Synthesis and characterization of activated carbon produced from waste human hair mass using chemical activation
In this study, hair waste was converted into active carbon for the first time and its characteristics were analyzed. As chemical activation tool, zinc chloride (ZnCl 2 ) was impregnated and then carbonized under different temperatures (250–300 °C). Scanning Electron Microscope (SEM) images showed an...
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| Veröffentlicht in: | Carbon Letters 2020-06, Vol.30 (3), p.307-313 |
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| creator | Bal Altuntaş, Derya Nevruzoğlu, Vagif Dokumacı, Meryem Cam, Şafak |
| description | In this study, hair waste was converted into active carbon for the first time and its characteristics were analyzed. As chemical activation tool, zinc chloride (ZnCl
2
) was impregnated and then carbonized under different temperatures (250–300 °C). Scanning Electron Microscope (SEM) images showed an increase in the pore density, radius and volume of pores. X-ray diffraction analysis (XRD) showed that the samples had an amorphous structure. In Fourier-transform infrared (FT-IR) spectroscope analysis, C=C and N–H vibrations observed in 1515–1520 cm
−1
wave number of protein molecules were found to disappear with the increase in temperature. With Raman spectroscopy, the behaviors of D peak at 1344 cm
−1
wave number and G peak at 1566 cm
−1
wave number expressing structure layout in carbonized structures were analyzed depending on the temperatures. Between these intensities, (
I
D
/
I
G
) the rate was found to differ in direct proportion to temperature. XRD spectrums showed that the samples are converted into a more irregular crystal structure. All these results implied that the waste hair mass could be used as an adsorbant material. |
| doi_str_mv | 10.1007/s42823-019-00099-9 |
| format | Article |
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2
) was impregnated and then carbonized under different temperatures (250–300 °C). Scanning Electron Microscope (SEM) images showed an increase in the pore density, radius and volume of pores. X-ray diffraction analysis (XRD) showed that the samples had an amorphous structure. In Fourier-transform infrared (FT-IR) spectroscope analysis, C=C and N–H vibrations observed in 1515–1520 cm
−1
wave number of protein molecules were found to disappear with the increase in temperature. With Raman spectroscopy, the behaviors of D peak at 1344 cm
−1
wave number and G peak at 1566 cm
−1
wave number expressing structure layout in carbonized structures were analyzed depending on the temperatures. Between these intensities, (
I
D
/
I
G
) the rate was found to differ in direct proportion to temperature. XRD spectrums showed that the samples are converted into a more irregular crystal structure. All these results implied that the waste hair mass could be used as an adsorbant material.</description><identifier>ISSN: 1976-4251</identifier><identifier>EISSN: 2233-4998</identifier><identifier>DOI: 10.1007/s42823-019-00099-9</identifier><language>eng</language><publisher>Singapore: Springer Singapore</publisher><subject>Activated carbon ; Carbon ; Characterization and Evaluation of Materials ; Chemical bonds ; Chemistry and Materials Science ; Crystal structure ; Fourier transforms ; Hair ; Immunoglobulins ; Infrared analysis ; Infrared spectroscopy ; Keratin ; Materials Engineering ; Materials Science ; Morphology ; Nanotechnology ; Original Article ; Raman spectroscopy ; Scanning electron microscopy ; Spectrum analysis ; Sulfur ; Temperature ; Vibrations ; Wavelengths ; X-ray diffraction ; Zinc chloride</subject><ispartof>Carbon Letters, 2020-06, Vol.30 (3), p.307-313</ispartof><rights>Korean Carbon Society 2019</rights><rights>Korean Carbon Society 2019.