Synthesis of Precursors of Complex Oxide Systems Al2O3–ZrO2–MxOy (M = La, Y, Ce) Using Electrogenerated Reagents and Their Physical and Chemical Properties
The scientific bases for the synthesis of precursors of nanostructured Al 2 O 3 –ZrO 2 –M x O y (M = La, Y, Ce) oxide systems are developed. The features of the formation of precursors of such systems under conditions of rapid mixing of electrically generated reagents, implemented in a diaphragmless...
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| Veröffentlicht in: | Glass physics and chemistry 2023-12, Vol.49 (Suppl 1), p.S28-S34 |
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| container_end_page | S34 |
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| container_issue | Suppl 1 |
| container_start_page | S28 |
| container_title | Glass physics and chemistry |
| container_volume | 49 |
| creator | Dresvyannikov, A. F. Petrova, E. V. Kashfrazyeva, L. I. Khairullina, A. I. |
| description | The scientific bases for the synthesis of precursors of nanostructured Al
2
O
3
–ZrO
2
–M
x
O
y
(M = La, Y, Ce) oxide systems are developed. The features of the formation of precursors of such systems under conditions of rapid mixing of electrically generated reagents, implemented in a diaphragmless coaxial electrolyzer reactor, are studied. Using the methods of potentiodynamic polarization curves, X-ray diffractometry, X-ray fluorescence, synchronous thermal analysis, and laser diffraction, the anodic processes occurring in the electrolyzer and the morphology of particles formed in solution and transformed during heat treatment, as well as the phase, granulometric, and elemental compositions of precursors and oxide systems, are studied. The proposed approach makes it possible to obtain oxide systems modified with rare earth elements based on the Al
2
O
3
–ZrO
2
binary system, characterized by the presence of a tetragonal zirconium dioxide phase in them. |
| doi_str_mv | 10.1134/S108765962360103X |
| format | Article |
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2
O
3
–ZrO
2
–M
x
O
y
(M = La, Y, Ce) oxide systems are developed. The features of the formation of precursors of such systems under conditions of rapid mixing of electrically generated reagents, implemented in a diaphragmless coaxial electrolyzer reactor, are studied. Using the methods of potentiodynamic polarization curves, X-ray diffractometry, X-ray fluorescence, synchronous thermal analysis, and laser diffraction, the anodic processes occurring in the electrolyzer and the morphology of particles formed in solution and transformed during heat treatment, as well as the phase, granulometric, and elemental compositions of precursors and oxide systems, are studied. The proposed approach makes it possible to obtain oxide systems modified with rare earth elements based on the Al
2
O
3
–ZrO
2
binary system, characterized by the presence of a tetragonal zirconium dioxide phase in them.</description><identifier>ISSN: 1087-6596</identifier><identifier>EISSN: 1608-313X</identifier><identifier>DOI: 10.1134/S108765962360103X</identifier><language>eng</language><publisher>Moscow: Pleiades Publishing</publisher><subject>Aluminum oxide ; Ceramics ; Cerium ; Characterization and Evaluation of Materials ; Chemical properties ; Chemistry and Materials Science ; Composites ; Glass ; Heat treatment ; Lanthanum ; Materials Science ; Natural Materials ; Physical Chemistry ; Precursors ; Rare earth elements ; Reagents ; Synthesis ; Thermal analysis ; X-ray fluorescence ; Zirconium dioxide</subject><ispartof>Glass physics and chemistry, 2023-12, Vol.49 (Suppl 1), p.S28-S34</ispartof><rights>Pleiades Publishing, Ltd. 2023. ISSN 1087-6596, Glass Physics and Chemistry, 2023, Vol. 49, Suppl. 