Optimization for testing conditions of inverse gas chromatography and surface energies of various carbon fiber bundles
Surface free energy is an important parameter in surface and interface properties of fiber reinforced polymer composite. The BET (Brunauer, Emmett, and Teller) surface area and surface energy of the sample can be obtained by Inverse Gas Chromatography (IGC) based on the adsorption principle. In this...
Gespeichert in:
| Veröffentlicht in: | Carbon Letters 2023-05, Vol.33 (3), p.909-920 |
|---|---|
| Hauptverfasser: | , , , |
| Format: | Artikel |
| Sprache: | eng |
| Schlagworte: | |
| Online-Zugang: | Volltext |
| Tags: |
Tag hinzufügen
Keine Tags, Fügen Sie den ersten Tag hinzu!
|
| container_end_page | 920 |
|---|---|
| container_issue | 3 |
| container_start_page | 909 |
| container_title | Carbon Letters |
| container_volume | 33 |
| creator | Liu, Yuwei Gu, Yizhuo Wang, Shaokai Li, Min |
| description | Surface free energy is an important parameter in surface and interface properties of fiber reinforced polymer composite. The BET (Brunauer, Emmett, and Teller) surface area and surface energy of the sample can be obtained by Inverse Gas Chromatography (IGC) based on the adsorption principle. In this paper, surface energy of carbon fiber bundle was tested by means of IGC under different conditions to find reliable test parameters. The main parameters involved include length, mass, and packing density of sample, target fractional surface coverage, flow rate, and maximum elution time. It is demonstrated that IGC has the advantages of simple sample preparation, stable test data, high automation, and high sensitivity for carbon fiber. Among all test conditions, packing density and flow rate have the greatest influences on the experimental results. The optimized test parameters are suitable for various kinds of carbon fiber bundles, including polyacrylonitrile-based and pitch-based carbon fibers with different tensile properties and tow sizes. Moreover, IGC can acutely characterize the surface properties of carbon fibers after carbon nanotube modification and heat treatment, which are hard to carry out using contact angle method. |
| doi_str_mv | 10.1007/s42823-023-00472-9 |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_korea</sourceid><recordid>TN_cdi_proquest_journals_2921225913</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2921225913</sourcerecordid><originalsourceid>FETCH-LOGICAL-c347t-29938854f52c36966b07dbf2b8c958fbac43a62ca60424f968b470f10035723e3</originalsourceid><addsrcrecordid>eNp9kU1LAzEURYMoWLR_wFXA9WjykvnIUopfUHCj6yFJk2m0TerLTEF_vTNW0JWLRyCcc0PeJeSCsyvOWH2dJTQgCjYNkzUU6ojMAIQopFLNMZlxVVeFhJKfknnOwYySYIqJakb2T7s-bMOn7kOK1Cekvct9iB21Ka7CdJtp8jTEvcPsaKcztWtMW92nDvVu_UF1XNE8oNfWURcddsF9K3uNIQ0jrtFM2cE4pGaIq43L5-TE601285_zjLzc3T4vHorl0_3j4mZZWCHrvgClRNOU0pdgRaWqyrB6ZTyYxqqy8UZbKXQFVldMgvSqaoysmR-3IsoahBNn5PKQu8P0Pow_a1_TgHF8sgUFHKBUXPxSbwmdznadNhp_yXG9nKuRggNlMeWMzrc7DFuNHy1n7VREeyiiZdNMRbSTJA5SHuHYuT-x_1hfyO-MdA</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2921225913</pqid></control><display><type>article</type><title>Optimization for testing conditions of inverse gas chromatography and surface energies of various carbon fiber bundles</title><source>ProQuest Central Essentials</source><source>ProQuest Central (Alumni Edition)</source><source>ProQuest Central Student</source><source>ProQuest Central Korea</source><source>ProQuest Central UK/Ireland</source><source>SpringerLink Journals - AutoHoldings</source><source>ProQuest Central</source><creator>Liu, Yuwei ; Gu, Yizhuo ; Wang, Shaokai ; Li, Min</creator><creatorcontrib>Liu, Yuwei ; Gu, Yizhuo ; Wang, Shaokai ; Li, Min</creatorcontrib><description>Surface