</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c347t-de14e01fb0957867c7920377f50eb231332d47c0121afc189cc1737b69029c3b3</citedby><cites>FETCH-LOGICAL-c347t-de14e01fb0957867c7920377f50eb231332d47c0121afc189cc1737b69029c3b3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.proquest.com/docview/2933465235?pq-origsite=primo$$EHTML$$P50$$Gproquest$$H</linktohtml><link.rule.ids>314,780,784,21387,21388,21389,21390,23255,27923,27924,33529,33702,33743,34004,34313,43658,43786,43804,43952,44066,64384,64388,72240</link.rule.ids></links><search><creatorcontrib>Bal Altuntaş, Derya</creatorcontrib><creatorcontrib>Nevruzoğlu, Vagif</creatorcontrib><creatorcontrib>Dokumacı, Meryem</creatorcontrib><creatorcontrib>Cam, Şafak</creatorcontrib><title>Synthesis and characterization of activated carbon produced from waste human hair mass using chemical activation</title><title>Carbon Letters</title><addtitle>Carbon Lett</addtitle><description>In this study, hair waste was converted into active carbon for the first time and its characteristics were analyzed. As chemical activation tool, zinc chloride (ZnCl
2
) was impregnated and then carbonized under different temperatures (250–300 °C). Scanning Electron Microscope (SEM) images showed an increase in the pore density, radius and volume of pores. X-ray diffraction analysis (XRD) showed that the samples had an amorphous structure. In Fourier-transform infrared (FT-IR) spectroscope analysis, C=C and N–H vibrations observed in 1515–1520 cm
−1
wave number of protein molecules were found to disappear with the increase in temperature. With Raman spectroscopy, the behaviors of D peak at 1344 cm
−1
wave number and G peak at 1566 cm
−1
wave number expressing structure layout in carbonized structures were analyzed depending on the temperatures. Between these intensities, (
I
D
/
I
G
) the rate was found to differ in direct proportion to temperature. XRD spectrums showed that the samples are converted into a more irregular crystal structure. All these results implied that the waste hair mass could be used as an adsorbant material.</description><subject>Activated carbon</subject><subject>Carbon</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical bonds</subject><subject>Chemistry and Materials Science</subject><subject>Crystal structure</subject><subject>Fourier transforms</subject><subject>Hair</subject><subject>Immunoglobulins</subject><subject>Infrared analysis</subject><subject>Infrared spectroscopy</subject><subject>Keratin</subject><subject>Materials Engineering</subject><subject>Materials Science</subject><subject>Morphology</subject><subject>Nanotechnology</subject><subject>Original Article</subject><subject>Raman spectroscopy</subject><subject>Scanning electron microscopy</subject><subject>Spectrum analysis</subject><subject>Sulfur</subject><subject>Temperature</subject><subject>Vibrations</subject><subject>Wavelengths</subject><subject>X-ray diffraction</subject><subject>Zinc chloride</subject><issn>1976-4251</issn><issn>2233-4998</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2020</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp9kc1KxDAURoMoOIzzAq4Crqs3uW3TLGXwDwZcqOuQpuk0Om3HpFXGpzdaZVy5Cjc537mBj5BTBucMQFyElBccE2AyAQApE3lAZpwjJqmUxSGZMSnyJOUZOyaLEFwZQwgSMJ-R7cOuGxobXKC6q6hptNdmsN596MH1He1rGmf3pgcbX7Uv493W99Vo4lz7vqXvOgyWNmOrO9po52mrQ6BjcN066mzrjN78OqLxhBzVehPs4ueck6frq8flbbK6v7lbXq4Sg6kYksqy1AKrS5CZKHJhhOSAQtQZ2JIjQ-RVKgwwznRtWCGNYQJFmUvg0mCJc3I2eeNvX0cbBvXcj76LKxWXiGmeccz21EvvrQ6m6Tfa78mUQ8bySPGJMr4Pwdtabb1rtd8pBuqrAjVVoGIF6rsCJWMIp1CIcLe2f7T_pD4BhM2J9w</recordid><startdate>20200601</startdate><enddate>20200601</enddate><creator>Bal Altuntaş, Derya</creator><creator>Nevruzoğlu, Vagif</creator><creator>Dokumacı, Meryem</creator><creator>Cam, Şafak</creator><general>Springer Singapore</general><general>한국탄소학회</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>KROLR</scope><scope>3V.