An investigation of the formation, the particulate properties and the rheological behaviour of cerium vanadate and zirconium titanate prepared by dicarboxylate coprecipitation method
Cerium vanadate (CeVO 4 ) and zirconium titanate (ZrTiO 4 ) powders have been synthesized by the dicarboxylate coprecipitation method. The formation of precursors and mixed oxides was confirmed by their elemental and thermal analysis (thermogravimetric analysis–differential thermal analysis), infrar...
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| Veröffentlicht in: | Bulletin of materials science 2022-06, Vol.45 (2), p.92, Article 92 |
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| creator | Nagawade, A V Nikumbh, A K Karale, N J Khanvilkar, M B Deshpande, A S Nagwade, P A |
| description | Cerium vanadate (CeVO
4
) and zirconium titanate (ZrTiO
4
) powders have been synthesized by the dicarboxylate coprecipitation method. The formation of precursors and mixed oxides was confirmed by their elemental and thermal analysis (thermogravimetric analysis–differential thermal analysis), infrared spectroscopy (Fourier transform infrared), X-ray fluorescence spectroscopy, energy-dispersive X-ray analysis and powder X-ray diffraction. X-ray analysis reveals the formation of a single-phasic CeVO
4
with tetragonal structure and ZrTiO
4
with orthorhombic structure. The morphological characteristics of these oxides were studied by field-emission scanning electron microscopy and a laser-based particle size analyzer. Different solid content and dispersants have been used to prepare various suspensions of these oxides in distilled water and ethanol. The rheological flow behaviour of the suspensions has been studied by measuring their viscosity against the increasing shear rate. The power-law model is applied to calculate consistency coefficient (
k
) and flow behaviour index (
n
). Minimum viscosities have been observed at pH = 10.6 for CeVO
4
–water–Darvan system and at pH = 10.5 for ZrTiO
4
–water–polyethylene imine system.
Graphic abstract |
| doi_str_mv | 10.1007/s12034-021-02641-w |
| format | Article |
| fullrecord | <record><control><sourceid>proquest_cross</sourceid><recordid>TN_cdi_proquest_journals_2920223591</recordid><sourceformat>XML</sourceformat><sourcesystem>PC</sourcesystem><sourcerecordid>2920223591</sourcerecordid><originalsourceid>FETCH-LOGICAL-c234w-e9fe67e771659e65067b4ad7f2d53f689bf571d55e8d613ecc43fdbec97565683</originalsourceid><addsrcrecordid>eNp9UctuGyEUHVWpVMftD3SF1G2n4TGAWVpRk1aylE26RgxcPFj24MLYjvNh-b4y40rJKgvEfZxzLpdTVV8J_kEwljeZUMyaGlNSjmhIffpQzbCSrJZCqKs38afqOucNxkQ1DZlVL8sehf4IeQhrM4TYo-jR0AHyMe2mwvcp3Zs0BHvYmqHEKe6hpJCR6d3UTh3EbVwHa7aohc4cQzykUcpCCocdOpreuJE7Ep5DsrEfy0MYSmOShDIBHGrPyBWV1Man8zTMxtKzYV-Q0_N2MHTRfa4-erPN8OX_Pa_-3P18vP1Vrx7uf98uV7WlrDnVoDwICVISwRUIjoVsG-Okp44zLxaq9VwSxzksnCAMrG2Ydy1YJbngYsHm1beLbtn576H8kt6UxfoyUlNFMaWMK1JQ9IKyKeacwOt9CjuTzppgPfqjL_7o4o-e_NGnQmIXUi7gfg3pVfod1j-KApmn</addsrcrecordid><sourcetype>Aggregation Database</sourcetype><iscdi>true</iscdi><recordtype>article</recordtype><pqid>2920223591</pqid></control><display><type>article</type><title>An investigation of the formation, the particulate properties and the rheological behaviour of cerium vanadate and zirconium titanate prepared by dicarboxylate coprecipitation method</title><source>Indian Academy of Sciences</source><source>SpringerLink</source><source>Free Full-Text Journals in Chemistry</source><source>EZB Electronic Journals Library</source><source>ProQuest Central</source><creator>Nagawade, A V ; Nikumbh, A K ; Karale, N J ; Khanvilkar, M B ; Deshpande, A S ; Nagwade, P A</creator><creatorcontrib>Nagawade, A V ; Nikumbh, A K ; Karale, N J ; Khanvilkar, M B ; Deshpande, A S ; Nagwade, P A</creatorcontrib><description>Cerium vanadate (CeVO
4
) and zirconium titanate (ZrTiO
4
) powders have been synthesized by the dicarboxylate coprecipitation method. The formation of precursors and mixed oxides was confirmed by their elemental and thermal analysis (thermogravimetric analysis–differential thermal analysis), infrared spectroscopy (Fourier transform infrared), X-ray fluorescence spectroscopy, energy-dispersive X-ray analysis and powder X-ray diffraction. X-ray analysis reveals the formation of a single-phasic CeVO
4
with tetragonal structure and ZrTiO
4
with orthorhombic structure. The morphological characteristics of these oxides were studied by field-emission scanning electron microscopy and a laser-based particle size analyzer. Different solid content and dispersants have been used to prepare various suspensions of these oxides in distilled water and ethanol. The rheological flow behaviour of the suspensions has been studied by measuring their viscosity against the increasing shear rate. The power-law model is applied to calculate consistency coefficient (
k
) and flow behaviour index (
n
). Minimum viscosities have been observed at pH = 10.6 for CeVO
4
–water–Darvan system and at pH = 10.5 for ZrTiO
4
–water–polyethylene imine system.
