Impact of Microstructural and Surface Modifications on the Ti-45Nb Alloy’s Response to Bio-Environment
The Ti-45Nb (mass%) alloy’s corrosive and biocompatible response in simulated physiological conditions was investigated before and after its additional high-pressure torsion (HPT) and laser irradiation processing. The grain size reduction from 2.76 µm to ~ 200 nm and the appearance of laser-induced...
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| Veröffentlicht in: | Acta metallurgica sinica : English letters 2024-07, Vol.37 (7), p.1215-1230 |
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| creator | Cvijović-Alagić, Ivana Laketić, Slađana Momčilović, Miloš Ciganović, Jovan Bajat, Jelena Kojić, Vesna |
| description | The Ti-45Nb (mass%) alloy’s corrosive and biocompatible response in simulated physiological conditions was investigated before and after its additional high-pressure torsion (HPT) and laser irradiation processing. The grain size reduction from 2.76 µm to ~ 200 nm and the appearance of laser-induced morphologically altered and highly oxidized surface led to the significant improvement of alloy corrosion resistance and cell–implant interaction. Moreover, an additional increase of the laser pulse energy from 5 to 15 mJ during the alloy irradiation in the air led to an increase in the surface oxygen content from 13.64 to 23.89% accompanied by an increase of excellent cell viability from 127.18 to 134.42%. As a result of the controlled alloy microstructural and surface modifications, the formation of protective bi-modal mixed Ti- and Nb-oxide external scale was enabled. The presence of this surface oxide scale enhanced the alloy’s resistance to corrosion deterioration and simultaneously boosted cell viability and proliferation. |
| doi_str_mv | 10.1007/s40195-024-01705-0 |
| format | Article |
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The grain size reduction from 2.76 µm to ~ 200 nm and the appearance of laser-induced morphologically altered and highly oxidized surface led to the significant improvement of alloy corrosion resistance and cell–implant interaction. Moreover, an additional increase of the laser pulse energy from 5 to 15 mJ during the alloy irradiation in the air led to an increase in the surface oxygen content from 13.64 to 23.89% accompanied by an increase of excellent cell viability from 127.18 to 134.42%. As a result of the controlled alloy microstructural and surface modifications, the formation of protective bi-modal mixed Ti- and Nb-oxide external scale was enabled. 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Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c270t-2c4bcd03d96df76b3f96096444ba1f040bf7ad7b342440e8d34f20c01e7588303</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s40195-024-01705-0$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s40195-024-01705-0$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Cvijović-Alagić, Ivana</creatorcontrib><creatorcontrib>Laketić, Slađana</creatorcontrib><creatorcontrib>Momčilović, Miloš</creatorcontrib><creatorcontrib>Ciganović, Jovan</creatorcontrib><creatorcontrib>Bajat, Jelena</creatorcontrib><creatorcontrib>Kojić, Vesna</creatorcontrib><title>Impact of Microstructural and Surface Modifications on the Ti-45Nb Alloy’s Response to Bio-Environment</title><title>Acta metallurgica sinica : English letters</title><addtitle>Acta Metall. Sin. (Engl. Lett.)</addtitle><description>The Ti-45Nb (mass%) alloy’s corrosive and biocompatible response in simulated physiological conditions was investigated before and after its additional high-pressure torsion (HPT) and laser irradiation processing. The grain size reduction from 2.76 µm to ~ 200 nm and the appearance of laser-induced morphologically altered and highly oxidized surface led to the significant improvement of alloy corrosion resistance and cell–implant interaction. Moreover, an additional increase of the laser pulse energy from 5 to 15 mJ during the alloy irradiation in the air led to an increase in the surface oxygen content from 13.64 to 23.89% accompanied by an increase of excellent cell viability from 127.18 to 134.42%. As a result of the controlled alloy microstructural and surface modifications, the formation of protective bi-modal mixed Ti- and Nb-oxide external scale was enabled. 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Sin. (Engl. Lett.)</stitle><date>2024-07-01</date><risdate>2024</risdate><volume>37</volume><issue>7</issue><spage>1215</spage><epage>1230</epage><pages>1215-1230</pages><issn>1006-7191</issn><eissn>2194-1289</eissn><abstract>The Ti-45Nb (mass%) alloy’s corrosive and biocompatible response in simulated physiological conditions was investigated before and after its additional high-pressure torsion (HPT) and laser irradiation processing. The grain size reduction from 2.76 µm to ~ 200 nm and the appearance of laser-induced morphologically altered and highly oxidized surface led to the significant improvement of alloy corrosion resistance and cell–implant interaction. Moreover, an additional increase of the laser pulse energy from 5 to 15 mJ during the alloy irradiation in the air led to an increase in the surface oxygen content from 13.64 to 23.89% accompanied by an increase of excellent cell viability from 127.18 to 134.42%. As a result of the controlled alloy microstructural and surface modifications, the formation of protective bi-modal mixed Ti- and Nb-oxide external scale was enabled. The presence of this surface oxide scale enhanced the alloy’s resistance to corrosion deterioration and simultaneously boosted cell viability and proliferation.</abstract><cop>Beijing</cop><pub>The Chinese Society for Metals</pub><doi>10.1007/s40195-024-01705-0</doi><tpages>16</tpages></addata></record> |
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| subjects | Alloys Biocompatibility Biomechanics Characterization and Evaluation of Materials Chemistry and Materials Science Corrosion and Coatings Corrosion cell Corrosion resistance Corrosion resistant alloys Cytotoxicity Grain size Irradiation Lasers Materials Science Metallic Materials Nanotechnology Organometallic Chemistry Orthopedics Oxygen content Physiology Scale (corrosion) Shear strain Spectroscopy/Spectrometry Surgery Titanium base alloys Topography Transplants & implants Tribology |
| title | Impact of Microstructural and Surface Modifications on the Ti-45Nb Alloy’s Response to Bio-Environment |
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