</scope><scope>7XB</scope><scope>88I</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M2P</scope><scope>M7S</scope><scope>PATMY</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><scope>PYCSY</scope><scope>Q9U</scope></search><sort><creationdate>20200601</creationdate><title>Synthesis and characterization of activated carbon produced from waste human hair mass using chemical activation</title><author>Bal Altuntaş, Derya ; Nevruzoğlu, Vagif ; Dokumacı, Meryem ; Cam, Şafak</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c347t-de14e01fb0957867c7920377f50eb231332d47c0121afc189cc1737b69029c3b3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2020</creationdate><topic>Activated carbon</topic><topic>Carbon</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical bonds</topic><topic>Chemistry and Materials Science</topic><topic>Crystal structure</topic><topic>Fourier transforms</topic><topic>Hair</topic><topic>Immunoglobulins</topic><topic>Infrared analysis</topic><topic>Infrared spectroscopy</topic><topic>Keratin</topic><topic>Materials Engineering</topic><topic>Materials Science</topic><topic>Morphology</topic><topic>Nanotechnology</topic><topic>Original Article</topic><topic>Raman spectroscopy</topic><topic>Scanning electron microscopy</topic><topic>Spectrum analysis</topic><topic>Sulfur</topic><topic>Temperature</topic><topic>Vibrations</topic><topic>Wavelengths</topic><topic>X-ray diffraction</topic><topic>Zinc chloride</topic><toplevel>online_resources</toplevel><creatorcontrib>Bal Altuntaş, Derya</creatorcontrib><creatorcontrib>Nevruzoğlu, Vagif</creatorcontrib><creatorcontrib>Dokumacı, Meryem</creatorcontrib><creatorcontrib>Cam, Şafak</creatorcontrib><collection>CrossRef</collection><collection>Korea Scholar</collection><collection>ProQuest Central (Corporate)</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Science Database (Alumni Edition)</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Science Database</collection><collection>Engineering Database</collection><collection>Environmental Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><collection>Environmental Science Collection</collection><collection>ProQuest Central Basic</collection><jtitle>Carbon Letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bal Altuntaş, Derya</au><au>Nevruzoğlu, Vagif</au><au>Dokumacı, Meryem</au><au>Cam, Şafak</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and characterization of activated carbon produced from waste human hair mass using chemical activation</atitle><jtitle>Carbon Letters</jtitle><stitle>Carbon Lett</stitle><date>2020-06-01</date><risdate>2020</risdate><volume>30</volume><issue>3</issue><spage>307</spage><epage>313</epage><pages>307-313</pages><issn>1976-4251</issn><eissn>2233-4998</eissn><abstract>In this study, hair waste was converted into active carbon for the first time and its characteristics were analyzed. As chemical activation tool, zinc chloride (ZnCl
2
) was impregnated and then carbonized under different temperatures (250–300 °C). Scanning Electron Microscope (SEM) images showed an increase in the pore density, radius and volume of pores. X-ray diffraction analysis (XRD) showed that the samples had an amorphous structure. In Fourier-transform infrared (FT-IR) spectroscope analysis, C=C and N–H vibrations observed in 1515–1520 cm
−1
wave number of protein molecules were found to disappear with the increase in temperature. With Raman spectroscopy, the behaviors of D peak at 1344 cm
−1
wave number and G peak at 1566 cm
−1
wave number expressing structure layout in carbonized structures were analyzed depending on the temperatures. Between these intensities, (
I
D
/
I
G
) the rate was found to differ in direct proportion to temperature. XRD spectrums showed that the samples are converted into a more irregular crystal structure. All these results implied that the waste hair mass could be used as an adsorbant material.</abstract><cop>Singapore</cop><pub>Springer Singapore</pub><doi>10.1007/s42823-019-00099-9</doi><tpages>7</tpages></addata></record> |
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| subjects | Activated carbon Carbon Characterization and Evaluation of Materials Chemical bonds Chemistry and Materials Science Crystal structure Fourier transforms Hair Immunoglobulins Infrared analysis Infrared spectroscopy Keratin Materials Engineering Materials Science Morphology Nanotechnology Original Article Raman spectroscopy Scanning electron microscopy Spectrum analysis Sulfur Temperature Vibrations Wavelengths X-ray diffraction Zinc chloride |
| title | Synthesis and characterization of activated carbon produced from waste human hair mass using chemical activation |
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