Three-dimensional graphene gel/carbon cloth electrode for detection of Cu2+ through two electrochemical methods of interactive verification
Here, conductive carbon cloth (CC) and three-dimensional (3D) graphene hydrogel (GH) were combined to develop an electrochemical sensor for the detection of trace Cu 2+ . 3D GH/CC has low production cost and high sensitivity, accuracy, and stability, which are suitable for creation of small portable...
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| Veröffentlicht in: | Journal of materials science. Materials in electronics 2024-02, Vol.35 (6), p.403, Article 403 |
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| creator | Wang, Yiding Hao, Changshi Duan, Shaojing Liang, Benliang Yan, Luting |
| description | Here, conductive carbon cloth (CC) and three-dimensional (3D) graphene hydrogel (GH) were combined to develop an electrochemical sensor for the detection of trace Cu
2+
. 3D GH/CC has low production cost and high sensitivity, accuracy, and stability, which are suitable for creation of small portable devices and large-scale commercial production. The limit of detection reached 1.87 nmol L
−1
, and the linear ranges were from 0.1 µmol L
−1
to 10 µmol L
−1
and from 10 µmol L
−1
to 1000 µmol L
−1
. Innovative interactive verification-based Cu
2+
detection was carried out using two electrochemical detection methods, namely, anodic stripping voltammetry and electrochemical impedance spectroscopy, and with the mutual support of the two methods, the recovery rate of Cu
2+
was estimated to 98%, which was improved considerably at medium and low concentrations in the actual water sample. The results showed that this preparation and detection method can be used as a new platform for the detection of trace Cu
2+
and provide a new commercialized case for evaluating the composition and content of inorganic pollutants in water. |
| doi_str_mv | 10.1007/s10854-024-12214-2 |
| format | Article |
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2+
. 3D GH/CC has low production cost and high sensitivity, accuracy, and stability, which are suitable for creation of small portable devices and large-scale commercial production. The limit of detection reached 1.87 nmol L
−1
, and the linear ranges were from 0.1 µmol L
−1
to 10 µmol L
−1
and from 10 µmol L
−1
to 1000 µmol L
−1
. Innovative interactive verification-based Cu
2+
detection was carried out using two electrochemical detection methods, namely, anodic stripping voltammetry and electrochemical impedance spectroscopy, and with the mutual support of the two methods, the recovery rate of Cu
2+
was estimated to 98%, which was improved considerably at medium and low concentrations in the actual water sample. The results showed that this preparation and detection method can be used as a new platform for the detection of trace Cu
2+
and provide a new commercialized case for evaluating the composition and content of inorganic pollutants in water.</description><identifier>ISSN: 0957-4522</identifier><identifier>EISSN: 1573-482X</identifier><identifier>DOI: 10.1007/s10854-024-12214-2</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Anodic stripping ; Carbon ; Characterization and Evaluation of Materials ; Chemical sensors ; Chemistry and Materials Science ; Cloth ; Commercialization ; Copper ; Electrochemical analysis ; Electrochemical impedance spectroscopy ; Electrodes ; Electrons ; Fourier transforms ; Graphene ; Heavy metals ; Low concentrations ; Materials Science ; Nanomaterials ; Optical and Electronic Materials ; Portable equipment ; Production costs ; Spectrum analysis ; Textiles ; Verification ; Voltammetry ; Water sampling ; Work stations</subject><ispartof>Journal of materials science. Materials in electronics, 2024-02, Vol.35 (6), p.403, Article 403</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2024. