Synthesis, characterization and gas sensing performance of aluminosilicate azide cancrinite
The present investigation deals with synthesis and gas sensing performance of Na 8 [AlSiO 4 ] 6 (N 3 ) 2.4 (H 2 O) 4.6 cancrinite-based thick film. The product obtained was characterized by Fourier transform infrared spectroscopy, X-ray diffraction, scanning electron microscope, thermogravimetric an...
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| Veröffentlicht in: | Bulletin of materials science 2016-10, Vol.39 (6), p.1557-1563 |
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| creator | BORHADE, A V KSHIRSAGAR, T A WAKCHAURE, S G DHOLI, A G |
| description | The present investigation deals with synthesis and gas sensing performance of Na
8
[AlSiO
4
]
6
(N
3
)
2.4
(H
2
O)
4.6
cancrinite-based thick film. The product obtained was characterized by Fourier transform infrared spectroscopy, X-ray diffraction, scanning electron microscope, thermogravimetric analysis and magic-angle spin nuclear magnetic resonance (MAS NMR). The crystal structure of the product was determined from X-ray powder diffraction data by applying Rietveld refinement. Refinement showed that azide cancrinite crystallize in the space group P6
3
. Alternate arrangement of Si and Al atoms was confirmed by single intense peak of MAS NMR analysis. For the first time, this study reports the gas sensing performance of aluminosilicate azide cancrinite. The effect of annealing and operating temperature on gas sensing characteristic of azide cancrinite thick film is investigated systematically for various gases at different operating temperatures. This sensor was observed to be highly sensitive and selective to ammonia gas. |
| doi_str_mv | 10.1007/s12034-016-1281-0 |
| format | Article |
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8
[AlSiO
4
]
6
(N
3
)
2.4
(H
2
O)
4.6
cancrinite-based thick film. The product obtained was characterized by Fourier transform infrared spectroscopy, X-ray diffraction, scanning electron microscope, thermogravimetric analysis and magic-angle spin nuclear magnetic resonance (MAS NMR). The crystal structure of the product was determined from X-ray powder diffraction data by applying Rietveld refinement. Refinement showed that azide cancrinite crystallize in the space group P6
3
. Alternate arrangement of Si and Al atoms was confirmed by single intense peak of MAS NMR analysis. For the first time, this study reports the gas sensing performance of aluminosilicate azide cancrinite. The effect of annealing and operating temperature on gas sensing characteristic of azide cancrinite thick film is investigated systematically for various gases at different operating temperatures. This sensor was observed to be highly sensitive and selective to ammonia gas.</description><identifier>ISSN: 0250-4707</identifier><identifier>EISSN: 0973-7669</identifier><identifier>DOI: 10.1007/s12034-016-1281-0</identifier><language>eng</language><publisher>Bangalore, India: Indian Academy of Sciences</publisher><subject>Aluminosilicates ; Aluminum silicates ; Ammonia ; Chemistry and Materials Science ; Crystal structure ; Decomposition ; Electron spin ; Engineering ; Fourier transforms ; Gas sensors ; Gases ; Glass substrates ; Infrared analysis ; Materials Science ; NMR ; NMR spectroscopy ; Nuclear magnetic resonance ; Operating temperature ; Screen printing ; Sensors ; Sodium ; Spectrum analysis ; Synthesis ; Temperature ; Thermogravimetric analysis ; Thin film coatings ; X ray powder diffraction ; Zeolites</subject><ispartof>Bulletin of materials science, 2016-10, Vol.39 (6), p.1557-1563</ispartof><rights>Indian Academy of Sciences 2016</rights><rights>Indian Academy of Sciences 2016.