Facile method to enhance the mechanical interfacial strength between carbon fibers and polyamide 6 using modified silane coupling agents
To address the need for a suitable thermoplastic resin-based sizing agent for accommodating the increasing demands of carbon fiber-reinforced plastic, in this work, alcohol-soluble polyamide 6 (PA6) and silane were chemically combined in a certain ratio to improve the mechanical interface properties...
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| Veröffentlicht in: | Carbon Letters 2022-10, Vol.32 (6), p.1463-1472 |
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| creator | Kim, Dong-Kyu Kang, Seong-Hyun Han, Woong Kim, Kwan-Woo Kim, Byung-Joo |
| description | To address the need for a suitable thermoplastic resin-based sizing agent for accommodating the increasing demands of carbon fiber-reinforced plastic, in this work, alcohol-soluble polyamide 6 (PA6) and silane were chemically combined in a certain ratio to improve the mechanical interface properties of the carbon fiber/PA6 composite, and the enhancement in the mechanical interface strength of the final composite according to the treatment time was confirmed. Carbon fiber surface properties were analyzed through ultrahigh-resolution field emission scanning electron microscopy (FE-SEM), X-ray photoelectron spectroscopy, and Fourier transform infrared spectrometry. The tensile strength of carbon fibers before and after hybrid sizing treatment and the mechanical interfacial shear strength of the final composite were analyzed using tensile and universal testing machines, respectively. After the hybrid sizing treatment, the introduction of the sizing agent to the carbon fiber surface was confirmed through FE-SEM, and a simultaneous increase in the surface roughness was observed. Moreover, the interfacial adhesion was confirmed to increase significantly, as compared to that of the desized carbon fiber. Therefore, this modified sizing agent treatment serves as an effective method for improving the mechanical interfacial adhesion between the carbon fiber and the PA6 matrix. |
| doi_str_mv | 10.1007/s42823-022-00388-w |
| format | Article |
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Carbon fiber surface properties were analyzed through ultrahigh-resolution field emission scanning electron microscopy (FE-SEM), X-ray photoelectron spectroscopy, and Fourier transform infrared spectrometry. The tensile strength of carbon fibers before and after hybrid sizing treatment and the mechanical interfacial shear strength of the final composite were analyzed using tensile and universal testing machines, respectively. After the hybrid sizing treatment, the introduction of the sizing agent to the carbon fiber surface was confirmed through FE-SEM, and a simultaneous increase in the surface roughness was observed. Moreover, the interfacial adhesion was confirmed to increase significantly, as compared to that of the desized carbon fiber. Therefore, this modified sizing agent treatment serves as an effective method for improving the mechanical interfacial adhesion between the carbon fiber and the PA6 matrix.</description><identifier>ISSN: 1976-4251</identifier><identifier>EISSN: 2233-4998</identifier><identifier>DOI: 10.1007/s42823-022-00388-w</identifier><language>eng</language><publisher>Singapore: Springer Nature Singapore</publisher><subject>Acids ; Adhesion ; Carbon ; Carbon fiber reinforced plastics ; Carbon fiber reinforcement ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Composite materials ; Coupling agents ; Emission analysis ; Fiber reinforced polymers ; Fibers ; Field emission microscopy ; Fourier transforms ; Infrared spectroscopy ; Interfacial properties ; Interfacial shear strength ; Interfacial strength ; Materials Engineering ; Materials Science ; Mechanical properties ; Nanotechnology ; Original Article ; Photoelectron spectroscopy ; Photoelectrons ; Physical properties ; Polyamide resins ; Polyamides ; Resins ; Scanning electron microscopy ; Scientific imaging ; Shear strength ; Silanes ; Sizing ; Spectrometry ; Surface properties ; Surface roughness ; Tensile strength ; Thermoplastic resins ; X ray photoelectron spectroscopy ; X-rays</subject><ispartof>Carbon Letters, 2022-10, Vol.32 (6), p.1463-1472</ispartof><rights>The Author(s), under exclusive licence to Korean Carbon Society 2022. 