Electrochemical behaviour of microwave-assisted synthesized cerium oxide annealed at different temperatures
In the recent past, the electrode materials with high capacitance and excellent cycle stability have attracted the global scientific community for the development of novel advanced supercapacitors. In that context, rare earth metal oxides like Cerium Oxide (CeO 2 ) have emerged as potential electrod...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2024-06, Vol.35 (17), p.1153, Article 1153 |
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| creator | Lokhande, P. E. Jagtap, Chaitali Kadam, Vishal Rednam, Udayabhaskar Aepur, Radhamanohar Tambe, Amol Naushad, Mu Thirumurugan, Arun |
| description | In the recent past, the electrode materials with high capacitance and excellent cycle stability have attracted the global scientific community for the development of novel advanced supercapacitors. In that context, rare earth metal oxides like Cerium Oxide (CeO
2
) have emerged as potential electrode material due to its characteristics such as prominent valency states, eco-friendly nature, abundance, and outstanding redox properties. The current study reports about the CeO
2
nanomaterial that is synthesized by microwave-assisted method followed by post-annealing at different temperatures and thereby examined for supercapacitor applications. The crystallographic and morphological study confirms the formation of CeO
2
nanoparticles and porous nature of the prepared materials. As annealing temperature was increased, the properties of CeO
2
changed and demonstrated different performance. The maximum specific capacitance of 656 Fg
−1
at 2 Ag
−1
was observed for the sample annealed at 500 °C. The asymmetric supercapacitor fabricated CeO
2
//AC exhibited an energy density of 18 Wh kg
−1
at a power density of 833 W kg
−1
along with excellent rate capability. Further cyclic stability test conducted for 3000 cycles exhibited a capacitance retention of 93% which demonstrated the superior stability of the material. The observed electrochemical results demonstrated the potential of CeO
2
that paves way for the further involvement of these in the energy storage field. |
| doi_str_mv | 10.1007/s10854-024-12900-1 |
| format | Article |
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2
) have emerged as potential electrode material due to its characteristics such as prominent valency states, eco-friendly nature, abundance, and outstanding redox properties. The current study reports about the CeO
2
nanomaterial that is synthesized by microwave-assisted method followed by post-annealing at different temperatures and thereby examined for supercapacitor applications. The crystallographic and morphological study confirms the formation of CeO
2
nanoparticles and porous nature of the prepared materials. As annealing temperature was increased, the properties of CeO
2
changed and demonstrated different performance. The maximum specific capacitance of 656 Fg
−1
at 2 Ag
−1
was observed for the sample annealed at 500 °C. The asymmetric supercapacitor fabricated CeO
2
//AC exhibited an energy density of 18 Wh kg
−1
at a power density of 833 W kg
−1
along with excellent rate capability. Further cyclic stability test conducted for 3000 cycles exhibited a capacitance retention of 93% which demonstrated the superior stability of the material. The observed electrochemical results demonstrated the potential of CeO
2
that paves way for the further involvement of these in the energy storage field.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-024-12900-1</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Annealing ; Capacitance ; Cerium oxides ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Crystallography ; Electrochemical analysis ; Electrode materials ; Electrodes ; Energy storage ; Materials Science ; Metal oxides ; Nanomaterials ; Optical and Electronic Materials ; Stability tests ; Supercapacitors ; Synthesis</subject><ispartof>Journal of materials science. Materials in electronics, 2024-06, Vol.35 (17), p.1153, Article 1153</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c200t-d5ebd9171fb7550b57e437e261bc6013e8630e21fc24955d33fcfe0cdfcf99853</cites><orcidid>0000-0002-1622-1049</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-024-12900-1$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-024-12900-1$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Lokhande, P. E.</creatorcontrib><creatorcontrib>Jagtap, Chaitali</creatorcontrib><creatorcontrib>Kadam, Vishal</creatorcontrib><creatorcontrib>Rednam, Udayabhaskar</creatorcontrib><creatorcontrib>Aepur, Radhamanohar</creatorcontrib><creatorcontrib>Tambe, Amol</creatorcontrib><creatorcontrib>Naushad, Mu</creatorcontrib><creatorcontrib>Thirumurugan, Arun</creatorcontrib><title>Electrochemical behaviour of microwave-assisted synthesized cerium oxide annealed at different temperatures</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>In the recent past, the electrode materials with high capacitance and excellent cycle stability have attracted the global scientific community for the development of novel advanced supercapacitors. In that context, rare earth metal oxides like Cerium Oxide (CeO
2
) have emerged as potential electrode material due to its characteristics such as prominent valency states, eco-friendly nature, abundance, and outstanding redox properties. The current study reports about the CeO
2
nanomaterial that is synthesized by microwave-assisted method followed by post-annealing at different temperatures and thereby examined for supercapacitor applications. The crystallographic and morphological study confirms the formation of CeO
