Structure and Properties of Composite Coatings with Zro2 and Tio2 Particles After Lehceb Treatment

The paper presents the comprehensive analysis of the structure, properties, and corrosion of micro-arc coatings with ZrO 2 and TiO 2 particles after the low-energy high-current electron beam (LEHCEB) treatment. The coating morphology, microstructure, phase and elemental compositions are investigated...

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Veröffentlicht in:Russian physics journal 2024-07, Vol.67 (7), p.895-903
Hauptverfasser: Sedelnikova, M. B., Kashin, A. D., Uvarkin, P. V., Sharkeev, Y. P., Ugodchikova, A. V., Luginin, N. A., Khimich, M. A., Ivanov, K. V.
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container_end_page 903
container_issue 7
container_start_page 895
container_title Russian physics journal
container_volume 67
creator Sedelnikova, M. B.
Kashin, A. D.
Uvarkin, P. V.
Sharkeev, Y. P.
Ugodchikova, A. V.
Luginin, N. A.
Khimich, M. A.
Ivanov, K. V.
description The paper presents the comprehensive analysis of the structure, properties, and corrosion of micro-arc coatings with ZrO 2 and TiO 2 particles after the low-energy high-current electron beam (LEHCEB) treatment. The coating morphology, microstructure, phase and elemental compositions are investigated by the scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray powder diffraction. After the LEHCEB treatment, the coating structure with ZrO 2 particles changes from friable and porous to denser with closed spheroidal pores. It is shown that the adhesive strength of the coating with ZrO 2 particles increases with the critical load growth from 10 to 18 N. Moreover, the treatment enhances its corrosion resistance, as evidenced by a reduction in the corrosion current from 7.48∙10 –7 to 1.05∙10 –8 A/cm 2 and an increase in polarization resistance from 0.9·10 4 to 5.77∙10 6 Ω·cm 2 . In contrast, the coatings with TiO 2 particles exhibit a more porous structure due to the volatilization of low-melting components (sodium silicates), as evidenced by a reduction in the concentration of Na and Si elements in their composition. The adhesive strength and corrosion resistance of the coatings with TiO 2 particles deteriorate after the treatment.
doi_str_mv 10.1007/s11182-024-03194-1
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subjects Adhesive strength
Coatings
Condensed Matter Physics
Corrosion currents
Corrosion resistance
Electron beams
Friability
Hadrons
Heavy Ions
Lasers
Mathematical and Computational Physics
Nuclear Physics
Optical Devices
Optics
Particulate composites
Photonics
Physics
Physics and Astronomy
Silicates
Silicon
Sodium
Sodium silicates
Theoretical
Titanium dioxide
X ray powder diffraction
Zirconium dioxide
title Structure and Properties of Composite Coatings with Zro2 and Tio2 Particles After Lehceb Treatment
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