Synthesis and structural characterization of Znb3Nb2 powder
Zinc nitride (Znb3Nb2) powder has been synthesized through the nitridation reaction of Zn powder with NH3 gas (at the flow rate of 500 ml/min) at the nitridation temperature of 600 for 120 min. X-ray diffraction (XRD) indicates that Znb3Nb2 is cubic in structure with the lattice constant being a = 0...
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Veröffentlicht in: | Science China. Physics, mechanics & astronomy mechanics & astronomy, 2005-04, Vol.48 (2), p.201-210 |
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container_title | Science China. Physics, mechanics & astronomy |
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creator | Zong, Fujian Ma, Honglei Xue, Chengshan Zhuang, Huizhao Zhang, Xijian Ma, Jin Ji, Feng Xiao, Hongdi |
description | Zinc nitride (Znb3Nb2) powder has been synthesized through the nitridation reaction of Zn powder with NH3 gas (at the flow rate of 500 ml/min) at the nitridation temperature of 600 for 120 min. X-ray diffraction (XRD) indicates that Znb3Nb2 is cubic in structure with the lattice constant being a = 0.9788 nm. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) show that Znb3Nb2 powder has surface morphology of various types. X-ray photoelectron spectroscopy (XPS) shows the differences in chemical bonding states between Znb3Nb2 and ZnO, and confirms the formation of N–Zn bonds. Observation through high resolution transmission electron microscopy (HRTEM) also indicates that the computer simulation of the structure of Znb3Nb2 is consistent with the structural model put forward by Partin. |
doi_str_mv | 10.1360/04yw0095 |
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X-ray diffraction (XRD) indicates that Znb3Nb2 is cubic in structure with the lattice constant being a = 0.9788 nm. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) show that Znb3Nb2 powder has surface morphology of various types. X-ray photoelectron spectroscopy (XPS) shows the differences in chemical bonding states between Znb3Nb2 and ZnO, and confirms the formation of N–Zn bonds. Observation through high resolution transmission electron microscopy (HRTEM) also indicates that the computer simulation of the structure of Znb3Nb2 is consistent with the structural model put forward by Partin.</description><identifier>ISSN: 1674-7348</identifier><identifier>EISSN: 1869-1927</identifier><identifier>DOI: 10.1360/04yw0095</identifier><language>eng</language><publisher>Beijing: Springer Nature B.V</publisher><subject>Ammonia ; Chemical bonds ; Cubic lattice ; Flow rates ; High resolution electron microscopy ; Lattice parameters ; Photoelectrons ; Structural analysis ; Structural models ; Transmission electron microscopy ; X ray photoelectron spectroscopy ; X-ray diffraction ; Zinc nitride ; Zinc oxide</subject><ispartof>Science China. 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Physics, mechanics & astronomy</title><description>Zinc nitride (Znb3Nb2) powder has been synthesized through the nitridation reaction of Zn powder with NH3 gas (at the flow rate of 500 ml/min) at the nitridation temperature of 600 for 120 min. X-ray diffraction (XRD) indicates that Znb3Nb2 is cubic in structure with the lattice constant being a = 0.9788 nm. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) show that Znb3Nb2 powder has surface morphology of various types. X-ray photoelectron spectroscopy (XPS) shows the differences in chemical bonding states between Znb3Nb2 and ZnO, and confirms the formation of N–Zn bonds. Observation through high resolution transmission electron microscopy (HRTEM) also indicates that the computer simulation of the structure of Znb3Nb2 is consistent with the structural model put forward by Partin.</description><subject>Ammonia</subject><subject>Chemical bonds</subject><subject>Cubic lattice</subject><subject>Flow rates</subject><subject>High resolution electron microscopy</subject><subject>Lattice parameters</subject><subject>Photoelectrons</subject><subject>Structural analysis</subject><subject>Structural models</subject><subject>Transmission electron microscopy</subject><subject>X ray photoelectron spectroscopy</subject><subject>X-ray diffraction</subject><subject>Zinc nitride</subject><subject>Zinc oxide</subject><issn>1674-7348</issn><issn>1869-1927</issn><fulltext>true</fulltext><rsrctype>article</rsrctype><creationdate>2005</creationdate><recordtype>article</recordtype><sourceid>AFKRA</sourceid><sourceid>BENPR</sourceid><sourceid>CCPQU</sourceid><sourceid>DWQXO</sourceid><recordid>eNqNjr0KwjAYRYMoWLTgIwScq1-a9Cc4iuLkopNLSduUtpSkJimlPr0dfADvcg_cM1yEdgQOhMZwBDaNADxaII-kMQ8ID5PlzHHCgoSydI18a1uYQzmwhHno9JiUq6VtLBaqxNaZoXCDER0uamFE4aRpPsI1WmFd4ZfK6T0Pca_HUpotWlWis9L_9Qbtr5fn-Rb0Rr8HaV3W6sGoecpCPv8BDhGn_1lfjzw9Mw</recordid><startdate>20050401</startdate><enddate>20050401</enddate><creator>Zong, Fujian</creator><creator>Ma, Honglei</creator><creator>Xue, Chengshan</creator><creator>Zhuang, Huizhao</creator><creator>Zhang, Xijian</creator><creator>Ma, Jin</creator><creator>Ji, Feng</creator><creator>Xiao, Hongdi</creator><general>Springer