1, pp. S28–S34. © Pleiades Publishing, Ltd., 2023.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c268t-ed73db0e063d4829808e89166e840d14e5a10d5effc296e3221f55f274b71dfe3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1134/S108765962360103X$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1134/S108765962360103X$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27922,27923,41486,42555,51317</link.rule.ids></links><search><creatorcontrib>Dresvyannikov, A. F.</creatorcontrib><creatorcontrib>Petrova, E. V.</creatorcontrib><creatorcontrib>Kashfrazyeva, L. I.</creatorcontrib><creatorcontrib>Khairullina, A. I.</creatorcontrib><title>Synthesis of Precursors of Complex Oxide Systems Al2O3–ZrO2–MxOy (M = La, Y, Ce) Using Electrogenerated Reagents and Their Physical and Chemical Properties</title><title>Glass physics and chemistry</title><addtitle>Glass Phys Chem</addtitle><description>The scientific bases for the synthesis of precursors of nanostructured Al
2
O
3
–ZrO
2
–M
x
O
y
(M = La, Y, Ce) oxide systems are developed. The features of the formation of precursors of such systems under conditions of rapid mixing of electrically generated reagents, implemented in a diaphragmless coaxial electrolyzer reactor, are studied. Using the methods of potentiodynamic polarization curves, X-ray diffractometry, X-ray fluorescence, synchronous thermal analysis, and laser diffraction, the anodic processes occurring in the electrolyzer and the morphology of particles formed in solution and transformed during heat treatment, as well as the phase, granulometric, and elemental compositions of precursors and oxide systems, are studied. The proposed approach makes it possible to obtain oxide systems modified with rare earth elements based on the Al
2
O
3
–ZrO
2
binary system, characterized by the presence of a tetragonal zirconium dioxide phase in them.</description><subject>Aluminum oxide</subject><subject>Ceramics</subject><subject>Cerium</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical properties</subject><subject>Chemistry and Materials Science</subject><subject>Composites</subject><subject>Glass</subject><subject>Heat treatment</subject><subject>Lanthanum</subject><subject>Materials Science</subject><subject>Natural Materials</subject><subject>Physical Chemistry</subject><subject>Precursors</subject><subject>Rare earth elements</subject><subject>Reagents</subject><subject>Synthesis</subject><subject>Thermal analysis</subject><subject>X-ray fluorescence</subject><subject>Zirconium dioxide</subject><issn>1087-6596</issn><issn>1608-313X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><recordid>eNp1UctKw0AUHUTBWv0AdwNuFBqdRzJJFi4k1Ae0pNgWqpuQZm6alDQTZ1Jodv6DH-C_-SWmreBCXN177nncxUHonJJrSrl9M6bEc4XjC8YFoYTPDlCHCuJZnPLZYbu3tLXlj9GJMUtCiO-6dgd9jpuyzsDkBqsUjzQka22U3qFAraoCNjjc5BLwuDE1rAy-K1jIv94_XnXI2jHchA2-HOJbPIh7-KWHA7jCU5OXC9wvIKm1WkAJOq5B4meIW1AbHJcSTzLINR5ljcmTuNidggxWOzDSqgJd52BO0VEaFwbOfmYXTe_7k-DRGoQPT8HdwEqY8GoLpMvlnAARXNoe8z3igedTIcCziaQ2ODEl0oE0TZgvgDNGU8dJmWvPXSpT4F10sc-ttHpbg6mjpVrrsn0ZMd-xGSOE0VZF96pEK2M0pFGl81Wsm4iSaNtD9KeH1sP2HtNqywXo3-T_Td9_2ouU</recordid><startdate>20231201</startdate><enddate>20231201</enddate><creator>Dresvyannikov, A. F.</creator><creator>Petrova, E. V.</creator><creator>Kashfrazyeva, L. I.</creator><creator>Khairullina, A. I.</creator><general>Pleiades Publishing</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7QQ</scope><scope>7SR</scope><scope>8FD</scope><scope>JG9</scope></search><sort><creationdate>20231201</creationdate><title>Synthesis of Precursors of Complex Oxide Systems Al2O3–ZrO2–MxOy (M = La, Y, Ce) Using Electrogenerated Reagents and Their Physical and Chemical Properties</title><author>Dresvyannikov, A. F. ; Petrova, E. V. ; Kashfrazyeva, L. I. ; Khairullina, A. I.