Long-term stability study on a Perna perna mussel candidate reference material

The long-term stability study, one of the steps in the characterization of new reference materials, is performed on freeze-dried biological reference materials to verify if they may be stored at room temperature without modification of the property values of interest. In this study, instrumental neu...

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Veröffentlicht in:Accreditation and quality assurance 2010-04, Vol.15 (4), p.233-238
Hauptverfasser: Moreira, Edson Gonçalves, Vasconcellos, M. B. A., Catharino, M. G. M., Maihara, V. A., Saiki, M.
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container_end_page 238
container_issue 4
container_start_page 233
container_title Accreditation and quality assurance
container_volume 15
creator Moreira, Edson Gonçalves
Vasconcellos, M. B. A.
Catharino, M. G. M.
Maihara, V. A.
Saiki, M.
description The long-term stability study, one of the steps in the characterization of new reference materials, is performed on freeze-dried biological reference materials to verify if they may be stored at room temperature without modification of the property values of interest. In this study, instrumental neutron activation analysis was used in a 12-month long isochronous long-term stability study performed on a Perna perna mussel candidate reference material. No trend in the results was observed in respect to measurement order and exposition period to room temperature. The assessment of the analysis of variance test as well as the normalized results to the control temperature showed no systematic changes in the mass fractions of Ag, As, Br, Co, Cr, Cs, Fe, Eu, La, Na, Rb, Sc, Se, Th and Zn during the test period. The result showed that the candidate reference material may be stored at room temperature without significant changes in composition for the determined elements.
doi_str_mv 10.1007/s00769-009-0628-2
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subjects Analytical Chemistry
Biochemistry
Chemistry
Chemistry and Materials Science
Commercial Law
Ecotoxicology
Exact sciences and technology
Food Science
Gamma rays
Hypotheses
Marketing
Mollusks
Neutron activation analysis
Neutrons
Polyethylene
Practitioner's Report
Property values
Radiochemical methods
Reference materials
Regression analysis
Room temperature
Spectrum analysis
Stability analysis
Temperature
Trends
Variance analysis
title Long-term stability study on a Perna perna mussel candidate reference material
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