Phosphorylation of 5-Amino-1H-1,2,4-triazoles with Diethyl Phosphorochloridate

Phosphorylation of 5-Amino-1H-1,2,4-triazoles with Diethyl Phosphorochloridate

New phosphorylated 5-amino-1 H -1,2,4-triazoles were obtained by the chemoselective reaction of diethyl phosphorochloridate with 5-amino-1 H -1,2,4-triazoles. The structure of the synthesized compounds was characterized by 1 H, 13 C, and 31 P NMR spectroscopy and mass spectrometry.

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Veröffentlicht in:Russian journal of general chemistry 2024, Vol.94 (1), p.66-72
Hauptverfasser: Voronina, D. Yu, Krylov, A. S., Tolstyakov, V. V., Dogadina, A. V.
Format: Artikel
Sprache:eng
Schlagworte:
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Mass spectrometry
NMR spectroscopy
Phosphorylation
Triazoles
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Zusammenfassung:New phosphorylated 5-amino-1 H -1,2,4-triazoles were obtained by the chemoselective reaction of diethyl phosphorochloridate with 5-amino-1 H -1,2,4-triazoles. The structure of the synthesized compounds was characterized by 1 H, 13 C, and 31 P NMR spectroscopy and mass spectrometry.
ISSN:1070-3632
1608-3350
DOI:10.1134/S1070363224010067