Extraction and recovery of capsaicin from scotch bonnet by alkaline-based deep eutectic solvent
Deep eutectic solvents (DESs) have emerged as green alternatives to conventional organic solvents for the efficient extraction of bioactive compounds. In this study, capsaicin was extracted from Capsicum annuum ( C. annuum ) by ultrasound-assisted extraction using strong to mild acid- and alkaline-b...
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creator | Cho, Ha-Seong Olawuyi, Ibukunoluwa Fola Park, Jong-Jin Said, Nurul Saadah Na, Yoo-jin Lee, Won-Young |
description | Deep eutectic solvents (DESs) have emerged as green alternatives to conventional organic solvents for the efficient extraction of bioactive compounds. In this study, capsaicin was extracted from
Capsicum annuum
(
C. annuum
) by ultrasound-assisted extraction using strong to mild acid- and alkaline-based DESs to compare their extraction efficiency with conventional solvent. Strong alkaline-based DESs extract showed the highest capsaicin content (17.58 ± 0.28 mg/g) compared with other DESs, including acid-based DES (12.88 ± 0.11 mg/g) and ethanol (13.85 ± 0.24 mg/g) (
p
|
doi_str_mv | 10.1007/s11694-023-02296-7 |
format | Article |
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Capsicum annuum
(
C. annuum
) by ultrasound-assisted extraction using strong to mild acid- and alkaline-based DESs to compare their extraction efficiency with conventional solvent. Strong alkaline-based DESs extract showed the highest capsaicin content (17.58 ± 0.28 mg/g) compared with other DESs, including acid-based DES (12.88 ± 0.11 mg/g) and ethanol (13.85 ± 0.24 mg/g) (
p
< 0.05) in the screening of DESs. Furthermore, optimization of alkaline-based DES extraction parameters achieved an increased capsaicin content 19.15 mg/g. Macroporous resins (SP850, XAD2, and XAD16N) were used to recover capsaicin from DES extract, and SP850 showed the highest adsorption and recovery ratio of capsaicin. Moreover, the antioxidant potency of the recovered capsaicin was confirmed using radical scavenging assays. This study provides an eco-friendly, novel, efficient extraction method for obtaining capsaicin from
C. annuum
.</description><identifier>ISSN: 2193-4126</identifier><identifier>EISSN: 2193-4134</identifier><identifier>DOI: 10.1007/s11694-023-02296-7</identifier><language>eng</language><publisher>New York: Springer US</publisher><subject>Acids ; Bioactive compounds ; Capsaicin ; Capsicum annuum ; Chemistry ; Chemistry and Materials Science ; Chemistry/Food Science ; Chloride ; Content analysis ; Efficiency ; Engineering ; Ethanol ; Food Science ; Glycerol ; Hydrogen bonds ; Optimization ; Organic solvents ; Original Paper ; Peppers ; Potash ; Potassium ; Recovery ; Resins ; Scavenging ; Solvents ; Ultrasonic imaging ; Variance analysis</subject><ispartof>Journal of food measurement & characterization, 2024-02, Vol.18 (2), p.1372-1381</ispartof><rights>The Author(s), under exclusive licence to Springer Science+Business Media, LLC, part of Springer Nature 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><cites>FETCH-LOGICAL-c270t-1a4589e588ce0189464d4d424f7aef19553e24d929a8060990b8b0a07f8c48163</cites><orcidid>0000-0001-5850-9692</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s11694-023-02296-7$$EPDF$$P50$$Gspringer$$H</linktopdf><linktohtml>$$Uhttps://link.springer.com/10.1007/s11694-023-02296-7$$EHTML$$P50$$Gspringer$$H</linktohtml><link.rule.ids>315,781,785,27926,27927,41490,42559,51321</link.rule.ids></links><search><creatorcontrib>Cho, Ha-Seong</creatorcontrib><creatorcontrib>Olawuyi, Ibukunoluwa Fola</creatorcontrib><creatorcontrib>Park, Jong-Jin</creatorcontrib><creatorcontrib>Said, Nurul Saadah</creatorcontrib><creatorcontrib>Na, Yoo-jin</creatorcontrib><creatorcontrib>Lee, Won-Young</creatorcontrib><title>Extraction and recovery of capsaicin from scotch bonnet by alkaline-based deep eutectic solvent</title><title>Journal of food measurement & characterization</title><addtitle>Food Measure</addtitle><description>Deep eutectic solvents (DESs) have emerged as green alternatives to conventional organic solvents for the efficient extraction of bioactive compounds. In this study, capsaicin was extracted from