2
nanoparticles and porous nature of the prepared materials. As annealing temperature was increased, the properties of CeO
2
changed and demonstrated different performance. The maximum specific capacitance of 656 Fg
−1
at 2 Ag
−1
was observed for the sample annealed at 500 °C. The asymmetric supercapacitor fabricated CeO
2
//AC exhibited an energy density of 18 Wh kg
−1
at a power density of 833 W kg
−1
along with excellent rate capability. Further cyclic stability test conducted for 3000 cycles exhibited a capacitance retention of 93% which demonstrated the superior stability of the material. The observed electrochemical results demonstrated the potential of CeO
2
that paves way for the further involvement of these in the energy storage field.</description><subject>Annealing</subject><subject>Capacitance</subject><subject>Cerium oxides</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Crystallography</subject><subject>Electrochemical analysis</subject><subject>Electrode materials</subject><subject>Electrodes</subject><subject>Energy storage</subject><subject>Materials Science</subject><subject>Metal oxides</subject><subject>Nanomaterials</subject><subject>Optical and Electronic Materials</subject><subject>Stability tests</subject><subject>Supercapacitors</subject><subject>Synthesis</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp9UE1LAzEUDKJgrf4BTwueoy_JZj-OUuoHFLwoeAvZ7Ivduh81yVbrrze6gjdP8xhm5jFDyDmDSwaQX3kGhUwp8JQyXgJQdkBmTOaCpgV_PiQzKGVOU8n5MTnxfgMAWSqKGXldtmiCG8wau8boNqlwrXfNMLpksEmk3PCud0i1940PWCd-34c1-uYz3gZdM3bJ8NHUmOi-R91GVoekbqxFh31IAnZbdDqMDv0pObK69Xj2i3PydLN8XNzR1cPt_eJ6RQ0HCLSWWNUly5mtcimhkjmmIkeescpkwAQWmQDkzBqellLWQlhjEUwdoSwLKebkYsrduuFtRB_UJvbp40slICvSEkTJo4pPqljRe4dWbV3TabdXDNT3qGoaVcVR1c-oikWTmEw-ivsXdH_R_7i-APEZfMQ</recordid><startdate>20240601</startdate><enddate>20240601</enddate><creator>Lokhande, P. 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E. ; Jagtap, Chaitali ; Kadam, Vishal ; Rednam, Udayabhaskar ; Aepur, Radhamanohar ; Tambe, Amol ; Naushad, Mu ; Thirumurugan, Arun</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c200t-d5ebd9171fb7550b57e437e261bc6013e8630e21fc24955d33fcfe0cdfcf99853</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Annealing</topic><topic>Capacitance</topic><topic>Cerium oxides</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Crystallography</topic><topic>Electrochemical analysis</topic><topic>Electrode materials</topic><topic>Electrodes</topic><topic>Energy storage</topic><topic>Materials Science</topic><topic>Metal oxides</topic><topic>Nanomaterials</topic><topic>Optical and Electronic Materials</topic><topic>Stability tests</topic><topic>Supercapacitors</topic><topic>Synthesis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Lokhande, P. E.</creatorcontrib><creatorcontrib>Jagtap, Chaitali</creatorcontrib><creatorcontrib>Kadam, Vishal</creatorcontrib><creatorcontrib>Rednam, Udayabhaskar</creatorcontrib><creatorcontrib>Aepur, Radhamanohar</creatorcontrib><creatorcontrib>Tambe, Amol</creatorcontrib><creatorcontrib>Naushad, Mu</creatorcontrib><creatorcontrib>Thirumurugan, Arun</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Lokhande, P. E.</au><au>Jagtap, Chaitali</au><au>Kadam, Vishal</au><au>Rednam, Udayabhaskar</au><au>Aepur, Radhamanohar</au><au>Tambe, Amol</au><au>Naushad, Mu</au><au>Thirumurugan, Arun</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Electrochemical behaviour of microwave-assisted synthesized cerium oxide annealed at different temperatures</atitle><jtitle>Journal of materials science. 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2
) have emerged as potential electrode material due to its characteristics such as prominent valency states, eco-friendly nature, abundance, and outstanding redox properties. The current study reports about the CeO
2
nanomaterial that is synthesized by microwave-assisted method followed by post-annealing at different temperatures and thereby examined for supercapacitor applications. The crystallographic and morphological study confirms the formation of CeO
2
nanoparticles and porous nature of the prepared materials. As annealing temperature was increased, the properties of CeO
2
changed and demonstrated different performance. The maximum specific capacitance of 656 Fg
−1
at 2 Ag
−1
was observed for the sample annealed at 500 °C. The asymmetric supercapacitor fabricated CeO
2
//AC exhibited an energy density of 18 Wh kg
−1
at a power density of 833 W kg
−1
along with excellent rate capability. Further cyclic stability test conducted for 3000 cycles exhibited a capacitance retention of 93% which demonstrated the superior stability of the material. The observed electrochemical results demonstrated the potential of CeO
2
that paves way for the further involvement of these in the energy storage field.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-024-12900-1</doi><orcidid>https://orcid.org/0000-0002-1622-1049</orcidid></addata></record> |
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| subjects | Annealing Capacitance Cerium oxides Characterization and Evaluation of Materials Chemistry and Materials Science Crystallography Electrochemical analysis Electrode materials Electrodes Energy storage Materials Science Metal oxides Nanomaterials Optical and Electronic Materials Stability tests Supercapacitors Synthesis |
| title | Electrochemical behaviour of microwave-assisted synthesized cerium oxide annealed at different temperatures |
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