Molecularly imprinted sensor based on carboxylated carbon nanotubes/Keggin-type polyoxometalates nanocomposite for the detection of furazolidone
Due to its properties of mutagenic, teratogenic, and carcinogenic, the detection of furazolidone (FZD) in aquaculture is of great importance for food safety and human health. In this study, molecularly imprinted films modified with carboxylated multi-walled carbon nanotube-phosphomolybdic acid compo...
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| Veröffentlicht in: | Tungsten 2024-06, Vol.6 (2), p.394-409 |
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| creator | Huang, Yu-Lan Zhang, Bing Li, Yu-Lian Wang, Li Dong, Le Li, Jian |
| description | Due to its properties of mutagenic, teratogenic, and carcinogenic, the detection of furazolidone (FZD) in aquaculture is of great importance for food safety and human health. In this study, molecularly imprinted films modified with carboxylated multi-walled carbon nanotube-phosphomolybdic acid composite were used to fabricate an electrochemical sensor for the determination of FZD. The nanocomposites were characterized using infrared spectroscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray diffraction. The electrochemical characteristics of the modified electrodes were examined using electrochemical impedance spectroscopy, cyclic voltammetry, and differential pulse voltammetry. The sensor exhibited exceptional catalytic performance. The calibration curves were acquired in the concentration range of 6 nmol·L
−1
to 0.6 μmol·L
−1
, with a limit of detection of 3.38 nmol·L
−1
. Additionally, the sensor proved successful in recognizing FZD in shrimp samples with satisfactory recoveries and precision. The method provides a strategy to construct a molecularly imprinted electrochemical sensing platform using nanomaterials, which has great promise in the field of food safety. |
| doi_str_mv | 10.1007/s42864-023-00242-0 |
| format | Article |
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−1
to 0.6 μmol·L
−1
, with a limit of detection of 3.38 nmol·L
−1
. Additionally, the sensor proved successful in recognizing FZD in shrimp samples with satisfactory recoveries and precision. The method provides a strategy to construct a molecularly imprinted electrochemical sensing platform using nanomaterials, which has great promise in the field of food safety.</description><identifier>ISSN: 2661-8028</identifier><identifier>EISSN: 2661-8036</identifier><identifier>DOI: 10.1007/s42864-023-00242-0</identifier><language>eng</language><publisher>Singapore: Springer Nature Singapore</publisher><subject>Aquaculture ; Carbon ; Carcinogens ; Chemical sensors ; Chemistry and Materials Science ; Electrochemical impedance spectroscopy ; Electrodes ; Electrons ; Fourier transforms ; Graphene ; Infrared spectroscopy ; Materials Engineering ; Materials Science ; Metallic Materials ; Multi wall carbon nanotubes ; Nanocomposites ; Nanomaterials ; Nuclear Chemistry ; Original Paper ; Particle and Nuclear Physics ; Phosphomolybdic acid ; Polyoxometallates ; Potassium ; Sensors ; Sodium ; Spectrum analysis ; Sulfur ; Voltammetry</subject><ispartof>Tungsten, 2024-06, Vol.6 (2), p.394-409</ispartof><rights>The Nonferrous Metals Society of China 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c270t-90ca0247fc4ffd5b203880e6227003bbd4b9ca2cc597c0ad35f5db3e9c2521e63</cites><orcidid>0009-0005-8005-8812 ; 0000-0002-4835-7792 ; 0000-0002-3444-3788</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s42864-023-00242-0$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s42864-023-00242-0$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,776,780,27901,27902,41464,42533,51294</link.rule.ids></links><search><creatorcontrib>Huang, Yu-Lan</creatorcontrib><creatorcontrib>Zhang, Bing</creatorcontrib><creatorcontrib>Li, Yu-Lian</creatorcontrib><creatorcontrib>Wang, Li</creatorcontrib><creatorcontrib>Dong, Le</creatorcontrib><creatorcontrib>Li, Jian</creatorcontrib><title>Molecularly