Investigation of slip systems activity and grain boundary sliding in fine-grained superplastic zinc alloy
Zn alloys are desirable candidates for biodegradable materials due to their great biocompatibility and sufficient mechanical properties. Nevertheless, the most popular strengthening method by grain refinement after cold processing is usually ineffective in Zn alloys. Besides highly anisotropic defor...
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| Veröffentlicht in: | Archives of Civil and Mechanical Engineering 2023-10, Vol.23 (4), p.253, Article 253 |
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| creator | Bednarczyk, Wiktor Kawałko, Jakub Wątroba, Maria Szuwarzyński, Michał Bała, Piotr |
| description | Zn alloys are desirable candidates for biodegradable materials due to their great biocompatibility and sufficient mechanical properties. Nevertheless, the most popular strengthening method by grain refinement after cold processing is usually ineffective in Zn alloys. Besides highly anisotropic deformation through a dislocation slip, grain boundary sliding (GBS) plays an important role in total deformation in fine-grained Zn alloys at room temperature (RT). Herein, Zn–0.5Cu (wt. %) alloy is fabricated by RT equal channel angular pressing, and its deformation mechanisms in tension were systematically analyzed at strain rates from 10
–4
s
−1
to 10
0
s
−1
. GBS contribution in total deformation was measured using surface markers and atomic force microscopy. In addition, dislocation slip activity was evaluated via electron-backscattered diffraction-based slip trace analysis. As a result, investigated alloy presents the GBS contribution in a total deformation at RT from 35% at the strain rate 10
0
s
−1
to 70% at 10
–4
s
−1
. Simultaneously, the number of slip-deformed grains decreased from 97.5% to 8%. Moreover, the basal slip system was dominant at all strain rates, while the prismatic and the pyramidal slip systems were activated at the higher strain rates. The results presented here for the first time clearly show the complexity of deformation mechanisms in fine-grained Zn–0.5Cu, at significantly different strain rate conditions. |
| doi_str_mv | 10.1007/s43452-023-00793-6 |
| format | Article |
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–4
s
−1
to 10
0
s
−1
. GBS contribution in total deformation was measured using surface markers and atomic force microscopy. In addition, dislocation slip activity was evaluated via electron-backscattered diffraction-based slip trace analysis. As a result, investigated alloy presents the GBS contribution in a total deformation at RT from 35% at the strain rate 10
0
s
−1
to 70% at 10
–4
s
−1
. Simultaneously, the number of slip-deformed grains decreased from 97.5% to 8%. Moreover, the basal slip system was dominant at all strain rates, while the prismatic and the pyramidal <
c
+
a
> slip systems were activated at the higher strain rates. The results presented here for the first time clearly show the complexity of deformation mechanisms in fine-grained Zn–0.5Cu, at significantly different strain rate conditions.</description><identifier>ISSN: 2083-3318</identifier><identifier>ISSN: 1644-9665</identifier><identifier>EISSN: 2083-3318</identifier><identifier>DOI: 10.1007/s43452-023-00793-6</identifier><language>eng</language><publisher>London: Springer London</publisher><subject>Alloys ; Biocompatibility ; Civil Engineering ; Deformation ; Deformation mechanisms ; Ductility ; Engineering ; Equal channel angular pressing ; Geometry ; Grain boundaries ; Grain boundary sliding ; Grain refinement ; Grain size ; Investigations ; Mechanical Engineering ; Mechanical properties ; Original Article ; Room temperature ; Slip ; Strain analysis ; Strain rate ; Structural Materials ; Superplasticity ; Zinc base alloys</subject><ispartof>Archives of Civil and Mechanical Engineering, 2023-10, Vol.23 (4), p.253, Article 253</ispartof><rights>The Author(s) 2023</rights><rights>The Author(s) 2023. This work is published under http://creativecommons.org/licenses/by/4.0/ (the “License”). Notwithstanding the ProQuest Terms and Conditions, you may use this content in accordance with the terms of the License.