Extraction and recovery of capsaicin from scotch bonnet by alkaline-based deep eutectic solvent

Deep eutectic solvents (DESs) have emerged as green alternatives to conventional organic solvents for the efficient extraction of bioactive compounds. In this study, capsaicin was extracted from Capsicum annuum ( C. annuum ) by ultrasound-assisted extraction using strong to mild acid- and alkaline-b...

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Veröffentlicht in:Journal of food measurement & characterization 2024-02, Vol.18 (2), p.1372-1381
Hauptverfasser: Cho, Ha-Seong, Olawuyi, Ibukunoluwa Fola, Park, Jong-Jin, Said, Nurul Saadah, Na, Yoo-jin, Lee, Won-Young
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container_title Journal of food measurement & characterization
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creator Cho, Ha-Seong
Olawuyi, Ibukunoluwa Fola
Park, Jong-Jin
Said, Nurul Saadah
Na, Yoo-jin
Lee, Won-Young
description Deep eutectic solvents (DESs) have emerged as green alternatives to conventional organic solvents for the efficient extraction of bioactive compounds. In this study, capsaicin was extracted from Capsicum annuum ( C. annuum ) by ultrasound-assisted extraction using strong to mild acid- and alkaline-based DESs to compare their extraction efficiency with conventional solvent. Strong alkaline-based DESs extract showed the highest capsaicin content (17.58 ± 0.28 mg/g) compared with other DESs, including acid-based DES (12.88 ± 0.11 mg/g) and ethanol (13.85 ± 0.24 mg/g) ( p  
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In this study, capsaicin was extracted from Capsicum annuum ( C. annuum ) by ultrasound-assisted extraction using strong to mild acid- and alkaline-based DESs to compare their extraction efficiency with conventional solvent. Strong alkaline-based DESs extract showed the highest capsaicin content (17.58 ± 0.28 mg/g) compared with other DESs, including acid-based DES (12.88 ± 0.11 mg/g) and ethanol (13.85 ± 0.24 mg/g) ( p  &lt; 0.05) in the screening of DESs. Furthermore, optimization of alkaline-based DES extraction parameters achieved an increased capsaicin content 19.15 mg/g. Macroporous resins (SP850, XAD2, and XAD16N) were used to recover capsaicin from DES extract, and SP850 showed the highest adsorption and recovery ratio of capsaicin. Moreover, the antioxidant potency of the recovered capsaicin was confirmed using radical scavenging assays. 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subjects Acids
Bioactive compounds
Capsaicin
Capsicum annuum
Chemistry
Chemistry and Materials Science
Chemistry/Food Science
Chloride
Content analysis
Efficiency
Engineering
Ethanol
Food Science
Glycerol
Hydrogen bonds
Optimization
Organic solvents
Original Paper
Peppers
Potash
Potassium
Recovery
Resins
Scavenging
Solvents
Ultrasonic imaging
Variance analysis
title Extraction and recovery of capsaicin from scotch bonnet by alkaline-based deep eutectic solvent
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