</rights><lds50>peer_reviewed</lds50><oa>free_for_read</oa><woscitedreferencessubscribed>false</woscitedreferencessubscribed><citedby>FETCH-LOGICAL-c425t-7bf2b610f5f26725b87c5f39693ec6621e98d88a010fada66d3331c32b1a531d3</citedby><cites>FETCH-LOGICAL-c425t-7bf2b610f5f26725b87c5f39693ec6621e98d88a010fada66d3331c32b1a531d3</cites></display><links><openurl>$$Topenurl_article</openurl><openurlfulltext>$$Topenurlfull_article</openurlfulltext><thumbnail>$$Tsyndetics_thumb_exl</thumbnail><linktopdf>$$Uhttps://www.proquest.com/docview/2919717069/fulltextPDF?pq-origsite=primo$$EPDF$$P50$$Gproquest$$H</linktopdf><linktohtml>$$Uhttps://www.proquest.com/docview/2919717069?pq-origsite=primo$$EHTML$$P50$$Gproquest$$H</linktohtml><link.rule.ids>314,776,780,21368,27903,27904,33723,41467,42536,43784,51297,64361,64365,72215,74048</link.rule.ids></links><search><creatorcontrib>BORHADE, A V</creatorcontrib><creatorcontrib>KSHIRSAGAR, T A</creatorcontrib><creatorcontrib>WAKCHAURE, S G</creatorcontrib><creatorcontrib>DHOLI, A G</creatorcontrib><title>Synthesis, characterization and gas sensing performance of aluminosilicate azide cancrinite</title><title>Bulletin of materials science</title><addtitle>Bull Mater Sci</addtitle><description>The present investigation deals with synthesis and gas sensing performance of Na
8
[AlSiO
4
]
6
(N
3
)
2.4
(H
2
O)
4.6
cancrinite-based thick film. The product obtained was characterized by Fourier transform infrared spectroscopy, X-ray diffraction, scanning electron microscope, thermogravimetric analysis and magic-angle spin nuclear magnetic resonance (MAS NMR). The crystal structure of the product was determined from X-ray powder diffraction data by applying Rietveld refinement. Refinement showed that azide cancrinite crystallize in the space group P6
3
. Alternate arrangement of Si and Al atoms was confirmed by single intense peak of MAS NMR analysis. For the first time, this study reports the gas sensing performance of aluminosilicate azide cancrinite. The effect of annealing and operating temperature on gas sensing characteristic of azide cancrinite thick film is investigated systematically for various gases at different operating temperatures. This sensor was observed to be highly sensitive and selective to ammonia gas.</description><subject>Aluminosilicates</subject><subject>Aluminum silicates</subject><subject>Ammonia</subject><subject>Chemistry and Materials Science</subject><subject>Crystal structure</subject><subject>Decomposition</subject><subject>Electron spin</subject><subject>Engineering</subject><subject>Fourier transforms</subject><subject>Gas sensors</subject><subject>Gases</subject><subject>Glass substrates</subject><subject>Infrared analysis</subject><subject>Materials Science</subject><subject>NMR</subject><subject>NMR spectroscopy</subject><subject>Nuclear magnetic resonance</subject><subject>Operating temperature</subject><subject>Screen printing</subject><subject>Sensors</subject><subject>Sodium</subject><subject>Spectrum analysis</subject><subject>Synthesis</subject><subject>Temperature</subject><subject>Thermogravimetric analysis</subject><subject>Thin film coatings</subject><subject>X ray powder diffraction</subject><subject>Zeolites</subject><issn>0250-4707</issn><issn>0973-7669</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2016</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNp1kE1LAzEQhoMoWKs_wFvAq9FMsptsjlL8goIH9eQhZLNJm9Jma7I9tL_elBU8eZqBed534EHoGugdUCrvMzDKK0JBEGANEHqCJlRJTqQQ6rTsrKakklSeo4ucV5SCqiqYoK_3fRyWLod8i-3SJGMHl8LBDKGP2MQOL0zG2cUc4gJvXfJ92phoHe49NuvdJsQ-h3WwZnDYHELnsC3nFGIY3CU682ad3dXvnKLPp8eP2QuZvz2_zh7mxFasHohsPWsFUF97JiSr20ba2nMlFHdWCAZONV3TGFoQ0xkhOs45WM5aMDWHjk_Rzdi7Tf33zuVBr_pdiuWlZgqUBElL1xTBSNnU55yc19sUNibtNVB9dKhHh7o41EeHmpYMGzO5sHHh0l_z_6EfhdR03w</recordid><startdate>20161001</startdate><enddate>20161001</enddate><creator>BORHADE, A V</creator><creator>KSHIRSAGAR, T A</creator><creator>WAKCHAURE, S G</creator><creator>DHOLI, A G</creator><general>Indian Academy of Sciences</general><general>Springer Nature B.V</general><scope>AAYXX</scope><scope>CITATION</scope><scope>7SR</scope><scope>8BQ</scope><scope>8FD</scope><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>CCPQU</scope><scope>D1I</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>JG9</scope><scope>KB.