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c363t-7500693af91b364d49d08f48cacbf2f1fae72bc5ab3fcfe32736bcc2d203c78a3</citedby><cites>FETCH-LOGICAL-c363t-7500693af91b364d49d08f48cacbf2f1fae72bc5ab3fcfe32736bcc2d203c78a3</cites><orcidid>0000-0003-0001-1693</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://link.springer.com/content/pdf/10.1007/s43452-023-00793-6$$EPDF$$P50$$Gspringer$$Hfree_for_read</linktopdf><linktohtml>$$Uhttps://www.proquest.com/docview/2921060580?pq-origsite=primo$$EHTML$$P50$$Gproquest$$H</linktohtml><link.rule.ids>314,780,784,21387,27923,27924,33743,41487,42556,43804,51318,64384,64388,72240</link.rule.ids></links><search><creatorcontrib>Bednarczyk, Wiktor</creatorcontrib><creatorcontrib>Kawałko, Jakub</creatorcontrib><creatorcontrib>Wątroba, Maria</creatorcontrib><creatorcontrib>Szuwarzyński, Michał</creatorcontrib><creatorcontrib>Bała, Piotr</creatorcontrib><title>Investigation of slip systems activity and grain boundary sliding in fine-grained superplastic zinc alloy</title><title>Archives of Civil and Mechanical Engineering</title><addtitle>Archiv.Civ.Mech.Eng</addtitle><description>Zn alloys are desirable candidates for biodegradable materials due to their great biocompatibility and sufficient mechanical properties. Nevertheless, the most popular strengthening method by grain refinement after cold processing is usually ineffective in Zn alloys. Besides highly anisotropic deformation through a dislocation slip, grain boundary sliding (GBS) plays an important role in total deformation in fine-grained Zn alloys at room temperature (RT). Herein, Zn–0.5Cu (wt. %) alloy is fabricated by RT equal channel angular pressing, and its deformation mechanisms in tension were systematically analyzed at strain rates from 10
–4
s
−1
to 10
0
s
−1
. GBS contribution in total deformation was measured using surface markers and atomic force microscopy. In addition, dislocation slip activity was evaluated via electron-backscattered diffraction-based slip trace analysis. As a result, investigated alloy presents the GBS contribution in a total deformation at RT from 35% at the strain rate 10
0
s
−1
to 70% at 10
–4
s
−1
. Simultaneously, the number of slip-deformed grains decreased from 97.5% to 8%. Moreover, the basal slip system was dominant at all strain rates, while the prismatic and the pyramidal <
c
+
a
> slip systems were activated at the higher strain rates. The results presented here for the first time clearly show the complexity of deformation mechanisms in fine-grained Zn–0.5Cu, at significantly different strain rate conditions.</description><subject>Alloys</subject><subject>Biocompatibility</subject><subject>Civil Engineering</subject><subject>Deformation</subject><subject>Deformation mechanisms</subject><subject>Ductility</subject><subject>Engineering</subject><subject>Equal channel angular pressing</subject><subject>Geometry</subject><subject>Grain boundaries</subject><subject>Grain boundary sliding</subject><subject>Grain refinement</subject><subject>Grain size</subject><subject>Investigations</subject><subject>Mechanical Engineering</subject><subject>Mechanical properties</subject><subject>Original Article</subject><subject>Room temperature</subject><subject>Slip</subject><subject>Strain analysis</subject><subject>Strain rate</subject><subject>Structural Materials</subject><subject>Superplasticity</subject><subject>Zinc base alloys</subject><issn>2083-3318</issn><issn>1644-9665</issn><issn>2083-3318</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2023</creationdate><recordtype>article</recordtype><sourceid>C6C</sourceid><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9UE1LxDAUDKLgsu4f8BTwHH1J2rQ9yuLHwoIXPYc0TUqWblqT7kL99Wa3gp48va-ZecwgdEvhngIUDzHjWc4IME7SWHEiLtCCQckJ57S8_NNfo1WMOwCgUDAq8gVyG380cXStGl3vcW9x7NyA4xRHs49Y6dEd3Thh5RvcBuU8rvuDb1SYTsDG-RannXXekPPZNDgeBhOGTiVVjb-c11h1XT_doCurumhWP3WJPp6f3tevZPv2slk_bonmgo-kyAFExZWtaM1F1mRVA6XNSq10bZmlVpmC1TpXNbfaGs4KLmqtWcOA66JUfInuZt0h9J-H5E3u-kPw6aVkFaMgIC8hodiM0qGPMRgrh-D2yZakIE-pyjlVmVKV51SlSCQ-k2IC-9aEX-l_WN9L0nyW</recordid><startdate>20231023</startdate><enddate>20231023</enddate><creator>Bednarczyk, Wiktor</creator><creator>Kawałko, Jakub</creator><creator>Wątroba, Maria</creator><creator>Szuwarzyński, Michał</creator><creator>Bała, Piotr</creator><general>Springer London</general><general>Springer Nature B.V</general><scope>C6C</scope><scope>AAYXX</scope><scope>CITATION</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>L6V</scope><scope>M7S</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope><orcidid>https://orcid.org/0000-0003-0001-1693</orcidid></search><sort><creationdate>20231023</creationdate><title>Investigation of slip systems activity