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Carbon fiber surface properties were analyzed through ultrahigh-resolution field emission scanning electron microscopy (FE-SEM), X-ray photoelectron spectroscopy, and Fourier transform infrared spectrometry. The tensile strength of carbon fibers before and after hybrid sizing treatment and the mechanical interfacial shear strength of the final composite were analyzed using tensile and universal testing machines, respectively. After the hybrid sizing treatment, the introduction of the sizing agent to the carbon fiber surface was confirmed through FE-SEM, and a simultaneous increase in the surface roughness was observed. Moreover, the interfacial adhesion was confirmed to increase significantly, as compared to that of the desized carbon fiber. Therefore, this modified sizing agent treatment serves as an effective method for improving the mechanical interfacial adhesion between the carbon fiber and the PA6 matrix.</description><subject>Acids</subject><subject>Adhesion</subject><subject>Carbon</subject><subject>Carbon fiber reinforced plastics</subject><subject>Carbon fiber reinforcement</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Composite materials</subject><subject>Coupling agents</subject><subject>Emission analysis</subject><subject>Fiber reinforced polymers</subject><subject>Fibers</subject><subject>Field emission microscopy</subject><subject>Fourier transforms</subject><subject>Infrared spectroscopy</subject><subject>Interfacial properties</subject><subject>Interfacial shear strength</subject><subject>Interfacial strength</subject><subject>Materials Engineering</subject><subject>Materials Science</subject><subject>Mechanical properties</subject><subject>Nanotechnology</subject><subject>Original Article</subject><subject>Photoelectron spectroscopy</subject><subject>Photoelectrons</subject><subject>Physical properties</subject><subject>Polyamide resins</subject><subject>Polyamides</subject><subject>Resins</subject><subject>Scanning electron microscopy</subject><subject>Scientific imaging</subject><subject>Shear strength</subject><subject>Silanes</subject><subject>Sizing</subject><subject>Spectrometry</subject><subject>Surface properties</subject><subject>Surface roughness</subject><subject>Tensile strength</subject><subject>Thermoplastic resins</subject><subject>X ray photoelectron spectroscopy</subject><subject>X-rays</subject><issn>1976-4251</issn><issn>2233-4998</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp9kc9qGzEQxkVIIcbxC_Qk6HkbrbTelY7FNE3BkEt6FrPSyKt2LbmSjPEb9LEr14XkFOYw_37fzOEj5GPLPreMDQ-545KLhnHeMCakbE43ZMG5EE2nlLwli1YNfdPxdXtHVjn7sYoEU0z0C_LnEYyfke6xTNHSEimGCYJBWqbL1NTGG5ipDwWTq3Ctc0kYdmWiI5YTYqAG0hgDdX7ElCkESw9xPsPeW6Q9PWYfdnQfrXceLc1-hoDUxONhvixgh6Hke_LBwZxx9T8vyY_Hry-bp2b7_O375su2MXwYSuNQCStl36FSpmVr44ywYy9BgIJRKGekGgZlFTCL3PVOdb2sCVE6AyMTS_LpeveQ4u8j5qJ_xmMK9aXmSggmawyv1K-YELKZ4gzplex4y3pRKX6lTIo5J3T6kPwe0lm3TF-s0VdrdLVG_7NGn6pIXEW5wmGHb86-o_oLhlaVNA</recordid><startdate>20221001</startdate><enddate>20221001</enddate><creator>Kim, Dong-Kyu</creator><creator>Kang, Seong-Hyun</creator><creator>Han, Woong</creator><creator>Kim, Kwan-Woo</creator><creator>Kim, Byung-Joo</creator><general>Springer Nature Singapore</general><general>한국탄소학회</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>KROLR</scope><scope>3V.</scope><scope>7XB</scope><scope>88I</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AEUYN</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M2P</scope><scope>M7S</scope><scope>PATMY</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><scope>PYCSY</scope><scope>Q9U</scope><orcidid>https://orcid.org/0000-0003-3331-4375</orcidid></search><sort><creationdate>20221001</creationdate><title>Facile method to enhance the mechanical interfacial strength between carbon fibers and polyamide 6 using modified silane coupling agents</title><author>Kim, Dong-Kyu ; Kang, Seong-Hyun ; Han, Woong ; Kim, Kwan-Woo ; Kim, Byung-Joo</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c277t-fe93d8864e99c105cfc3db68a3a9ab39fc89779d9a0de2f6f9468f6fee8fcab03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Acids</topic><topic>Adhesion</topic><topic>Carbon</topic><topic>Carbon fiber reinforced plastics</topic><topic>Carbon fiber reinforcement</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Composite materials</topic><topic>Coupling agents</topic><topic>Emission analysis</topic><topic>Fiber reinforced polymers</topic><topic>Fibers</topic><topic>Field emission microscopy</topic><topic>Fourier transforms</topic><topic>Infrared spectroscopy</topic><topic>Interfacial properties</topic><topic>Interfacial shear strength</topic><topic>Interfacial strength</topic><topic>Materials Engineering</topic><topic>Materials Science</topic><topic>Mechanical properties</topic><topic>Nanotechnology</topic><topic>Original Article</topic><topic>Photoelectron spectroscopy</topic><topic>Photoelectrons</topic><topic>Physical