Graphic abstract</description><identifier>ISSN: 0973-7669</identifier><identifier>ISSN: 0250-4707</identifier><identifier>EISSN: 0973-7669</identifier><identifier>DOI: 10.1007/s12034-021-02641-w</identifier><language>eng</language><publisher>Bangalore: Indian Academy of Sciences</publisher><subject>Cerium compounds ; Chemistry and Materials Science ; Coprecipitation ; Decomposition ; Differential thermal analysis ; Dispersants ; Distilled water ; Emission analysis ; Energy dispersive X ray analysis ; Engineering ; Ethanol ; Fourier transforms ; Infrared analysis ; Infrared spectroscopy ; Investigations ; Laser applications ; Materials Science ; Mixed oxides ; Particle size ; Polyethylene ; Rheological properties ; Rheology ; Sedimentation & deposition ; Sensors ; Shear rate ; Spectroscopic analysis ; Spectrum analysis ; Thermogravimetric analysis ; Titanium ; Vanadates ; Viscosity ; X ray analysis ; X ray powder diffraction ; X-ray fluorescence ; Zirconium ; Zirconium titanates</subject><ispartof>Bulletin of materials science, 2022-06, Vol.45 (2), p.92, Article 92</ispartof><rights>Indian Academy of Sciences 2022</rights><rights>Indian Academy of Sciences 2022.</rights><lds50>peer_reviewed</lds50><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c234w-e9fe67e771659e65067b4ad7f2d53f689bf571d55e8d613ecc43fdbec97565683</citedby><cites>FETCH-LOGICAL-c234w-e9fe67e771659e65067b4ad7f2d53f689bf571d55e8d613ecc43fdbec97565683</cites><orcidid>0000-0003-1036-7079</orcidid></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.proquest.com/docview/2920223591/fulltextPDF?pq-origsite=primo$$EPDF$$P50$$Gproquest$$H</linktopdf><linktohtml>$$Uhttps://www.proquest.com/docview/2920223591?pq-origsite=primo$$EHTML$$P50$$Gproquest$$H</linktohtml><link.rule.ids>314,780,784,21386,27922,27923,33742,41486,42555,43803,51317,64383,64387,72239,74072</link.rule.ids></links><search><creatorcontrib>Nagawade, A V</creatorcontrib><creatorcontrib>Nikumbh, A K</creatorcontrib><creatorcontrib>Karale, N J</creatorcontrib><creatorcontrib>Khanvilkar, M B</creatorcontrib><creatorcontrib>Deshpande, A S</creatorcontrib><creatorcontrib>Nagwade, P A</creatorcontrib><title>An investigation of the formation, the particulate properties and the rheological behaviour of cerium vanadate and zirconium titanate prepared by dicarboxylate coprecipitation method</title><title>Bulletin of materials science</title><addtitle>Bull Mater Sci</addtitle><description>Cerium vanadate (CeVO
4
) and zirconium titanate (ZrTiO
4
) powders have been synthesized by the dicarboxylate coprecipitation method. The formation of precursors and mixed oxides was confirmed by their elemental and thermal analysis (thermogravimetric analysis–differential thermal analysis), infrared spectroscopy (Fourier transform infrared), X-ray fluorescence spectroscopy, energy-dispersive X-ray analysis and powder X-ray diffraction. X-ray analysis reveals the formation of a single-phasic CeVO
4
with tetragonal structure and ZrTiO
4
with orthorhombic structure. The morphological characteristics of these oxides were studied by field-emission scanning electron microscopy and a laser-based particle size analyzer. Different solid content and dispersants have been used to prepare various suspensions of these oxides in distilled water and ethanol. The rheological flow behaviour of the suspensions has been studied by measuring their viscosity against the increasing shear rate. The power-law model is applied to calculate consistency coefficient (
k
) and flow behaviour index (
n
). Minimum viscosities have been observed at pH = 10.6 for CeVO
4
–water–Darvan system and at pH = 10.5 for ZrTiO
4
–water–polyethylene imine system.