and grain boundary sliding in fine-grained superplastic zinc alloy</title><author>Bednarczyk, Wiktor ; Kawałko, Jakub ; Wątroba, Maria ; Szuwarzyński, Michał ; Bała, Piotr</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c363t-7500693af91b364d49d08f48cacbf2f1fae72bc5ab3fcfe32736bcc2d203c78a3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2023</creationdate><topic>Alloys</topic><topic>Biocompatibility</topic><topic>Civil Engineering</topic><topic>Deformation</topic><topic>Deformation mechanisms</topic><topic>Ductility</topic><topic>Engineering</topic><topic>Equal channel angular pressing</topic><topic>Geometry</topic><topic>Grain boundaries</topic><topic>Grain boundary sliding</topic><topic>Grain refinement</topic><topic>Grain size</topic><topic>Investigations</topic><topic>Mechanical Engineering</topic><topic>Mechanical properties</topic><topic>Original Article</topic><topic>Room temperature</topic><topic>Slip</topic><topic>Strain analysis</topic><topic>Strain rate</topic><topic>Structural Materials</topic><topic>Superplasticity</topic><topic>Zinc base alloys</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Bednarczyk, Wiktor</creatorcontrib><creatorcontrib>Kawałko, Jakub</creatorcontrib><creatorcontrib>Wątroba, Maria</creatorcontrib><creatorcontrib>Szuwarzyński, Michał</creatorcontrib><creatorcontrib>Bała, Piotr</creatorcontrib><collection>Springer Nature OA Free Journals</collection><collection>CrossRef</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><jtitle>Archives of Civil and Mechanical Engineering</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Bednarczyk, Wiktor</au><au>Kawałko, Jakub</au><au>Wątroba, Maria</au><au>Szuwarzyński, Michał</au><au>Bała, Piotr</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Investigation of slip systems activity and grain boundary sliding in fine-grained superplastic zinc alloy</atitle><jtitle>Archives of Civil and Mechanical Engineering</jtitle><stitle>Archiv.Civ.Mech.Eng</stitle><date>2023-10-23</date><risdate>2023</risdate><volume>23</volume><issue>4</issue><spage>253</spage><pages>253-</pages><artnum>253</artnum><issn>2083-3318</issn><issn>1644-9665</issn><eissn>2083-3318</eissn><abstract>Zn alloys are desirable candidates for biodegradable materials due to their great biocompatibility and sufficient mechanical properties. Nevertheless, the most popular strengthening method by grain refinement after cold processing is usually ineffective in Zn alloys. Besides highly anisotropic deformation through a dislocation slip, grain boundary sliding (GBS) plays an important role in total deformation in fine-grained Zn alloys at room temperature (RT). Herein, Zn–0.5Cu (wt. %) alloy is fabricated by RT equal channel angular pressing, and its deformation mechanisms in tension were systematically analyzed at strain rates from 10
–4
s
−1
to 10
0
s
−1
. GBS contribution in total deformation was measured using surface markers and atomic force microscopy. In addition, dislocation slip activity was evaluated via electron-backscattered diffraction-based slip trace analysis. As a result, investigated alloy presents the GBS contribution in a total deformation at RT from 35% at the strain rate 10
0
s
−1
to 70% at 10
–4
s
−1
. Simultaneously, the number of slip-deformed grains decreased from 97.5% to 8%. Moreover, the basal slip system was dominant at all strain rates, while the prismatic and the pyramidal <
c
+
a
> slip systems were activated at the higher strain rates. The results presented here for the first time clearly show the complexity of deformation mechanisms in fine-grained Zn–0.5Cu, at significantly different strain rate conditions.</abstract><cop>London</cop><pub>Springer London</pub><doi>10.1007/s43452-023-00793-6</doi><orcidid>https://orcid.org/0000-0003-0001-1693</orcidid><oa>free_for_read</oa></addata></record> |
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| subjects | Alloys Biocompatibility Civil Engineering Deformation Deformation mechanisms Ductility Engineering Equal channel angular pressing Geometry Grain boundaries Grain boundary sliding Grain refinement Grain size Investigations Mechanical Engineering Mechanical properties Original Article Room temperature Slip Strain analysis Strain rate Structural Materials Superplasticity Zinc base alloys |
| title | Investigation of slip systems activity and grain boundary sliding in fine-grained superplastic zinc alloy |
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