free energy is an important parameter in surface and interface properties of fiber reinforced polymer composite. The BET (Brunauer, Emmett, and Teller) surface area and surface energy of the sample can be obtained by Inverse Gas Chromatography (IGC) based on the adsorption principle. In this paper, surface energy of carbon fiber bundle was tested by means of IGC under different conditions to find reliable test parameters. The main parameters involved include length, mass, and packing density of sample, target fractional surface coverage, flow rate, and maximum elution time. It is demonstrated that IGC has the advantages of simple sample preparation, stable test data, high automation, and high sensitivity for carbon fiber. Among all test conditions, packing density and flow rate have the greatest influences on the experimental results. The optimized test parameters are suitable for various kinds of carbon fiber bundles, including polyacrylonitrile-based and pitch-based carbon fibers with different tensile properties and tow sizes. Moreover, IGC can acutely characterize the surface properties of carbon fibers after carbon nanotube modification and heat treatment, which are hard to carry out using contact angle method.</description><identifier>ISSN: 1976-4251</identifier><identifier>EISSN: 2233-4998</identifier><identifier>DOI: 10.1007/s42823-023-00472-9</identifier><language>eng</language><publisher>Singapore: Springer Nature Singapore</publisher><subject>Adsorption ; Automation ; Carbon ; Carbon fiber reinforced plastics ; Carbon fibers ; Carbon nanotubes ; Characterization and Evaluation of Materials ; Chemistry and Materials Science ; Chromatography ; Composite materials ; Contact angle ; Energy ; Fiber composites ; Fiber reinforced polymers ; Fibers ; Flow rates ; Flow velocity ; Free energy ; Gas chromatography ; Heat ; Heat treatment ; Heat treatments ; Interfacial properties ; Inverse gas chromatography ; Materials Engineering ; Materials Science ; Nanotechnology ; Original Article ; Packing density ; Parameters ; Polyacrylonitrile ; Polymer matrix composites ; Polymers ; Retention ; Sample preparation ; Surface energy ; Surface properties ; Tensile properties</subject><ispartof>Carbon Letters, 2023-05, Vol.33 (3), p.909-920</ispartof><rights>The Author(s), under exclusive licence to Korean Carbon Society 2023. Springer Nature or its licensor (e.g. a society or other partner) holds exclusive rights to this article under a publishing agreement with the author(s) or other rightsholder(s); author self-archiving of the accepted manuscript version of this article is solely governed by the terms of such publishing agreement and applicable law.</rights><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c347t-29938854f52c36966b07dbf2b8c958fbac43a62ca60424f968b470f10035723e3</citedby><cites>FETCH-LOGICAL-c347t-29938854f52c36966b07dbf2b8c958fbac43a62ca60424f968b470f10035723e3</cites><orcidid>0000-0001-8614-5179</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktohtml>$$Uhttps://www.proquest.com/docview/2921225913?pq-origsite=primo$$EHTML$$P50$$Gproquest$$H</linktohtml><link.rule.ids>314,780,784,21388,21389,21390,21391,23256,27924,27925,33530,33703,33744,34005,34314,43659,43787,43805,43953,44067,64385,64389,72469</link.rule.ids></links><search><creatorcontrib>Liu, Yuwei</creatorcontrib><creatorcontrib>Gu, Yizhuo</creatorcontrib><creatorcontrib>Wang, Shaokai</creatorcontrib><creatorcontrib>Li, Min</creatorcontrib><title>Optimization for testing conditions of inverse gas chromatography and surface energies of various carbon fiber bundles</title><title>Carbon Letters</title><addtitle>Carbon Lett</addtitle><description>Surface free energy is an