properties</topic><topic>Polyamide resins</topic><topic>Polyamides</topic><topic>Resins</topic><topic>Scanning electron microscopy</topic><topic>Scientific imaging</topic><topic>Shear strength</topic><topic>Silanes</topic><topic>Sizing</topic><topic>Spectrometry</topic><topic>Surface properties</topic><topic>Surface roughness</topic><topic>Tensile strength</topic><topic>Thermoplastic resins</topic><topic>X ray photoelectron spectroscopy</topic><topic>X-rays</topic><toplevel>online_resources</toplevel><creatorcontrib>Kim, Dong-Kyu</creatorcontrib><creatorcontrib>Kang, Seong-Hyun</creatorcontrib><creatorcontrib>Han, Woong</creatorcontrib><creatorcontrib>Kim, Kwan-Woo</creatorcontrib><creatorcontrib>Kim, Byung-Joo</creatorcontrib><collection>CrossRef</collection><collection>Korea Scholar</collection><collection>ProQuest Central (Corporate)</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Science Database (Alumni Edition)</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest One Sustainability</collection><collection>ProQuest Central UK/Ireland</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Science Database</collection><collection>Engineering Database</collection><collection>Environmental Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><collection>Environmental Science Collection</collection><collection>ProQuest Central Basic</collection><jtitle>Carbon Letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Kim, Dong-Kyu</au><au>Kang, Seong-Hyun</au><au>Han, Woong</au><au>Kim, Kwan-Woo</au><au>Kim, Byung-Joo</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Facile method to enhance the mechanical interfacial strength between carbon fibers and polyamide 6 using modified silane coupling agents</atitle><jtitle>Carbon Letters</jtitle><stitle>Carbon Lett</stitle><date>2022-10-01</date><risdate>2022</risdate><volume>32</volume><issue>6</issue><spage>1463</spage><epage>1472</epage><pages>1463-1472</pages><issn>1976-4251</issn><eissn>2233-4998</eissn><abstract>To address the need for a suitable thermoplastic resin-based sizing agent for accommodating the increasing demands of carbon fiber-reinforced plastic, in this work, alcohol-soluble polyamide 6 (PA6) and silane were chemically combined in a certain ratio to improve the mechanical interface properties of the carbon fiber/PA6 composite, and the enhancement in the mechanical interface strength of the final composite according to the treatment time was confirmed. Carbon fiber surface properties were analyzed through ultrahigh-resolution field emission scanning electron microscopy (FE-SEM), X-ray photoelectron spectroscopy, and Fourier transform infrared spectrometry. The tensile strength of carbon fibers before and after hybrid sizing treatment and the mechanical interfacial shear strength of the final composite were analyzed using tensile and universal testing machines, respectively. After the hybrid sizing treatment, the introduction of the sizing agent to the carbon fiber surface was confirmed through FE-SEM, and a simultaneous increase in the surface roughness was observed. Moreover, the interfacial adhesion was confirmed to increase significantly, as compared to that of the desized carbon fiber. Therefore, this modified sizing agent treatment serves as an effective method for improving the mechanical interfacial adhesion between the carbon fiber and the PA6 matrix.</abstract><cop>Singapore</cop><pub>Springer Nature Singapore</pub><doi>10.1007/s42823-022-00388-w</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0003-3331-4375</orcidid></addata></record> |
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| subjects | Acids Adhesion Carbon Carbon fiber reinforced plastics Carbon fiber reinforcement Characterization and Evaluation of Materials Chemistry and Materials Science Composite materials Coupling agents Emission analysis Fiber reinforced polymers Fibers Field emission microscopy Fourier transforms Infrared spectroscopy Interfacial properties Interfacial shear strength Interfacial strength Materials Engineering Materials Science Mechanical properties Nanotechnology Original Article Photoelectron spectroscopy Photoelectrons Physical properties Polyamide resins Polyamides Resins Scanning electron microscopy Scientific imaging Shear strength Silanes Sizing Spectrometry Surface properties Surface roughness Tensile strength Thermoplastic resins X ray photoelectron spectroscopy X-rays |
| title | Facile method to enhance the mechanical interfacial strength between carbon fibers and polyamide 6 using modified silane coupling agents |
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