Nature B.V</general><scope>8FE</scope><scope>8FG</scope><scope>ABJCF</scope><scope>AFKRA</scope><scope>ARAPS</scope><scope>BENPR</scope><scope>BGLVJ</scope><scope>BHPHI</scope><scope>BKSAR</scope><scope>CCPQU</scope><scope>DWQXO</scope><scope>HCIFZ</scope><scope>L6V</scope><scope>M7S</scope><scope>P5Z</scope><scope>P62</scope><scope>PCBAR</scope><scope>PQEST</scope><scope>PQQKQ</scope><scope>PQUKI</scope><scope>PTHSS</scope></search><sort><creationdate>20050401</creationdate><title>Synthesis and structural characterization of Znb3Nb2 powder</title><author>Zong, Fujian ; Ma, Honglei ; Xue, Chengshan ; Zhuang, Huizhao ; Zhang, Xijian ; Ma, Jin ; Ji, Feng ; Xiao, Hongdi</author></sort><facets><frbrtype>5</frbrtype><frbrgroupid>cdi_FETCH-proquest_journals_29186090593</frbrgroupid><rsrctype>articles</rsrctype><prefilter>articles</prefilter><language>eng</language><creationdate>2005</creationdate><topic>Ammonia</topic><topic>Chemical bonds</topic><topic>Cubic lattice</topic><topic>Flow rates</topic><topic>High resolution electron microscopy</topic><topic>Lattice parameters</topic><topic>Photoelectrons</topic><topic>Structural analysis</topic><topic>Structural models</topic><topic>Transmission electron microscopy</topic><topic>X ray photoelectron spectroscopy</topic><topic>X-ray diffraction</topic><topic>Zinc nitride</topic><topic>Zinc oxide</topic><toplevel>peer_reviewed</toplevel><toplevel>online_resources</toplevel><creatorcontrib>Zong, Fujian</creatorcontrib><creatorcontrib>Ma, Honglei</creatorcontrib><creatorcontrib>Xue, Chengshan</creatorcontrib><creatorcontrib>Zhuang, Huizhao</creatorcontrib><creatorcontrib>Zhang, Xijian</creatorcontrib><creatorcontrib>Ma, Jin</creatorcontrib><creatorcontrib>Ji, Feng</creatorcontrib><creatorcontrib>Xiao, Hongdi</creatorcontrib><collection>ProQuest SciTech Collection</collection><collection>ProQuest Technology Collection</collection><collection>Materials Science & Engineering Collection</collection><collection>ProQuest Central UK/Ireland</collection><collection>Advanced Technologies & Aerospace Collection</collection><collection>ProQuest Central</collection><collection>Technology Collection</collection><collection>Natural Science Collection</collection><collection>Earth, Atmospheric & Aquatic Science Collection</collection><collection>ProQuest One Community College</collection><collection>ProQuest Central Korea</collection><collection>SciTech Premium Collection</collection><collection>ProQuest Engineering Collection</collection><collection>Engineering Database</collection><collection>Advanced Technologies & Aerospace Database</collection><collection>ProQuest Advanced Technologies & Aerospace Collection</collection><collection>Earth, Atmospheric & Aquatic Science Database</collection><collection>ProQuest One Academic Eastern Edition (DO NOT USE)</collection><collection>ProQuest One Academic</collection><collection>ProQuest One Academic UKI Edition</collection><collection>Engineering Collection</collection><jtitle>Science China. Physics, mechanics & astronomy</jtitle></facets><delivery><delcategory>Remote Search Resource</delcategory><fulltext>fulltext</fulltext></delivery><addata><au>Zong, Fujian</au><au>Ma, Honglei</au><au>Xue, Chengshan</au><au>Zhuang, Huizhao</au><au>Zhang, Xijian</au><au>Ma, Jin</au><au>Ji, Feng</au><au>Xiao, Hongdi</au><format>journal</format><genre>article</genre><ristype>JOUR</ristype><atitle>Synthesis and structural characterization of Znb3Nb2 powder</atitle><jtitle>Science China. Physics, mechanics & astronomy</jtitle><date>2005-04-01</date><risdate>2005</risdate><volume>48</volume><issue>2</issue><spage>201</spage><epage>210</epage><pages>201-210</pages><issn>1674-7348</issn><eissn>1869-1927</eissn><abstract>Zinc nitride (Znb3Nb2) powder has been synthesized through the nitridation reaction of Zn powder with NH3 gas (at the flow rate of 500 ml/min) at the nitridation temperature of 600 for 120 min. X-ray diffraction (XRD) indicates that Znb3Nb2 is cubic in structure with the lattice constant being a = 0.9788 nm. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) show that Znb3Nb2 powder has surface morphology of various types. X-ray photoelectron spectroscopy (XPS) shows the differences in chemical bonding states between Znb3Nb2 and ZnO, and confirms the formation of N–Zn bonds. Observation through high resolution transmission electron microscopy (HRTEM) also indicates that the computer simulation of the structure of Znb3Nb2 is consistent with the structural model put forward by Partin.</abstract><cop>Beijing</cop><pub>Springer Nature B.V</pub><doi>10.1360/04yw0095</doi></addata></record> |
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subjects | Ammonia Chemical bonds Cubic lattice Flow rates High resolution electron microscopy Lattice parameters Photoelectrons Structural analysis Structural models Transmission electron microscopy X ray photoelectron spectroscopy X-ray diffraction Zinc nitride Zinc oxide |
title | Synthesis and structural characterization of Znb3Nb2 powder |
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