imprinted sensor based on carboxylated carbon nanotubes/Keggin-type polyoxometalates nanocomposite for the detection of furazolidone</title><title>Tungsten</title><addtitle>Tungsten</addtitle><description>Due to its properties of mutagenic, teratogenic, and carcinogenic, the detection of furazolidone (FZD) in aquaculture is of great importance for food safety and human health. In this study, molecularly imprinted films modified with carboxylated multi-walled carbon nanotube-phosphomolybdic acid composite were used to fabricate an electrochemical sensor for the determination of FZD. The nanocomposites were characterized using infrared spectroscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray diffraction. The electrochemical characteristics of the modified electrodes were examined using electrochemical impedance spectroscopy, cyclic voltammetry, and differential pulse voltammetry. The sensor exhibited exceptional catalytic performance. The calibration curves were acquired in the concentration range of 6 nmol·L
−1
to 0.6 μmol·L
−1
, with a limit of detection of 3.38 nmol·L
−1
. Additionally, the sensor proved successful in recognizing FZD in shrimp samples with satisfactory recoveries and precision. The method provides a strategy to construct a molecularly imprinted electrochemical sensing platform using nanomaterials, which has great promise in the field of food safety.</description><subject>Aquaculture</subject><subject>Carbon</subject><subject>Carcinogens</subject><subject>Chemical sensors</subject><subject>Chemistry and Materials Science</subject><subject>Electrochemical impedance spectroscopy</subject><subject>Electrodes</subject><subject>Electrons</subject><subject>Fourier transforms</subject><subject>Graphene</subject><subject>Infrared spectroscopy</subject><subject>Materials Engineering</subject><subject>Materials Science</subject><subject>Metallic Materials</subject><subject>Multi wall carbon nanotubes</subject><subject>Nanocomposites</subject><subject>Nanomaterials</subject><subject>Nuclear Chemistry</subject><subject>Original Paper</subject><subject>Particle and Nuclear Physics</subject><subject>Phosphomolybdic acid</subject><subject>Polyoxometallates</subject><subject>Potassium</subject><subject>Sensors</subject><subject>Sodium</subject><subject>Spectrum analysis</subject><subject>Sulfur</subject><subject>Voltammetry</subject><issn>2661-8028</issn><issn>2661-8036</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp9kMtOwzAQRSMEElXpD7CyxDp0Yue5RBUvUcQG1pbjjEuq1A62IzV8BZ-M0yLYsbJHc-61fKLoMoHrBKBYupSWeRoDZTEATWkMJ9GM5nkSl8Dy0987Lc-jhXNbCFRWQUKLWfT1bDqUQydsN5J219tWe2yIQ-2MJbVwYTCaSGFrsx87MS0PgyZaaOOHGt3yCTebVsd-7JH0phvN3uzQi4l2B0yaXW9c65Go0OrfkTToUfo21BhF1GDFp-naxmi8iM6U6Bwufs559HZ3-7p6iNcv94-rm3UsaQE-rkCK8NdCyVSpJqspsLIEzGnYAqvrJq0rKaiUWVVIEA3LVNbUDCtJM5pgzubR1bG3t-ZjQOf51gxWhyc5rQrG0iLPWaDokZLWOGdR8WBoJ-zIE-CTfH6Uz4N8fpDPIYTYMeQmnRu0f9X_pL4B2yOLyw</recordid><startdate>20240601</startdate><enddate>20240601</enddate><creator>Huang, Yu-Lan</creator><creator>Zhang, Bing</creator><creator>Li, Yu-Lian</creator><creator>Wang, Li</creator><creator>Dong, Le</creator><creator>Li, Jian</creator><general>Springer Nature Singapore</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><orcidid>https://orcid.org/0009-0005-8005-8812</orcidid><orcidid>https://orcid.org/0000-0002-4835-7792</orcidid><orcidid>https://orcid.org/0000-0002-3444-3788</orcidid></search><sort><creationdate>20240601</creationdate><title>Molecularly imprinted sensor based on carboxylated carbon nanotubes/Keggin-type polyoxometalates nanocomposite for the detection of furazolidone</title><author>Huang, Yu-Lan ; Zhang, Bing ; Li, Yu-Lian ; Wang, Li ; Dong, Le ; Li, Jian</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c270t-90ca0247fc4ffd5b203880e6227003bbd4b9ca2cc597c0ad35f5db3e9c2521e63</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Aquaculture</topic><topic>Carbon</topic><topic>Carcinogens</topic><topic>Chemical