Laser power modulated microstructure evolution, phase transformation and mechanical properties in NiTi fabricated by laser powder bed fusion

In this study, two sets of optimized laser powder bed fusion (LPBF) additive manufacturing parameters with similar energy density but different laser powers (HP: high laser power with high scanning speed, LP: low laser power with low scanning speed) were used to produce fully dense and crack-free Ni...

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Veröffentlicht in:Journal of alloys and compounds 2021-04, Vol.861, p.157959, Article 157959
Hauptverfasser: Chen, Wenliang, Yang, Qin, Huang, Shuke, Huang, Shiyang, Kruzic, Jamie J., Li, Xiaopeng
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container_start_page 157959
container_title Journal of alloys and compounds
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creator Chen, Wenliang
Yang, Qin
Huang, Shuke
Huang, Shiyang
Kruzic, Jamie J.
Li, Xiaopeng
description In this study, two sets of optimized laser powder bed fusion (LPBF) additive manufacturing parameters with similar energy density but different laser powers (HP: high laser power with high scanning speed, LP: low laser power with low scanning speed) were used to produce fully dense and crack-free NiTi samples. The microstructure, phase transformation and mechanical properties of the LPBF fabricated HP and LP NiTi were investigated using scanning electron microscopy (SEM), differential scanning calorimeter (DSC), X-ray diffraction (XRD) and dynamic mechanical analysis (DMA). The results showed that the HP and LP NiTi samples had different microstructures, phase transformation temperatures and mechanical properties. It was found that the HP NiTi samples predominantly contained austenite at room temperature and exhibited lower phase transformation temperatures. In contrast, the LP NiTi samples contained a large amount of martensite and had larger thermal memory recovery and better damping capacity. Additionally, the microstructure, phase transformation temperatures and mechanical properties were found to vary at different locations along the building direction in both HP and LP NiTi. This study implies that by manipulating the LPBF processing parameters, in particular the laser power, the phase transformation, microstructure and dynamic mechanical properties of the LPBF fabricated NiTi can be controlled to target different applications. •High and low laser power can be used to fabricate fully dense NiTi by LPBF.•High power LPBF NiTi forms austenite with lower phase transformation temperatures.•Low power LPBF fabricated NiTi forms martensite with better damping capacity.•Different regions in NiTi have different microstructures and mechanical properties.
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The microstructure, phase transformation and mechanical properties of the LPBF fabricated HP and LP NiTi were investigated using scanning electron microscopy (SEM), differential scanning calorimeter (DSC), X-ray diffraction (XRD) and dynamic mechanical analysis (DMA). The results showed that the HP and LP NiTi samples had different microstructures, phase transformation temperatures and mechanical properties. It was found that the HP NiTi samples predominantly contained austenite at room temperature and exhibited lower phase transformation temperatures. In contrast, the LP NiTi samples contained a large amount of martensite and had larger thermal memory recovery and better damping capacity. Additionally, the microstructure, phase transformation temperatures and mechanical properties were found to vary at different locations along the building direction in both HP and LP NiTi. This study implies that by manipulating the LPBF processing parameters, in particular the laser power, the phase transformation, microstructure and dynamic mechanical properties of the LPBF fabricated NiTi can be controlled to target different applications. •High and low laser power can be used to fabricate fully dense NiTi by LPBF.•High power LPBF NiTi forms austenite with lower phase transformation temperatures.•Low power LPBF fabricated NiTi forms martensite with better damping capacity.•Different regions in NiTi have different microstructures and mechanical properties.