</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c268t-ed73db0e063d4829808e89166e840d14e5a10d5effc296e3221f55f274b71dfe3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Aluminum oxide</topic><topic>Ceramics</topic><topic>Cerium</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical properties</topic><topic>Chemistry and Materials Science</topic><topic>Composites</topic><topic>Glass</topic><topic>Heat treatment</topic><topic>Lanthanum</topic><topic>Materials Science</topic><topic>Natural Materials</topic><topic>Physical Chemistry</topic><topic>Precursors</topic><topic>Rare earth elements</topic><topic>Reagents</topic><topic>Synthesis</topic><topic>Thermal analysis</topic><topic>X-ray fluorescence</topic><topic>Zirconium dioxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Dresvyannikov, A. F.</creatorcontrib><creatorcontrib>Petrova, E. V.</creatorcontrib><creatorcontrib>Kashfrazyeva, L. I.</creatorcontrib><creatorcontrib>Khairullina, A. I.</creatorcontrib><collection>CrossRef</collection><collection>Ceramic Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>Technology Research Database</collection><collection>Materials Research Database</collection><jtitle>Glass physics and chemistry</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Dresvyannikov, A. F.</au><au>Petrova, E. V.</au><au>Kashfrazyeva, L. I.</au><au>Khairullina, A. I.</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis of Precursors of Complex Oxide Systems Al2O3–ZrO2–MxOy (M = La, Y, Ce) Using Electrogenerated Reagents and Their Physical and Chemical Properties</atitle><jtitle>Glass physics and chemistry</jtitle><stitle>Glass Phys Chem</stitle><date>2023-12-01</date><risdate>2023</risdate><volume>49</volume><issue>Suppl 1</issue><spage>S28</spage><epage>S34</epage><pages>S28-S34</pages><issn>1087-6596</issn><eissn>1608-313X</eissn><abstract>The scientific bases for the synthesis of precursors of nanostructured Al
2
O
3
–ZrO
2
–M
x
O
y
(M = La, Y, Ce) oxide systems are developed. The features of the formation of precursors of such systems under conditions of rapid mixing of electrically generated reagents, implemented in a diaphragmless coaxial electrolyzer reactor, are studied. Using the methods of potentiodynamic polarization curves, X-ray diffractometry, X-ray fluorescence, synchronous thermal analysis, and laser diffraction, the anodic processes occurring in the electrolyzer and the morphology of particles formed in solution and transformed during heat treatment, as well as the phase, granulometric, and elemental compositions of precursors and oxide systems, are studied. The proposed approach makes it possible to obtain oxide systems modified with rare earth elements based on the Al
2
O
3
–ZrO
2
binary system, characterized by the presence of a tetragonal zirconium dioxide phase in them.</abstract><cop>Moscow</cop><pub>Pleiades Publishing</pub><doi>10.1134/S108765962360103X</doi></addata></record> |
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| ispartof | Glass physics and chemistry, 2023-12, Vol.49 (Suppl 1), p.S28-S34 |
| issn | 1087-6596 1608-313X |
| language | eng |
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| source | SpringerLink Journals - AutoHoldings |
| subjects | Aluminum oxide Ceramics Cerium Characterization and Evaluation of Materials Chemical properties Chemistry and Materials Science Composites Glass Heat treatment Lanthanum Materials Science Natural Materials Physical Chemistry Precursors Rare earth elements Reagents Synthesis Thermal analysis X-ray fluorescence Zirconium dioxide |
| title | Synthesis of Precursors of Complex Oxide Systems Al2O3–ZrO2–MxOy (M = La, Y, Ce) Using Electrogenerated Reagents and Their Physical and Chemical Properties |
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