Endosulfan pesticide detection using an electrochemical sensor based on molecularly imprinted polymer (MIP)
Pesticides and herbicides are active chemicals used to eradicate plant pests which constitute contamination if they exceed the threshold for the environment and humans. Molecularly Imprinted Polymer (MIP) is a technique for making polymers that are obtained from cross-linked polymers and have caviti...
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| Veröffentlicht in: | IOP conference series. Earth and environmental science 2024-06, Vol.1356 (1), p.12065 |
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| creator | Bow, Y Syakdani, A Purnamasari, I Pratama, MY |
| description | Pesticides and herbicides are active chemicals used to eradicate plant pests which constitute contamination if they exceed the threshold for the environment and humans. Molecularly Imprinted Polymer (MIP) is a technique for making polymers that are obtained from cross-linked polymers and have cavities that match the template, where the cavities function as a medium for mechanical interaction of molecules with the same size, shape, structure, and physicochemical properties. The polymer produced from the MIP technique is applied to the surface of the sensor material as an endosulfan detection. This research aims to create an endosulfan MIP to obtain a potentiometric MIP sensor capable of detecting endosulfan. The results showed that the optimum conditions for making MIP endosulfan were obtained with a composition of 6.02 mL of chloroform; 0.025 g endosulfan; 0.9 mL methacrylic acid (MAA); 1.57 mL ethylene glycol dimethacrylate acid (EGDMA); 0.07 g benzoyl peroxide with a heating time of 150 minutes at a temperature of 70 °C. The sensor performance test was carried out potentiometrically and it was found that the MIP endosulfan sensor that was made had sensitivity and stability in the concentration range of 0.01-1.0x10 −6 ppm with a lifetime up to 90 days. |
| doi_str_mv | 10.1088/1755-1315/1356/1/012065 |
| format | Article |
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Molecularly Imprinted Polymer (MIP) is a technique for making polymers that are obtained from cross-linked polymers and have cavities that match the template, where the cavities function as a medium for mechanical interaction of molecules with the same size, shape, structure, and physicochemical properties. The polymer produced from the MIP technique is applied to the surface of the sensor material as an endosulfan detection. This research aims to create an endosulfan MIP to obtain a potentiometric MIP sensor capable of detecting endosulfan. The results showed that the optimum conditions for making MIP endosulfan were obtained with a composition of 6.02 mL of chloroform; 0.025 g endosulfan; 0.9 mL methacrylic acid (MAA); 1.57 mL ethylene glycol dimethacrylate acid (EGDMA); 0.07 g benzoyl peroxide with a heating time of 150 minutes at a temperature of 70 °C. The sensor performance test was carried out potentiometrically and it was found that the MIP endosulfan sensor that was made had sensitivity and stability in the concentration range of 0.01-1.0x10 −6 ppm with a lifetime up to 90 days.</description><identifier>ISSN: 1755-1307</identifier><identifier>EISSN: 1755-1315</identifier><identifier>DOI: 10.1088/1755-1315/1356/1/012065</identifier><language>eng</language><publisher>Bristol: IOP Publishing</publisher><subject>Benzoyl peroxide ; Cavities ; Chemical sensors ; Chloroform ; Electrochemistry ; Endosulfan ; Ethylene glycol ; Glycol dimethacrylates ; Herbicides ; Imprinted polymers ; Mechanical properties ; Methacrylic acid ; Molecular structure ; Performance tests ; Pesticides ; Pests ; Physicochemical properties ; Polymers ; Sensitivity analysis ; Sensors ; Structure-function relationships</subject><ispartof>IOP conference series. Earth and environmental science, 2024-06, Vol.1356 (1), p.12065</ispartof><rights>Published under licence by IOP Publishing Ltd</rights><rights>Published under licence by IOP Publishing Ltd. This work is published under https://creativecommons.org/licenses/by/4.0/ (the “License”). 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Earth and environmental science</title><addtitle>IOP Conf. Ser.: Earth Environ. Sci</addtitle><description>Pesticides and herbicides are active chemicals used to eradicate plant pests which constitute contamination if they exceed the threshold for the environment and humans. Molecularly Imprinted Polymer (MIP) is a technique for making polymers that are obtained from cross-linked polymers and have cavities that match the template, where the cavities function as a medium for mechanical interaction of molecules with the same size, shape, structure, and physicochemical properties. The polymer produced from the MIP technique is applied to the surface of the sensor material as an endosulfan detection. This research aims to create an endosulfan MIP to obtain a potentiometric MIP sensor capable of detecting endosulfan. 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| subjects | Benzoyl peroxide Cavities Chemical sensors Chloroform Electrochemistry Endosulfan Ethylene glycol Glycol dimethacrylates Herbicides Imprinted polymers Mechanical properties Methacrylic acid Molecular structure Performance tests Pesticides Pests Physicochemical properties Polymers Sensitivity analysis Sensors Structure-function relationships |
| title | Endosulfan pesticide detection using an electrochemical sensor based on molecularly imprinted polymer (MIP) |
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