Capsicum annuum
(
C. annuum
) by ultrasound-assisted extraction using strong to mild acid- and alkaline-based DESs to compare their extraction efficiency with conventional solvent. Strong alkaline-based DESs extract showed the highest capsaicin content (17.58 ± 0.28 mg/g) compared with other DESs, including acid-based DES (12.88 ± 0.11 mg/g) and ethanol (13.85 ± 0.24 mg/g) (
p
< 0.05) in the screening of DESs. Furthermore, optimization of alkaline-based DES extraction parameters achieved an increased capsaicin content 19.15 mg/g. Macroporous resins (SP850, XAD2, and XAD16N) were used to recover capsaicin from DES extract, and SP850 showed the highest adsorption and recovery ratio of capsaicin. Moreover, the antioxidant potency of the recovered capsaicin was confirmed using radical scavenging assays. This study provides an eco-friendly, novel, efficient extraction method for obtaining capsaicin from
C. annuum
.</description><subject>Acids</subject><subject>Bioactive compounds</subject><subject>Capsaicin</subject><subject>Capsicum annuum</subject><subject>Chemistry</subject><subject>Chemistry and Materials Science</subject><subject>Chemistry/Food Science</subject><subject>Chloride</subject><subject>Content analysis</subject><subject>Efficiency</subject><subject>Engineering</subject><subject>Ethanol</subject><subject>Food Science</subject><subject>Glycerol</subject><subject>Hydrogen bonds</subject><subject>Optimization</subject><subject>Organic solvents</subject><subject>Original Paper</subject><subject>Peppers</subject><subject>Potash</subject><subject>Potassium</subject><subject>Recovery</subject><subject>Resins</subject><subject>Scavenging</subject><subject>Solvents</subject><subject>Ultrasonic imaging</subject><subject>Variance analysis</subject><issn>2193-4126</issn><issn>2193-4134</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2024</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9kE1LxDAQhoMouOj-AU8Bz9VJmjbJUZb1Axa86Dmk6VS7dpOaZBf331td0ZsMw8zh_YCHkAsGVwxAXifGai0K4OW0XNeFPCIzznRZCFaK49-f16dkntIaABiTQtTljJjlR47W5T54an1LI7qww7inoaPOjsn2rve0i2FDkwvZvdImeI-ZNntqhzc79B6LxiZsaYs4UtxmnNIcTWHYoc_n5KSzQ8L5zz0jz7fLp8V9sXq8e1jcrArHJeSCWVEpjZVSDoEpLWrRTsNFJy12TFdViVy0mmuroAatoVENWJCdckKxujwjl4fcMYb3LaZs1mEb_VRpuOaMCw5STCp-ULkYUorYmTH2Gxv3hoH5YmkOLM3E0nyzNHIylQdTmsT-BeNf9D-uT664dls</recordid><startdate>20240201</startdate><enddate>20240201</enddate><creator>Cho, Ha-Seong</creator><creator>Olawuyi, Ibukunoluwa Fola</creator><creator>Park, Jong-Jin</creator><creator>Said, Nurul Saadah</creator><creator>Na, Yoo-jin</creator><creator>Lee, Won-Young</creator><general>Springer US</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>3V.</scope><scope>7X2</scope><scope>8FE</scope><scope>8FG</scope><scope>8FH</scope><scope>8FK</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>L6V</scope><scope>M0K</scope><scope>M7S</scope><scope>PIMPY</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><orcidid>https://orcid.org/0000-0001-5850-9692</orcidid></search><sort><creationdate>20240201</creationdate><title>Extraction and recovery of capsaicin from scotch bonnet by alkaline-based deep eutectic solvent</title><author>Cho, Ha-Seong ; Olawuyi, Ibukunoluwa Fola ; Park, Jong-Jin ; Said, Nurul Saadah ; Na, Yoo-jin ; Lee, Won-Young</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c270t-1a4589e588ce0189464d4d424f7aef19553e24d929a8060990b8b0a07f8c48163</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2024</creationdate><topic>Acids</topic><topic>Bioactive compounds</topic><topic>Capsaicin</topic><topic>Capsicum annuum</topic><topic>Chemistry</topic><topic>Chemistry and Materials Science</topic><topic>Chemistry/Food