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c200t-2194d19b27d3470f73533fbc4781f427a931b90238f6aa1e9a480d6107eb0dd03</cites><orcidid>0000-0003-1417-2439</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s10854-024-12214-2$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s10854-024-12214-2$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>314,780,784,27924,27925,41488,42557,51319</link.rule.ids></links><search><creatorcontrib>Wang, Yiding</creatorcontrib><creatorcontrib>Hao, Changshi</creatorcontrib><creatorcontrib>Duan, Shaojing</creatorcontrib><creatorcontrib>Liang, Benliang</creatorcontrib><creatorcontrib>Yan, Luting</creatorcontrib><title>Three-dimensional graphene gel/carbon cloth electrode for detection of Cu2+ through two electrochemical methods of interactive verification</title><title>Journal of materials science. Materials in electronics</title><addtitle>J Mater Sci: Mater Electron</addtitle><description>Here, conductive carbon cloth (CC) and three-dimensional (3D) graphene hydrogel (GH) were combined to develop an electrochemical sensor for the detection of trace Cu
2+
. 3D GH/CC has low production cost and high sensitivity, accuracy, and stability, which are suitable for creation of small portable devices and large-scale commercial production. The limit of detection reached 1.87 nmol L
−1
, and the linear ranges were from 0.1 µmol L
−1
to 10 µmol L
−1
and from 10 µmol L
−1
to 1000 µmol L
−1
. Innovative interactive verification-based Cu
2+
detection was carried out using two electrochemical detection methods, namely, anodic stripping voltammetry and electrochemical impedance spectroscopy, and with the mutual support of the two methods, the recovery rate of Cu
2+
was estimated to 98%, which was improved considerably at medium and low concentrations in the actual water sample. The results showed that this preparation and detection method can be used as a new platform for the detection of trace Cu
2+
and provide a new commercialized case for evaluating the composition and content of inorganic pollutants in water.</description><subject>Anodic stripping</subject><subject>Carbon</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemical sensors</subject><subject>Chemistry and Materials Science</subject><subject>Cloth</subject><subject>Commercialization</subject><subject>Copper</subject><subject>Electrochemical analysis</subject><subject>Electrochemical impedance spectroscopy</subject><subject>Electrodes</subject><subject>Electrons</subject><subject>Fourier transforms</subject><subject>Graphene</subject><subject>Heavy metals</subject><subject>Low concentrations</subject><subject>Materials Science</subject><subject>Nanomaterials</subject><subject>Optical and Electronic Materials</subject><subject>Portable equipment</subject><subject>Production costs</subject><subject>Spectrum analysis</subject><subject>Textiles</subject><subject>Verification</subject><subject>Voltammetry</subject><subject>Water sampling</subject><subject>Work stations</subject><issn>0957-4522</issn><issn>1573-482X</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><recordid>eNp9kMFq3DAURUVJoZO0P9CVoMui5ulJHtnLMLRJIZBNCt0J2XoaO3isiaRJ6Tf0p6vpJHSXlXhwzgFdxj5K-CIBzGWW0DZaAGohEaUW-IatZGOU0C3-PGMr6BojdIP4jp3n_AAAa63aFftzPyYi4acdLXmKi5v5Nrn9SAvxLc2Xg0t9XPgwxzJymmkoKXriISbuqdSzOjwGvjngZ17GFA_bkZdf8YUdRtpNQ63uqIzR5yM7LYWSq-oT8SdKU6jAsfOevQ1uzvTh-b1gP759vd_ciNu76--bq1sxIEARKDvtZdej8UobCEY1SoV-0KaVQaNxnZJ9B6jasHZOUud0C34twVAP3oO6YJ9O3X2KjwfKxT7EQ6pfzxari9C0Zl0pPFFDijknCnafpp1Lv60Eexzdnka3dXT7b3SLVVInKVd42VL6n37F-gsT8obM</recordid><startdate>20240201</startdate><enddate>20240201</enddate><creator>Wang, Yiding</creator><creator>Hao, Changshi</creator><creator>Duan, Shaojing</creator><creator>Liang, Benliang</creator><creator>Yan, Luting</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SP</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>F28</scope><scope>FR3</scope><scope>JG9</scope><scope>L7M</scope><orcidid>https://orcid.org/0000-0003-1417-2439</orcidid></search><sort><creationdate>20240201</creationdate><title>Three-dimensional graphene gel/carbon cloth electrode for detection of Cu2+ through two electrochemical methods of interactive verification</title><author>Wang, Yiding ; Hao, Changshi ; Duan, Shaojing ; Liang, Benliang ; Yan, Luting</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c200t-2194d19b27d3470f73533fbc4781f427a931b90238f6aa1e9a480d6107eb0dd03</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Anodic