Controlled release study of phenol formaldehyde based microcapsules containing various loading percentage of core cypermethrin at different agitation rates

s Cypermethrin is a synthetic pyrethroid that acts as a neurotoxin and is used on large scale in both agricultural and domestic purposes. It is easily degraded on soil and plants but can be effective for weeks when applied to indoor inert surfaces. Sometimes it develops tingling, burning, dizziness,...

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Veröffentlicht in:Polymer bulletin (Berlin, Germany) Germany), 2019-05, Vol.76 (5), p.2519-2536
Hauptverfasser: Karandikar, Pravin S., Rajput, Jamatsing D., Bagul, Suresh D., Gite, Vikas V., Bendre, Ratnamala S.
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container_issue 5
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container_title Polymer bulletin (Berlin, Germany)
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creator Karandikar, Pravin S.
Rajput, Jamatsing D.
Bagul, Suresh D.
Gite, Vikas V.
Bendre, Ratnamala S.
description s Cypermethrin is a synthetic pyrethroid that acts as a neurotoxin and is used on large scale in both agricultural and domestic purposes. It is easily degraded on soil and plants but can be effective for weeks when applied to indoor inert surfaces. Sometimes it develops tingling, burning, dizziness, and itching to the operator which is why there is a need to develop a safe and effective formulation, which can release cypermethrin under controlled conditions. In this communication, we report a successful encapsulation of cypermethrin within shell of phenol formaldehyde (PF). A series of PF microcapsules have been prepared at various loading percentage and varying agitation rates by in situ polymerization. The formulation consists of mainly two parts, namely emulsification of the oil and wall formation. The morphology of formulated microcapsules was confirmed initially by observing under optical microscope and further with FESEM, which indicated spherical shape, smooth surface, and rigid nature to the microcapsules. The microcapsules were characterized by FTIR, TGA, and particle size analyzer. Release rate of cypermethrin from polymeric microcapsules was calculated by UV spectrophotometer and also by a simple gravimetric method. The stable, safe, and controlled release formulation of easily degradable, highly burning and etching cypermethrin is the success of our present work. Graphical abstract
doi_str_mv 10.1007/s00289-018-2508-6
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It is easily degraded on soil and plants but can be effective for weeks when applied to indoor inert surfaces. Sometimes it develops tingling, burning, dizziness, and itching to the operator which is why there is a need to develop a safe and effective formulation, which can release cypermethrin under controlled conditions. In this communication, we report a successful encapsulation of cypermethrin within shell of phenol formaldehyde (PF). A series of PF microcapsules have been prepared at various loading percentage and varying agitation rates by in situ polymerization. The formulation consists of mainly two parts, namely emulsification of the oil and wall formation. The morphology of formulated microcapsules was confirmed initially by observing under optical microscope and further with FESEM, which indicated spherical shape, smooth surface, and rigid nature to the microcapsules. The microcapsules were characterized by FTIR, TGA, and particle size analyzer. Release rate of cypermethrin from polymeric microcapsules was calculated by UV spectrophotometer and also by a simple gravimetric method. The stable, safe, and controlled release formulation of easily degradable, highly burning and etching cypermethrin is the success of our present work. 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Bull</addtitle><description>s Cypermethrin is a synthetic pyrethroid that acts as a neurotoxin and is used on large scale in both agricultural and domestic purposes. It is easily degraded on soil and plants but can be effective for weeks when applied to indoor inert surfaces. Sometimes it develops tingling, burning, dizziness, and itching to the operator which is why there is a need to develop a safe and effective formulation, which can release cypermethrin under controlled conditions. In this communication, we report a successful encapsulation of cypermethrin within shell of phenol formaldehyde (PF). A series of PF microcapsules have been prepared at various loading percentage and varying agitation rates by in situ polymerization. The formulation consists of mainly two parts, namely emulsification of the oil and wall formation. 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subjects Agitation
Aqueous solutions
Characterization and Evaluation of Materials
Chemistry
Chemistry and Materials Science
Complex Fluids and Microfluidics
Controlled release
Emulsion polymerization
Itching
Microencapsulation
Morphology
Optical microscopes
Organic Chemistry
Original Paper
Particle size
Phenol formaldehyde
Phenols
Physical Chemistry
Polylactic acid
Polymer Sciences
Polymerization
Soft and Granular Matter
Toxins
title Controlled release study of phenol formaldehyde based microcapsules containing various loading percentage of core cypermethrin at different agitation rates
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