important parameter in surface and interface properties of fiber reinforced polymer composite. The BET (Brunauer, Emmett, and Teller) surface area and surface energy of the sample can be obtained by Inverse Gas Chromatography (IGC) based on the adsorption principle. In this paper, surface energy of carbon fiber bundle was tested by means of IGC under different conditions to find reliable test parameters. The main parameters involved include length, mass, and packing density of sample, target fractional surface coverage, flow rate, and maximum elution time. It is demonstrated that IGC has the advantages of simple sample preparation, stable test data, high automation, and high sensitivity for carbon fiber. Among all test conditions, packing density and flow rate have the greatest influences on the experimental results. The optimized test parameters are suitable for various kinds of carbon fiber bundles, including polyacrylonitrile-based and pitch-based carbon fibers with different tensile properties and tow sizes. Moreover, IGC can acutely characterize the surface properties of carbon fibers after carbon nanotube modification and heat treatment, which are hard to carry out using contact angle method.</description><subject>Adsorption</subject><subject>Automation</subject><subject>Carbon</subject><subject>Carbon fiber reinforced plastics</subject><subject>Carbon fibers</subject><subject>Carbon nanotubes</subject><subject>Characterization and Evaluation of Materials</subject><subject>Chemistry and Materials Science</subject><subject>Chromatography</subject><subject>Composite materials</subject><subject>Contact angle</subject><subject>Energy</subject><subject>Fiber composites</subject><subject>Fiber reinforced polymers</subject><subject>Fibers</subject><subject>Flow rates</subject><subject>Flow velocity</subject><subject>Free energy</subject><subject>Gas chromatography</subject><subject>Heat</subject><subject>Heat treatment</subject><subject>Heat treatments</subject><subject>Interfacial properties</subject><subject>Inverse gas chromatography</subject><subject>Materials Engineering</subject><subject>Materials Science</subject><subject>Nanotechnology</subject><subject>Original Article</subject><subject>Packing density</subject><subject>Parameters</subject><subject>Polyacrylonitrile</subject><subject>Polymer matrix composites</subject><subject>Polymers</subject><subject>Retention</subject><subject>Sample preparation</subject><subject>Surface energy</subject><subject>Surface properties</subject><subject>Tensile properties</subject><issn>1976-4251</issn><issn>2233-4998</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>ABUWG</sourceid><sourceid>AFKRA</sourceid><sourceid>AZQEC</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><sourceid>GNUQQ</sourceid><recordid>eNp9kU1LAzEURYMoWLR_wFXA9WjykvnIUopfUHCj6yFJk2m0TerLTEF_vTNW0JWLRyCcc0PeJeSCsyvOWH2dJTQgCjYNkzUU6ojMAIQopFLNMZlxVVeFhJKfknnOwYySYIqJakb2T7s-bMOn7kOK1Cekvct9iB21Ka7CdJtp8jTEvcPsaKcztWtMW92nDvVu_UF1XNE8oNfWURcddsF9K3uNIQ0jrtFM2cE4pGaIq43L5-TE601285_zjLzc3T4vHorl0_3j4mZZWCHrvgClRNOU0pdgRaWqyrB6ZTyYxqqy8UZbKXQFVldMgvSqaoysmR-3IsoahBNn5PKQu8P0Pow_a1_TgHF8sgUFHKBUXPxSbwmdznadNhp_yXG9nKuRggNlMeWMzrc7DFuNHy1n7VREeyiiZdNMRbSTJA5SHuHYuT-x_1hfyO-MdA</recordid><startdate>20230501</startdate><enddate>20230501</enddate><creator>Liu, Yuwei</creator><creator>Gu, Yizhuo</creator><creator>Wang, Shaokai</creator><creator>Li, Min</creator><general>Springer Nature Singapore</general><general>한국탄소학회</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>KROLR</scope><scope>3V.</scope><scope>7XB</scope><scope>88I</scope><scope>8FE</scope><scope>8FG</scope><scope>8FK</scope><scope>ABJCF</scope><scope>ABUWG</scope><scope>AFKRA</scope><scope>ATCPS</scope><scope>AZQEC</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>GNUQQ</scope><scope>HCIFZ</scope><scope>KB.