stripping</topic><topic>Carbon</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemical sensors</topic><topic>Chemistry and Materials Science</topic><topic>Cloth</topic><topic>Commercialization</topic><topic>Copper</topic><topic>Electrochemical analysis</topic><topic>Electrochemical impedance spectroscopy</topic><topic>Electrodes</topic><topic>Electrons</topic><topic>Fourier transforms</topic><topic>Graphene</topic><topic>Heavy metals</topic><topic>Low concentrations</topic><topic>Materials Science</topic><topic>Nanomaterials</topic><topic>Optical and Electronic Materials</topic><topic>Portable equipment</topic><topic>Production costs</topic><topic>Spectrum analysis</topic><topic>Textiles</topic><topic>Verification</topic><topic>Voltammetry</topic><topic>Water sampling</topic><topic>Work stations</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Wang, Yiding</creatorcontrib><creatorcontrib>Hao, Changshi</creatorcontrib><creatorcontrib>Duan, Shaojing</creatorcontrib><creatorcontrib>Liang, Benliang</creatorcontrib><creatorcontrib>Yan, Luting</creatorcontrib><collection>CrossRef</collection><collection>Electronics & Communications Abstracts</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ANTE: Abstracts in New Technology & Engineering</collection><collection>Engineering Research Database</collection><collection>Materials Research Database</collection><collection>Advanced Technologies Database with Aerospace</collection><jtitle>Journal of materials science. Materials in electronics</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Wang, Yiding</au><au>Hao, Changshi</au><au>Duan, Shaojing</au><au>Liang, Benliang</au><au>Yan, Luting</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Three-dimensional graphene gel/carbon cloth electrode for detection of Cu2+ through two electrochemical methods of interactive verification</atitle><jtitle>Journal of materials science. Materials in electronics</jtitle><stitle>J Mater Sci: Mater Electron</stitle><date>2024-02-01</date><risdate>2024</risdate><volume>35</volume><issue>6</issue><spage>403</spage><pages>403-</pages><artnum>403</artnum><issn>0957-4522</issn><eissn>1573-482X</eissn><abstract>Here, conductive carbon cloth (CC) and three-dimensional (3D) graphene hydrogel (GH) were combined to develop an electrochemical sensor for the detection of trace Cu
2+
. 3D GH/CC has low production cost and high sensitivity, accuracy, and stability, which are suitable for creation of small portable devices and large-scale commercial production. The limit of detection reached 1.87 nmol L
−1
, and the linear ranges were from 0.1 µmol L
−1
to 10 µmol L
−1
and from 10 µmol L
−1
to 1000 µmol L
−1
. Innovative interactive verification-based Cu
2+
detection was carried out using two electrochemical detection methods, namely, anodic stripping voltammetry and electrochemical impedance spectroscopy, and with the mutual support of the two methods, the recovery rate of Cu
2+
was estimated to 98%, which was improved considerably at medium and low concentrations in the actual water sample. The results showed that this preparation and detection method can be used as a new platform for the detection of trace Cu
2+
and provide a new commercialized case for evaluating the composition and content of inorganic pollutants in water.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s10854-024-12214-2</doi><orcidid>https://orcid.org/0000-0003-1417-2439</orcidid></addata></record> |
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| subjects | Anodic stripping Carbon Characterization and Evaluation of Materials Chemical sensors Chemistry and Materials Science Cloth Commercialization Copper Electrochemical analysis Electrochemical impedance spectroscopy Electrodes Electrons Fourier transforms Graphene Heavy metals Low concentrations Materials Science Nanomaterials Optical and Electronic Materials Portable equipment Production costs Spectrum analysis Textiles Verification Voltammetry Water sampling Work stations |
| title | Three-dimensional graphene gel/carbon cloth electrode for detection of Cu2+ through two electrochemical methods of interactive verification |
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