Graphic abstract</description><subject>Cerium compounds</subject><subject>Chemistry and Materials Science</subject><subject>Coprecipitation</subject><subject>Decomposition</subject><subject>Differential thermal analysis</subject><subject>Dispersants</subject><subject>Distilled water</subject><subject>Emission analysis</subject><subject>Energy dispersive X ray analysis</subject><subject>Engineering</subject><subject>Ethanol</subject><subject>Fourier transforms</subject><subject>Infrared analysis</subject><subject>Infrared spectroscopy</subject><subject>Investigations</subject><subject>Laser applications</subject><subject>Materials Science</subject><subject>Mixed oxides</subject><subject>Particle size</subject><subject>Polyethylene</subject><subject>Rheological properties</subject><subject>Rheology</subject><subject>Sedimentation & deposition</subject><subject>Sensors</subject><subject>Shear rate</subject><subject>Spectroscopic analysis</subject><subject>Spectrum analysis</subject><subject>Thermogravimetric analysis</subject><subject>Titanium</subject><subject>Vanadates</subject><subject>Viscosity</subject><subject>X ray analysis</subject><subject>X ray powder diffraction</subject><subject>X-ray fluorescence</subject><subject>Zirconium</subject><subject>Zirconium titanates</subject><issn>0973-7669</issn><issn>0250-4707</issn><issn>0973-7669</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2022</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp9UctuGyEUHVWpVMftD3SF1G2n4TGAWVpRk1aylE26RgxcPFj24MLYjvNh-b4y40rJKgvEfZxzLpdTVV8J_kEwljeZUMyaGlNSjmhIffpQzbCSrJZCqKs38afqOucNxkQ1DZlVL8sehf4IeQhrM4TYo-jR0AHyMe2mwvcp3Zs0BHvYmqHEKe6hpJCR6d3UTh3EbVwHa7aohc4cQzykUcpCCocdOpreuJE7Ep5DsrEfy0MYSmOShDIBHGrPyBWV1Man8zTMxtKzYV-Q0_N2MHTRfa4-erPN8OX_Pa_-3P18vP1Vrx7uf98uV7WlrDnVoDwICVISwRUIjoVsG-Okp44zLxaq9VwSxzksnCAMrG2Ydy1YJbngYsHm1beLbtn576H8kt6UxfoyUlNFMaWMK1JQ9IKyKeacwOt9CjuTzppgPfqjL_7o4o-e_NGnQmIXUi7gfg3pVfod1j-KApmn</recordid><startdate>20220601</startdate><enddate>20220601</enddate><creator>Nagawade, A V</creator><creator>Nikumbh, A K</creator><creator>Karale, N J</creator><creator>Khanvilkar, M B</creator><creator>Deshpande, A S</creator><creator>Nagwade, P A</creator><general>Indian Academy of Sciences</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><orcidid>https://orcid.org/0000-0003-1036-7079</orcidid></search><sort><creationdate>20220601</creationdate><title>An investigation of the formation, the particulate properties and the rheological behaviour of cerium vanadate and zirconium titanate prepared by dicarboxylate coprecipitation method</title><author>Nagawade, A V ; Nikumbh, A K ; Karale, N J ; Khanvilkar, M B ; Deshpande, A S ; Nagwade, P A</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c234w-e9fe67e771659e65067b4ad7f2d53f689bf571d55e8d613ecc43fdbec97565683</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2022</creationdate><topic>Cerium compounds</topic><topic>Chemistry and Materials Science</topic><topic>Coprecipitation</topic><topic>Decomposition</topic><topic>Differential thermal analysis</topic><topic>Dispersants</topic><topic>Distilled water</topic><topic>Emission analysis</topic><topic>Energy dispersive X ray analysis</topic><topic>Engineering</topic><topic>Ethanol</topic><topic>Fourier transforms</topic><topic>Infrared analysis</topic><topic>Infrared spectroscopy</topic><topic>Investigations</topic><topic>Laser applications</topic><topic>Materials Science</topic><topic>Mixed oxides</topic><topic>Particle size</topic><topic>Polyethylene</topic><topic>Rheological properties</topic><topic>Rheology</topic><topic>Sedimentation & deposition</topic><topic>Sensors</topic><topic>Shear rate</topic><topic>Spectroscopic analysis</topic><topic>Spectrum analysis</topic><topic>Thermogravimetric analysis</topic><topic>Titanium</topic><topic>Vanadates</topic><topic>Viscosity</topic><topic>X ray analysis</topic><topic>X