</scope><scope>L6V</scope><scope>M2P</scope><scope>M7S</scope><scope>PATMY</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><scope>PYCSY</scope><scope>Q9U</scope><orcidid>https://orcid.org/0000-0001-8614-5179</orcidid></search><sort><creationdate>20230501</creationdate><title>Optimization for testing conditions of inverse gas chromatography and surface energies of various carbon fiber bundles</title><author>Liu, Yuwei ; Gu, Yizhuo ; Wang, Shaokai ; Li, Min</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c347t-29938854f52c36966b07dbf2b8c958fbac43a62ca60424f968b470f10035723e3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Adsorption</topic><topic>Automation</topic><topic>Carbon</topic><topic>Carbon fiber reinforced plastics</topic><topic>Carbon fibers</topic><topic>Carbon nanotubes</topic><topic>Characterization and Evaluation of Materials</topic><topic>Chemistry and Materials Science</topic><topic>Chromatography</topic><topic>Composite materials</topic><topic>Contact angle</topic><topic>Energy</topic><topic>Fiber composites</topic><topic>Fiber reinforced polymers</topic><topic>Fibers</topic><topic>Flow rates</topic><topic>Flow velocity</topic><topic>Free energy</topic><topic>Gas chromatography</topic><topic>Heat</topic><topic>Heat treatment</topic><topic>Heat treatments</topic><topic>Interfacial properties</topic><topic>Inverse gas chromatography</topic><topic>Materials Engineering</topic><topic>Materials Science</topic><topic>Nanotechnology</topic><topic>Original Article</topic><topic>Packing density</topic><topic>Parameters</topic><topic>Polyacrylonitrile</topic><topic>Polymer matrix composites</topic><topic>Polymers</topic><topic>Retention</topic><topic>Sample preparation</topic><topic>Surface energy</topic><topic>Surface properties</topic><topic>Tensile properties</topic><toplevel>online_resources</toplevel><creatorcontrib>Liu, Yuwei</creatorcontrib><creatorcontrib>Gu, Yizhuo</creatorcontrib><creatorcontrib>Wang, Shaokai</creatorcontrib><creatorcontrib>Li, Min</creatorcontrib><collection>CrossRef</collection><collection>Korea Scholar</collection><collection>ProQuest Central (Corporate)</collection><collection>ProQuest Central (purchase pre-March 2016)</collection><collection>Science Database (Alumni Edition)</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>ProQuest Central (Alumni) (purchase pre-March 2016)</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central (Alumni Edition)</collection><collection>ProQuest Central UK/Ireland</collection><collection>Agricultural & Environmental Science Collection</collection><collection>ProQuest Central Essentials</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>ProQuest Central Student</collection><collection>SciTech Premium Collection</collection><collection>Materials Science Database</collection><collection>ProQuest Engineering Collection</collection><collection>Science Database</collection><collection>Engineering Database</collection><collection>Environmental Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><collection>Environmental Science Collection</collection><collection>ProQuest Central Basic</collection><jtitle>Carbon Letters</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Liu, Yuwei</au><au>Gu, Yizhuo</au><au>Wang, Shaokai</au><au>Li, Min</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Optimization for testing conditions of inverse gas chromatography and surface energies of various carbon fiber bundles</atitle><jtitle>Carbon Letters</jtitle><stitle>Carbon