sensors</topic><topic>Chemistry and Materials Science</topic><topic>Electrochemical impedance spectroscopy</topic><topic>Electrodes</topic><topic>Electrons</topic><topic>Fourier transforms</topic><topic>Graphene</topic><topic>Infrared spectroscopy</topic><topic>Materials Engineering</topic><topic>Materials Science</topic><topic>Metallic Materials</topic><topic>Multi wall carbon nanotubes</topic><topic>Nanocomposites</topic><topic>Nanomaterials</topic><topic>Nuclear Chemistry</topic><topic>Original Paper</topic><topic>Particle and Nuclear Physics</topic><topic>Phosphomolybdic acid</topic><topic>Polyoxometallates</topic><topic>Potassium</topic><topic>Sensors</topic><topic>Sodium</topic><topic>Spectrum analysis</topic><topic>Sulfur</topic><topic>Voltammetry</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Huang, Yu-Lan</creatorcontrib><creatorcontrib>Zhang, Bing</creatorcontrib><creatorcontrib>Li, Yu-Lian</creatorcontrib><creatorcontrib>Wang, Li</creatorcontrib><creatorcontrib>Dong, Le</creatorcontrib><creatorcontrib>Li, Jian</creatorcontrib><collection>CrossRef</collection><jtitle>Tungsten</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Huang, Yu-Lan</au><au>Zhang, Bing</au><au>Li, Yu-Lian</au><au>Wang, Li</au><au>Dong, Le</au><au>Li, Jian</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Molecularly imprinted sensor based on carboxylated carbon nanotubes/Keggin-type polyoxometalates nanocomposite for the detection of furazolidone</atitle><jtitle>Tungsten</jtitle><stitle>Tungsten</stitle><date>2024-06-01</date><risdate>2024</risdate><volume>6</volume><issue>2</issue><spage>394</spage><epage>409</epage><pages>394-409</pages><issn>2661-8028</issn><eissn>2661-8036</eissn><abstract>Due to its properties of mutagenic, teratogenic, and carcinogenic, the detection of furazolidone (FZD) in aquaculture is of great importance for food safety and human health. In this study, molecularly imprinted films modified with carboxylated multi-walled carbon nanotube-phosphomolybdic acid composite were used to fabricate an electrochemical sensor for the determination of FZD. The nanocomposites were characterized using infrared spectroscopy, scanning electron microscopy, energy-dispersive X-ray spectroscopy, and X-ray diffraction. The electrochemical characteristics of the modified electrodes were examined using electrochemical impedance spectroscopy, cyclic voltammetry, and differential pulse voltammetry. The sensor exhibited exceptional catalytic performance. The calibration curves were acquired in the concentration range of 6 nmol·L
−1
to 0.6 μmol·L
−1
, with a limit of detection of 3.38 nmol·L
−1
. Additionally, the sensor proved successful in recognizing FZD in shrimp samples with satisfactory recoveries and precision. The method provides a strategy to construct a molecularly imprinted electrochemical sensing platform using nanomaterials, which has great promise in the field of food safety.</abstract><cop>Singapore</cop><pub>Springer Nature Singapore</pub><doi>10.1007/s42864-023-00242-0</doi><tpages>16</tpages><orcidid>https://orcid.org/0009-0005-8005-8812</orcidid><orcidid>https://orcid.org/0000-0002-4835-7792</orcidid><orcidid>https://orcid.org/0000-0002-3444-3788</orcidid></addata></record> |
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| subjects | Aquaculture Carbon Carcinogens Chemical sensors Chemistry and Materials Science Electrochemical impedance spectroscopy Electrodes Electrons Fourier transforms Graphene Infrared spectroscopy Materials Engineering Materials Science Metallic Materials Multi wall carbon nanotubes Nanocomposites Nanomaterials Nuclear Chemistry Original Paper Particle and Nuclear Physics Phosphomolybdic acid Polyoxometallates Potassium Sensors Sodium Spectrum analysis Sulfur Voltammetry |
| title | Molecularly imprinted sensor based on carboxylated carbon nanotubes/Keggin-type polyoxometalates nanocomposite for the detection of furazolidone |
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