 170 ℃ for 12 h under assistance of guanidinoacetic acid (GAA). As a result, the zeolite obtained from the synthesis possesses little crystal size (120–220 nm), high-quality and good monodispersity. Being associated with the superior morphology and structure, the zeolite displayed not only longer one-pass catalytic lifetime but also much higher regeneration stability in methanol-to-olefin reaction, comparing with the zeolite synthesized without GAA addition. |
| doi_str_mv | 10.1007/s10934-024-01615-7 |
| format | Article |
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| subjects | Catalysis Characterization and Evaluation of Materials Chemical synthesis Chemistry Chemistry and Materials Science Gels Industrial applications Methanol Physical Chemistry Zeolites |
| title | Tuning crystal size and inhibiting aggregation by adding guanidinoacetic acid in ZSM-5 zeolite synthesis for catalysing methanol-to-olefin reaction |
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