Science</topic><topic>Chloride</topic><topic>Content analysis</topic><topic>Efficiency</topic><topic>Engineering</topic><topic>Ethanol</topic><topic>Food Science</topic><topic>Glycerol</topic><topic>Hydrogen bonds</topic><topic>Optimization</topic><topic>Organic solvents</topic><topic>Original Paper</topic><topic>Peppers</topic><topic>Potash</topic><topic>Potassium</topic><topic>Recovery</topic><topic>Resins</topic><topic>Scavenging</topic><topic>Solvents</topic><topic>Ultrasonic imaging</topic><topic>Variance analysis</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Cho, Ha-Seong</creatorcontrib><creatorcontrib>Olawuyi, Ibukunoluwa Fola</creatorcontrib><creatorcontrib>Park, Jong-Jin</creatorcontrib><creatorcontrib>Said, Nurul Saadah</creatorcontrib><creatorcontrib>Na, Yoo-jin</creatorcontrib><creatorcontrib>Lee, Won-Young</creatorcontrib><collection>CrossRef</collection><collection>ProQuest Central (Corporate)</collection><collection>Agricultural Science Collection</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Natural Science Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Engineering Collection</collection><collection>Agricultural Science Database</collection><collection>Engineering Database</collection><collection>Publicly Available Content Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><jtitle>Journal of food measurement & characterization</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Cho, Ha-Seong</au><au>Olawuyi, Ibukunoluwa Fola</au><au>Park, Jong-Jin</au><au>Said, Nurul Saadah</au><au>Na, Yoo-jin</au><au>Lee, Won-Young</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Extraction and recovery of capsaicin from scotch bonnet by alkaline-based deep eutectic solvent</atitle><jtitle>Journal of food measurement & characterization</jtitle><stitle>Food Measure</stitle><date>2024-02-01</date><risdate>2024</risdate><volume>18</volume><issue>2</issue><spage>1372</spage><epage>1381</epage><pages>1372-1381</pages><issn>2193-4126</issn><eissn>2193-4134</eissn><abstract>Deep eutectic solvents (DESs) have emerged as green alternatives to conventional organic solvents for the efficient extraction of bioactive compounds. In this study, capsaicin was extracted from
Capsicum annuum
(
C. annuum
) by ultrasound-assisted extraction using strong to mild acid- and alkaline-based DESs to compare their extraction efficiency with conventional solvent. Strong alkaline-based DESs extract showed the highest capsaicin content (17.58 ± 0.28 mg/g) compared with other DESs, including acid-based DES (12.88 ± 0.11 mg/g) and ethanol (13.85 ± 0.24 mg/g) (
p
< 0.05) in the screening of DESs. Furthermore, optimization of alkaline-based DES extraction parameters achieved an increased capsaicin content 19.15 mg/g. Macroporous resins (SP850, XAD2, and XAD16N) were used to recover capsaicin from DES extract, and SP850 showed the highest adsorption and recovery ratio of capsaicin. Moreover, the antioxidant potency of the recovered capsaicin was confirmed using radical scavenging assays. This study provides an eco-friendly, novel, efficient extraction method for obtaining capsaicin from
C. annuum
.</abstract><cop>New York</cop><pub>Springer US</pub><doi>10.1007/s11694-023-02296-7</doi><tpages>10</tpages><orcidid>https://orcid.org/0000-0001-5850-9692</orcidid><oa>free_for_read</oa></addata></record> |
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subjects | Acids Bioactive compounds Capsaicin Capsicum annuum Chemistry Chemistry and Materials Science Chemistry/Food Science Chloride Content analysis Efficiency Engineering Ethanol Food Science Glycerol Hydrogen bonds Optimization Organic solvents Original Paper Peppers Potash Potassium Recovery Resins Scavenging Solvents Ultrasonic imaging Variance analysis |
title | Extraction and recovery of capsaicin from scotch bonnet by alkaline-based deep eutectic solvent |
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