Lett</stitle><date>2023-05-01</date><risdate>2023</risdate><volume>33</volume><issue>3</issue><spage>909</spage><epage>920</epage><pages>909-920</pages><issn>1976-4251</issn><eissn>2233-4998</eissn><abstract>Surface free energy is an important parameter in surface and interface properties of fiber reinforced polymer composite. The BET (Brunauer, Emmett, and Teller) surface area and surface energy of the sample can be obtained by Inverse Gas Chromatography (IGC) based on the adsorption principle. In this paper, surface energy of carbon fiber bundle was tested by means of IGC under different conditions to find reliable test parameters. The main parameters involved include length, mass, and packing density of sample, target fractional surface coverage, flow rate, and maximum elution time. It is demonstrated that IGC has the advantages of simple sample preparation, stable test data, high automation, and high sensitivity for carbon fiber. Among all test conditions, packing density and flow rate have the greatest influences on the experimental results. The optimized test parameters are suitable for various kinds of carbon fiber bundles, including polyacrylonitrile-based and pitch-based carbon fibers with different tensile properties and tow sizes. Moreover, IGC can acutely characterize the surface properties of carbon fibers after carbon nanotube modification and heat treatment, which are hard to carry out using contact angle method.</abstract><cop>Singapore</cop><pub>Springer Nature Singapore</pub><doi>10.1007/s42823-023-00472-9</doi><tpages>12</tpages><orcidid>https://orcid.org/0000-0001-8614-5179</orcidid></addata></record> |
| fulltext | fulltext |
| identifier | ISSN: 1976-4251 |
| ispartof | Carbon Letters, 2023-05, Vol.33 (3), p.909-920 |
| issn | 1976-4251 2233-4998 |
| language | eng |
| recordid | cdi_proquest_journals_2921225913 |
| source | ProQuest Central Essentials; ProQuest Central (Alumni Edition); ProQuest Central Student; ProQuest Central Korea; ProQuest Central UK/Ireland; SpringerLink Journals - AutoHoldings; ProQuest Central |
| subjects | Adsorption Automation Carbon Carbon fiber reinforced plastics Carbon fibers Carbon nanotubes Characterization and Evaluation of Materials Chemistry and Materials Science Chromatography Composite materials Contact angle Energy Fiber composites Fiber reinforced polymers Fibers Flow rates Flow velocity Free energy Gas chromatography Heat Heat treatment Heat treatments Interfacial properties Inverse gas chromatography Materials Engineering Materials Science Nanotechnology Original Article Packing density Parameters Polyacrylonitrile Polymer matrix composites Polymers Retention Sample preparation Surface energy Surface properties Tensile properties |
| title | Optimization for testing conditions of inverse gas chromatography and surface energies of various carbon fiber bundles |
| url | https://sfx.bib-bvb.de/sfx_tum?ctx_ver=Z39.88-2004&ctx_enc=info:ofi/enc:UTF-8&ctx_tim=2025-01-02T08%3A08%3A24IST&url_ver=Z39.88-2004&url_ctx_fmt=infofi/fmt:kev:mtx:ctx&rfr_id=info:sid/primo.exlibrisgroup.com:primo3-Article-proquest_korea&rft_val_fmt=info:ofi/fmt:kev:mtx:journal&rft.genre=article&rft.atitle=Optimization%20for%20testing%20conditions%20of%20inverse%20gas%20chromatography%20and%20surface%20energies%20of%20various%20carbon%20fiber%20bundles&rft.jtitle=Carbon%20Letters&rft.au=Liu,%20Yuwei&rft.date=2023-05-01&rft.volume=33&rft.issue=3&rft.spage=909&rft.epage=920&rft.pages=909-920&rft.issn=1976-4251&rft.eissn=2233-4998&rft_id=info:doi/10.1007/s42823-023-00472-9&rft_dat=%3Cproquest_korea%3E2921225913%3C/proquest_korea%3E%3Curl%3E%3C/url%3E&disable_directlink=true&sfx.directlink=off&sfx.report_link=0&rft_id=info:oai/&rft_pqid=2921225913&rft_id=info:pmid/&rfr_iscdi=true |