</description><identifier>ISSN: 0925-8388</identifier><identifier>EISSN: 1873-4669</identifier><identifier>DOI: 10.1016/j.jallcom.2020.157959</identifier><language>eng</language><publisher>Lausanne: Elsevier B.V</publisher><subject>Additive manufacturing ; Damping capacity ; Dynamic mechanical analysis ; Dynamic mechanical properties ; Flux density ; Heat treating ; Intermetallic compounds ; Laser powder bed fusion ; Lasers ; Martensite ; Mechanical properties ; Microstructure ; Nickel titanides ; NiTi shape memory alloy ; Phase transformation ; Phase transitions ; Powder beds ; Process parameters ; Room temperature ; Transformation temperature</subject><ispartof>Journal of alloys and compounds, 2021-04, Vol.861, p.157959, Article 157959</ispartof><rights>2020 Elsevier B.V.</rights><rights>Copyright Elsevier BV Apr 25, 2021</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c384t-afda9abfa59c0485d28994cdbd1e8f5a0b65cfd4d14bf52723bafdc86527c8823</citedby><cites>FETCH-LOGICAL-c384t-afda9abfa59c0485d28994cdbd1e8f5a0b65cfd4d14bf52723bafdc86527c8823</cites><orcidid>0000-0002-9695-1921</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.sciencedirect.com/science/article/pii/S0925838820343231$$EHTML$$P50$$Gelsevier$$H</linktohtml><link.rule.ids>314,776,780,3537,27901,27902,65306</link.rule.ids></links><search><creatorcontrib>Chen, Wenliang</creatorcontrib><creatorcontrib>Yang, Qin</creatorcontrib><creatorcontrib>Huang, Shuke</creatorcontrib><creatorcontrib>Huang, Shiyang</creatorcontrib><creatorcontrib>Kruzic, Jamie J.</creatorcontrib><creatorcontrib>Li, Xiaopeng</creatorcontrib><title>Laser power modulated microstructure evolution, phase transformation and mechanical properties in NiTi fabricated by laser powder bed fusion</title><title>Journal of alloys and compounds</title><description>In this study, two sets of optimized laser powder bed fusion (LPBF) additive manufacturing parameters with similar energy density but different laser powers (HP: high laser power with high scanning speed, LP: low laser power with low scanning speed) were used to produce fully dense and crack-free NiTi samples. The microstructure, phase transformation and mechanical properties of the LPBF fabricated HP and LP NiTi were investigated using scanning electron microscopy (SEM), differential scanning calorimeter (DSC), X-ray diffraction (XRD) and dynamic mechanical analysis (DMA). The results showed that the HP and LP NiTi samples had different microstructures, phase transformation temperatures and mechanical properties. It was found that the HP NiTi samples predominantly contained austenite at room temperature and exhibited lower phase transformation temperatures. In contrast, the LP NiTi samples contained a large amount of martensite and had larger thermal memory recovery and better damping capacity. Additionally, the microstructure, phase transformation temperatures and mechanical properties were found to vary at different locations along the building direction in both HP and LP NiTi. 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This study implies that by manipulating the LPBF processing parameters, in particular the laser power, the phase transformation, microstructure and dynamic mechanical properties of the LPBF fabricated NiTi can be controlled to target different applications. •High and low laser power can be used to fabricate fully dense NiTi by LPBF.•High power LPBF NiTi forms austenite with lower phase transformation temperatures.•Low power LPBF fabricated NiTi forms martensite with better damping capacity.•Different regions in NiTi have different microstructures and mechanical properties.</abstract><cop>Lausanne</cop><pub>Elsevier B.V</pub><doi>10.1016/j.jallcom.2020.157959</doi><orcidid>https://orcid.org/0000-0002-9695-1921</orcidid><oa>free_for_read</oa></addata></record>
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subjects Additive manufacturing
Damping capacity
Dynamic mechanical analysis
Dynamic mechanical properties
Flux density
Heat treating
Intermetallic compounds
Laser powder bed fusion
Lasers
Martensite
Mechanical properties
Microstructure
Nickel titanides
NiTi shape memory alloy
Phase transformation
Phase transitions
Powder beds
Process parameters
Room temperature
Transformation temperature
title Laser power modulated microstructure evolution, phase transformation and mechanical properties in NiTi fabricated by laser powder bed fusion
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