ray powder diffraction</topic><topic>X-ray fluorescence</topic><topic>Zirconium</topic><topic>Zirconium titanates</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Nagawade, A V</creatorcontrib><creatorcontrib>Nikumbh, A K</creatorcontrib><creatorcontrib>Karale, N J</creatorcontrib><creatorcontrib>Khanvilkar, M B</creatorcontrib><creatorcontrib>Deshpande, A S</creatorcontrib><creatorcontrib>Nagwade, P A</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><jtitle>Bulletin of materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Nagawade, A V</au><au>Nikumbh, A K</au><au>Karale, N J</au><au>Khanvilkar, M B</au><au>Deshpande, A S</au><au>Nagwade, P A</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>An investigation of the formation, the particulate properties and the rheological behaviour of cerium vanadate and zirconium titanate prepared by dicarboxylate coprecipitation method</atitle><jtitle>Bulletin of materials science</jtitle><stitle>Bull Mater Sci</stitle><date>2022-06-01</date><risdate>2022</risdate><volume>45</volume><issue>2</issue><spage>92</spage><pages>92-</pages><artnum>92</artnum><issn>0973-7669</issn><issn>0250-4707</issn><eissn>0973-7669</eissn><abstract>Cerium vanadate (CeVO
4
) and zirconium titanate (ZrTiO
4
) powders have been synthesized by the dicarboxylate coprecipitation method. The formation of precursors and mixed oxides was confirmed by their elemental and thermal analysis (thermogravimetric analysis–differential thermal analysis), infrared spectroscopy (Fourier transform infrared), X-ray fluorescence spectroscopy, energy-dispersive X-ray analysis and powder X-ray diffraction. X-ray analysis reveals the formation of a single-phasic CeVO
4
with tetragonal structure and ZrTiO
4
with orthorhombic structure. The morphological characteristics of these oxides were studied by field-emission scanning electron microscopy and a laser-based particle size analyzer. Different solid content and dispersants have been used to prepare various suspensions of these oxides in distilled water and ethanol. The rheological flow behaviour of the suspensions has been studied by measuring their viscosity against the increasing shear rate. The power-law model is applied to calculate consistency coefficient (
k
) and flow behaviour index (
n
). Minimum viscosities have been observed at pH = 10.6 for CeVO
4
–water–Darvan system and at pH = 10.5 for ZrTiO
4
–water–polyethylene imine system.
Graphic abstract</abstract><cop>Bangalore</cop><pub>Indian Academy of Sciences</pub><doi>10.1007/s12034-021-02641-w</doi><orcidid>https://orcid.org/0000-0003-1036-7079</orcidid></addata></record> |
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| identifier | ISSN: 0973-7669 |
| ispartof | Bulletin of materials science, 2022-06, Vol.45 (2), p.92, Article 92 |
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| source | Indian Academy of Sciences; SpringerLink; Free Full-Text Journals in Chemistry; EZB Electronic Journals Library; ProQuest Central |
| subjects | Cerium compounds Chemistry and Materials Science Coprecipitation Decomposition Differential thermal analysis Dispersants Distilled water Emission analysis Energy dispersive X ray analysis Engineering Ethanol Fourier transforms Infrared analysis Infrared spectroscopy Investigations Laser applications Materials Science Mixed oxides Particle size Polyethylene Rheological properties Rheology Sedimentation & deposition Sensors Shear rate Spectroscopic analysis Spectrum analysis Thermogravimetric analysis Titanium Vanadates Viscosity X ray analysis X ray powder diffraction X-ray fluorescence Zirconium Zirconium titanates |
| title | An investigation of the formation, the particulate properties and the rheological behaviour of cerium vanadate and zirconium titanate prepared by dicarboxylate coprecipitation method |
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