</scope><scope>PDBOC</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope></search><sort><creationdate>20161001</creationdate><title>Synthesis, characterization and gas sensing performance of aluminosilicate azide cancrinite</title><author>BORHADE, A V ; KSHIRSAGAR, T A ; WAKCHAURE, S G ; DHOLI, A G</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-LOGICAL-c425t-7bf2b610f5f26725b87c5f39693ec6621e98d88a010fada66d3331c32b1a531d3</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2016</creationdate><topic>Aluminosilicates</topic><topic>Aluminum silicates</topic><topic>Ammonia</topic><topic>Chemistry and Materials Science</topic><topic>Crystal structure</topic><topic>Decomposition</topic><topic>Electron spin</topic><topic>Engineering</topic><topic>Fourier transforms</topic><topic>Gas sensors</topic><topic>Gases</topic><topic>Glass substrates</topic><topic>Infrared analysis</topic><topic>Materials Science</topic><topic>NMR</topic><topic>NMR spectroscopy</topic><topic>Nuclear magnetic resonance</topic><topic>Operating temperature</topic><topic>Screen printing</topic><topic>Sensors</topic><topic>Sodium</topic><topic>Spectrum analysis</topic><topic>Synthesis</topic><topic>Temperature</topic><topic>Thermogravimetric analysis</topic><topic>Thin film coatings</topic><topic>X ray powder diffraction</topic><topic>Zeolites</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>BORHADE, A V</creatorcontrib><creatorcontrib>KSHIRSAGAR, T A</creatorcontrib><creatorcontrib>WAKCHAURE, S G</creatorcontrib><creatorcontrib>DHOLI, A G</creatorcontrib><collection>CrossRef</collection><collection>Engineered Materials Abstracts</collection><collection>METADEX</collection><collection>Technology Research Database</collection><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Materials Science Collection</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>Materials Research Database</collection><collection>Materials Science Database</collection><collection>Materials Science Collection</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><jtitle>Bulletin of materials science</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>BORHADE, A V</au><au>KSHIRSAGAR, T A</au><au>WAKCHAURE, S G</au><au>DHOLI, A G</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis, characterization and gas sensing performance of aluminosilicate azide cancrinite</atitle><jtitle>Bulletin of materials science</jtitle><stitle>Bull Mater Sci</stitle><date>2016-10-01</date><risdate>2016</risdate><volume>39</volume><issue>6</issue><spage>1557</spage><epage>1563</epage><pages>1557-1563</pages><issn>0250-4707</issn><eissn>0973-7669</eissn><abstract>The present investigation deals with synthesis and gas sensing performance of Na
8
[AlSiO
4
]
6
(N
3
)
2.4
(H
2
O)
4.6
cancrinite-based thick film. The product obtained was characterized by Fourier transform infrared spectroscopy, X-ray diffraction, scanning electron microscope, thermogravimetric analysis and magic-angle spin nuclear magnetic resonance (MAS NMR). The crystal structure of the product was determined from X-ray powder diffraction data by applying Rietveld refinement. Refinement showed that azide cancrinite crystallize in the space group P6
3
. Alternate arrangement of Si and Al atoms was confirmed by single intense peak of MAS NMR analysis. For the first time, this study reports the gas sensing performance of aluminosilicate azide cancrinite. The effect of annealing and operating temperature on gas sensing characteristic of azide cancrinite thick film is investigated systematically for various gases at different operating temperatures. This sensor was observed to be highly sensitive and selective to ammonia gas.</abstract><cop>Bangalore, India</cop><pub>Indian Academy of Sciences</pub><doi>10.1007/s12034-016-1281-0</doi><tpages>7</tpages><oa>free_for_read</oa></addata></record> |
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| language | eng |
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| source | SpringerLink Journals; Elektronische Zeitschriftenbibliothek - Frei zugängliche E-Journals; Indian Academy of Sciences; ProQuest Central UK/Ireland; Free Full-Text Journals in Chemistry; ProQuest Central |
| subjects | Aluminosilicates Aluminum silicates Ammonia Chemistry and Materials Science Crystal structure Decomposition Electron spin Engineering Fourier transforms Gas sensors Gases Glass substrates Infrared analysis Materials Science NMR NMR spectroscopy Nuclear magnetic resonance Operating temperature Screen printing Sensors Sodium Spectrum analysis Synthesis Temperature Thermogravimetric analysis Thin film coatings X ray powder diffraction Zeolites |
| title | Synthesis, characterization and gas sensing performance of aluminosilicate azide cancrinite |
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